SE9904284D0 - Ceramic insulation in reactors for sub-stoichiometric gasification of residual products from chemical pulp production - Google Patents

Ceramic insulation in reactors for sub-stoichiometric gasification of residual products from chemical pulp production

Info

Publication number
SE9904284D0
SE9904284D0 SE9904284A SE9904284A SE9904284D0 SE 9904284 D0 SE9904284 D0 SE 9904284D0 SE 9904284 A SE9904284 A SE 9904284A SE 9904284 A SE9904284 A SE 9904284A SE 9904284 D0 SE9904284 D0 SE 9904284D0
Authority
SE
Sweden
Prior art keywords
layer
sub
lining
chemical pulp
gasification
Prior art date
Application number
SE9904284A
Other languages
Swedish (sv)
Other versions
SE9904284L (en
Inventor
Bengt Nilsson
Original Assignee
Kvaerner Chemrec Ab
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kvaerner Chemrec Ab filed Critical Kvaerner Chemrec Ab
Priority to SE9904284A priority Critical patent/SE9904284L/en
Publication of SE9904284D0 publication Critical patent/SE9904284D0/en
Priority to PCT/SE2000/002302 priority patent/WO2001037984A1/en
Publication of SE9904284L publication Critical patent/SE9904284L/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10JPRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J3/00Production of combustible gases containing carbon monoxide from solid carbonaceous fuels
    • C10J3/72Other features
    • C10J3/74Construction of shells or jackets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10BDESTRUCTIVE DISTILLATION OF CARBONACEOUS MATERIALS FOR PRODUCTION OF GAS, COKE, TAR, OR SIMILAR MATERIALS
    • C10B29/00Other details of coke ovens
    • C10B29/02Brickwork, e.g. casings, linings, walls
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10JPRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J3/00Production of combustible gases containing carbon monoxide from solid carbonaceous fuels
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10JPRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J3/00Production of combustible gases containing carbon monoxide from solid carbonaceous fuels
    • C10J3/02Fixed-bed gasification of lump fuel
    • C10J3/06Continuous processes
    • C10J3/08Continuous processes with ash-removal in liquid state
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C11/00Regeneration of pulp liquors or effluent waste waters
    • D21C11/12Combustion of pulp liquors
    • D21C11/125Decomposition of the pulp liquors in reducing atmosphere or in the absence of oxidants, i.e. gasification or pyrolysis
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D1/00Casings; Linings; Walls; Roofs
    • F27D1/0003Linings or walls
    • F27D1/0006Linings or walls formed from bricks or layers with a particular composition or specific characteristics
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28FDETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F19/00Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers
    • F28F19/02Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers by using coatings, e.g. vitreous or enamel coatings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00106Controlling the temperature by indirect heat exchange
    • B01J2208/00168Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00203Coils
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00477Controlling the temperature by thermal insulation means
    • B01J2208/00495Controlling the temperature by thermal insulation means using insulating materials or refractories
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00083Coils
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/0015Controlling the temperature by thermal insulation means
    • B01J2219/00155Controlling the temperature by thermal insulation means using insulating materials or refractories
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02Apparatus characterised by their chemically-resistant properties
    • B01J2219/0204Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
    • B01J2219/0218Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components of ceramic
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02Apparatus characterised by their chemically-resistant properties
    • B01J2219/025Apparatus characterised by their chemically-resistant properties characterised by the construction materials of the reactor vessel proper
    • B01J2219/0263Ceramic
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10JPRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J2300/00Details of gasification processes
    • C10J2300/09Details of the feed, e.g. feeding of spent catalyst, inert gas or halogens
    • C10J2300/0913Carbonaceous raw material
    • C10J2300/0946Waste, e.g. MSW, tires, glass, tar sand, peat, paper, lignite, oil shale
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10JPRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J2300/00Details of gasification processes
    • C10J2300/09Details of the feed, e.g. feeding of spent catalyst, inert gas or halogens
    • C10J2300/0953Gasifying agents
    • C10J2300/0973Water
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10JPRODUCTION OF PRODUCER GAS, WATER-GAS, SYNTHESIS GAS FROM SOLID CARBONACEOUS MATERIAL, OR MIXTURES CONTAINING THESE GASES; CARBURETTING AIR OR OTHER GASES
    • C10J2300/00Details of gasification processes
    • C10J2300/09Details of the feed, e.g. feeding of spent catalyst, inert gas or halogens
    • C10J2300/0953Gasifying agents
    • C10J2300/0973Water
    • C10J2300/0979Water as supercritical steam

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Combustion & Propulsion (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Paper (AREA)
  • Furnace Housings, Linings, Walls, And Ceilings (AREA)

