SG10201901082VA - Methods for synthesis of graphene derivatives and functional materials from asphaltenes, graphene derivatives, 2d materials and applications of use - Google Patents

Methods for synthesis of graphene derivatives and functional materials from asphaltenes, graphene derivatives, 2d materials and applications of use

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Publication number
SG10201901082VA
SG10201901082VA SG10201901082VA SG10201901082VA SG10201901082VA SG 10201901082V A SG10201901082V A SG 10201901082VA SG 10201901082V A SG10201901082V A SG 10201901082VA SG 10201901082V A SG10201901082V A SG 10201901082VA SG 10201901082V A SG10201901082V A SG 10201901082VA
Authority
SG
Singapore
Prior art keywords
graphene
materials
derivatives
methods
graphene derivatives
Prior art date
Application number
SG10201901082VA
Inventor
Olanrewaju Tanimola
Original Assignee
Olanrewaju Tanimola
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Olanrewaju Tanimola filed Critical Olanrewaju Tanimola
Publication of SG10201901082VA publication Critical patent/SG10201901082VA/en

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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/182—Graphene
    • C01B32/184—Preparation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/158—Carbon nanotubes
    • C01B32/168—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/152—Fullerenes
    • C01B32/156—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/15—Nano-sized carbon materials
    • C01B32/182—Graphene
    • C01B32/194—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/02—Elements
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
    • C30B29/60—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape characterised by shape
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
    • C30B7/02—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by evaporation of the solvent
    • C30B7/06—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by evaporation of the solvent using non-aqueous solvents
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
    • C30B7/14—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions the crystallising materials being formed by chemical reactions in the solution
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/20—Waste processing or separation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/58—Construction or demolition [C&D] waste

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Metallurgy (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

METHODS FOR SYNTHESIS OF GRAPHENE DERIVATIVES AND FUNCTIONAL MATERIALS FROM ASPHALTENES, GRAPHENE DERIVATIVES, D MATERIALS AND APPLICATIONS OF USE Embodiments described are directed to methods for the functionalization of asphaltene materials and to compositions made from functionalized asphaltenes. Disclosed is a method for synthesizing graphene derivatives, such as 2D single crystalline carbon allotropes of graphene and functional materials, such as sulfonic acid and its derivatives. Also disclosed is a method for the transformation of asphaltene into a source of graphene derivatives and functional materials, such as, 0D, 1D, 2D and combinations of 0D and 1D by utilizing chemical substitution reaction mechanism, such as, electrophilic aromatic substitution, nucleophilic aromatic substitution and Sandmeyer mechanism. Also disclosed are novel graphene materials comprising: acetylenic linkage and hydrogenated graphene. These novel materials, which may be produced by these methods, include, e.g.: 2D single crystalline carbon allotropes of graphene with asymmetric unit formulas C 7H6N2O4, C 6H4N2O4, C 7H7O3S- H 3O+, C 7H7O3SH+, and a 2D single crystal with asymmetric unit formula (Na 6O16 S4)n. Fig. 19 77
SG10201901082VA 2014-08-08 2015-08-10 Methods for synthesis of graphene derivatives and functional materials from asphaltenes, graphene derivatives, 2d materials and applications of use SG10201901082VA (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US201462035140P 2014-08-08 2014-08-08

Publications (1)

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SG10201901082VA true SG10201901082VA (en) 2019-03-28

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SG11201701842UA SG11201701842UA (en) 2014-08-08 2015-08-10 Methods for synthesis of graphene derivatives and functional materials from asphaltenes, graphene derivatives, 2d materials and applications of use
SG10201901082VA SG10201901082VA (en) 2014-08-08 2015-08-10 Methods for synthesis of graphene derivatives and functional materials from asphaltenes, graphene derivatives, 2d materials and applications of use

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Country Status (11)

Country Link
US (1) US11479466B2 (en)
EP (1) EP3177563A4 (en)
KR (1) KR20170040348A (en)
CN (1) CN107108219A (en)
AP (1) AP2017009797A0 (en)
AU (1) AU2015300742A1 (en)
CA (2) CA2960807A1 (en)
EA (1) EA201790348A1 (en)
PH (1) PH12017500437A1 (en)
SG (2) SG11201701842UA (en)
WO (1) WO2016023041A2 (en)