Abstract

The present invention relates to an improved lining for a reactor for the sub-stoichiometric gasification of waste liquor or black liquor formed in the manufacture of chemical pulp. The lining is divided into at least one ceramic wear layer (4) having a low porosity, a high density and a high thermal conductivity, which is mounted internally to the reaction chamber, and an outer ceramic backing layer (3) that has a lower density and a lower thermal conductivity. The first and second ceramic layers (4 and 3) have suitable thermal conductivities and thicknesses to ensure that the condensation or solidification point (SP) for the resulting gasification products always lies inside the second layer, irrespective of the effective degree of wear and tear of the first layer. The invention also relates to a process for maintaining the desired temperature profile in the lining.
SE9904284A 1999-11-26 1999-11-26 Ceramic insulation in reactors for sub-stoichiometric gasification of residual products from chemical pulp production SE9904284L (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
SE9904284A SE9904284L (en) 1999-11-26 1999-11-26 Ceramic insulation in reactors for sub-stoichiometric gasification of residual products from chemical pulp production
PCT/SE2000/002302 WO2001037984A1 (en) 1999-11-26 2000-11-23 Ceramic insulation in reactor for gasification of residual products obtained from pulp production

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SE9904284A SE9904284L (en) 1999-11-26 1999-11-26 Ceramic insulation in reactors for sub-stoichiometric gasification of residual products from chemical pulp production

Publications (2)

Publication Number Publication Date
SE9904284D0 true SE9904284D0 (en) 1999-11-26
SE9904284L SE9904284L (en) 2001-05-27

Family

ID=20417865

Family Applications (1)

Application Number Title Priority Date Filing Date
SE9904284A SE9904284L (en) 1999-11-26 1999-11-26 Ceramic insulation in reactors for sub-stoichiometric gasification of residual products from chemical pulp production

Country Status (2)

Country Link
SE (1) SE9904284L (en)
WO (1) WO2001037984A1 (en)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2816041B1 (en) * 2000-10-27 2003-03-14 Novatherm REFRACTORY AND INSULATING LINING COMPRISING A NON-METALLIC WATERPROOFING LAYER AND HEAT TREATMENT OVEN EQUIPPED WITH THE LINING
FR2816040A1 (en) * 2000-10-27 2002-05-03 Novatherm Fireproof cladding, for inner wall of furnace housing, has non-metal sealing layer against wall covered by groups of structured insulating layers to prevent corrosive vapors condensing on wall
SE0203605D0 (en) * 2002-12-04 2002-12-04 Chemrec Ab Device for the gasification or oxidization of an energy containing fuel
ES2237262B1 (en) * 2003-01-31 2006-11-01 Environmental International Engineering, S.L. GASIFICATION REACTOR.
DE10313529A1 (en) * 2003-03-26 2004-10-14 Basf Ag Reactor for high temperature reactions and use
DE10313527A1 (en) * 2003-03-26 2004-10-14 Basf Ag Process for carrying out a high-temperature reaction, reactor for carrying out the process, process for scale-up a reactor and use
DE10313528A1 (en) * 2003-03-26 2004-10-14 Basf Ag Method for scale-up of a reactor for carrying out a high-temperature reaction, reactor and use
SE530199C2 (en) * 2005-09-07 2008-03-25 Chemrec Ab Process for arranging a ceramic barrier in a gasification reactor, chemical reactor comprising such a ceramic barrier and reactor lining intended for use in such a reactor
CN102206516A (en) 2010-03-29 2011-10-05 通用电气公司 Flame shield and gasification device and method

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3048481A (en) * 1958-06-18 1962-08-07 Texaco Inc Method of forming gas tight seal between vessel wall and refractory lining of a synthesis gas generator
FR2389826A1 (en) * 1977-05-03 1978-12-01 Bertin & Cie Furnace wall insulating module - has high density insulating material around low density core
DE3009850C2 (en) * 1980-03-14 1983-04-21 Karrena GmbH, 4000 Düsseldorf Reactor vessel
US4357305A (en) * 1981-03-17 1982-11-02 The United States Of America As Represented By The United States Department Of Energy Coal gasification vessel
US4637823A (en) * 1981-06-19 1987-01-20 Texaco Inc. High temperature furnace
DE3124263A1 (en) * 1981-06-19 1983-01-05 Karrena GmbH, 4000 Düsseldorf LINING FOR A ROUND BURNING ROOM AT LEAST APPROXIMATELY CROSS-SECTIONED
US4840131A (en) * 1986-09-13 1989-06-20 Foseco International Limited Insulating linings for furnaces and kilns
DE3908206A1 (en) * 1989-03-14 1990-10-31 Linn High Therm Gmbh Insulation for a high-temperature heating apparatus, and use of the same
NO172153C (en) * 1989-12-22 1993-06-09 Icelandic Alloys Ltd ILDFAST COATING COMPOSITION IN THE FORM OF A FORMAT OR SPRAY MASS FOR PROTECTION OF LINES IN METAL SURGICAL MOLDS, TAPES AND CASTLE OILS, RUNS AND TAPPETS
CA2017297A1 (en) * 1990-05-22 1991-11-22 Claude Allaire Refractory linings capable of resisting sodium and sodium salts

Also Published As

Publication number Publication date
WO2001037984A1 (en) 2001-05-31
SE9904284L (en) 2001-05-27

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