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CA3013625C (en) * 2016-02-05 2024-04-09 University Of Miami Carbon dots for diagnostic analysis and drug delivery
DE102016102594A1 (en) * 2016-02-15 2017-08-17 Albert-Ludwigs-Universität Freiburg Process for the preparation of doped graphene oxide and / or graphene
TWI593134B (en) * 2016-05-19 2017-07-21 Method and structure for manufacturing graphene quantum dot on light-emitting diode
CN107903946B (en) * 2017-10-24 2019-09-27 昆明理工大学 A kind of preparation method of montanin wax resin distillate
US11511258B2 (en) 2018-04-04 2022-11-29 King Fahd University Of Petroleum And Minerals Using porous activated asphaltenes as effective adsorbents for the removal of heavy metals in water
CN108584929A (en) * 2018-07-01 2018-09-28 张阳 A kind of production equipment of graphene
CN111333061B (en) * 2018-12-18 2022-08-02 青岛科技大学 Preparation method of graphdiyne film and graphdiyne film
CN110243957B (en) * 2019-05-29 2022-05-10 中国石油天然气股份有限公司 Method for extracting biomarker compounds in high/over-mature asphalt
US11918975B2 (en) 2019-06-18 2024-03-05 Academia Sinica Modified carbonaceous material, carbon dioxide adsorbent and method for cellulose hydrolysis using the same
TWI704955B (en) * 2019-06-18 2020-09-21 中央研究院 Modified carbonaceous material, carbon dioxide adsorbent and method for cellulose hydrolysis using the same
WO2021041897A1 (en) * 2019-08-29 2021-03-04 West Virginia University Process for preparing multicolor, fluorescent carbon quantum dot nanoparticles from coal under mild oxidation conditions
CN110669539B (en) * 2019-10-25 2021-04-02 华东理工大学 Preparation method of isotropic high-softening-point coal pitch
CN111351818B (en) * 2020-04-22 2021-11-12 中山大学 Gas sensor and application thereof in nitrogen dioxide gas detection
CN112275256B (en) * 2020-10-19 2021-10-15 中南大学 Graphite alkyne/aluminum oxide material and preparation method and application thereof
CN114437749B (en) * 2020-11-02 2023-04-11 中国石油化工股份有限公司 Amino-enriched asphalt and preparation method of microspheres thereof
CN112433404B (en) * 2020-11-22 2021-08-27 北京科技大学 Method for preparing wide wave reflection cholesteric liquid crystal film by photo-thermal response technology
CN112777584B (en) * 2021-01-27 2022-08-09 安徽工业大学 Graphene alkyne, preparation method and application thereof
CN114806551A (en) * 2021-06-01 2022-07-29 四川大学 Graphene fluorescent nano material and preparation method and application thereof
CN113528132B (en) * 2021-06-10 2023-07-21 广东碳紫科技有限公司 Oil-soluble ultraviolet absorber
CN114002353A (en) * 2021-10-29 2022-02-01 重庆长安汽车股份有限公司 Qualitative analysis method for semi-volatile organic compounds of non-metallic materials for vehicles
CN114540063B (en) * 2022-03-03 2023-10-31 中国人民解放军96901部队23分队 Preparation method of low-softening-point asphalt for ionization chamber
US11505466B1 (en) * 2022-07-20 2022-11-22 Kuwait Institute For Scientific Research Synthesizing graphene derivatives from asphaltene
CN115583649B (en) * 2022-10-28 2023-09-26 西安科技大学 Method for directly preparing graphene from anthracite
CN117363055B (en) * 2023-10-16 2024-06-04 甘肃省交通规划勘察设计院股份有限公司 Porphyrin modified graphene and preparation method and application thereof

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Publication number Publication date
EA201790348A1 (en) 2018-12-28
EP3177563A2 (en) 2017-06-14
WO2016023041A2 (en) 2016-02-11
WO2016023041A3 (en) 2016-03-31
EP3177563A4 (en) 2018-09-19
CA3189208A1 (en) 2016-02-11
KR20170040348A (en) 2017-04-12
US20160039678A1 (en) 2016-02-11
CN107108219A (en) 2017-08-29
SG11201701842UA (en) 2017-04-27
PH12017500437A1 (en) 2017-07-31
AU2015300742A1 (en) 2017-03-30
US11479466B2 (en) 2022-10-25
AP2017009797A0 (en) 2017-03-31
WO2016023041A4 (en) 2016-05-19
CA2960807A1 (en) 2016-02-11

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