SE7504666L - SET FOR RELEASE OF A HYDRATION REACTOR. - Google Patents
SET FOR RELEASE OF A HYDRATION REACTOR.Info
- Publication number
- SE7504666L SE7504666L SE7504666A SE7504666A SE7504666L SE 7504666 L SE7504666 L SE 7504666L SE 7504666 A SE7504666 A SE 7504666A SE 7504666 A SE7504666 A SE 7504666A SE 7504666 L SE7504666 L SE 7504666L
- Authority
- SE
- Sweden
- Prior art keywords
- reactor
- temperature
- oxygen
- feed
- purge gas
- Prior art date
Links
- 230000036571 hydration Effects 0.000 title 1
- 238000006703 hydration reaction Methods 0.000 title 1
- 239000007789 gas Substances 0.000 abstract 8
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 5
- 239000003054 catalyst Substances 0.000 abstract 5
- 239000001301 oxygen Substances 0.000 abstract 5
- 229910052760 oxygen Inorganic materials 0.000 abstract 5
- 238000010926 purge Methods 0.000 abstract 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 2
- 239000001257 hydrogen Substances 0.000 abstract 2
- 229910052739 hydrogen Inorganic materials 0.000 abstract 2
- 239000011261 inert gas Substances 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- 239000004215 Carbon black (E152) Substances 0.000 abstract 1
- 239000005864 Sulphur Substances 0.000 abstract 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 1
- 230000003197 catalytic effect Effects 0.000 abstract 1
- 238000009903 catalytic hydrogenation reaction Methods 0.000 abstract 1
- 230000020169 heat generation Effects 0.000 abstract 1
- 229930195733 hydrocarbon Natural products 0.000 abstract 1
- 150000002430 hydrocarbons Chemical class 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000000377 silicon dioxide Substances 0.000 abstract 1
- VRRFSFYSLSPWQY-UHFFFAOYSA-N sulfanylidenecobalt Chemical compound [Co]=S VRRFSFYSLSPWQY-UHFFFAOYSA-N 0.000 abstract 1
- PTISTKLWEJDJID-UHFFFAOYSA-N sulfanylidenemolybdenum Chemical compound [Mo]=S PTISTKLWEJDJID-UHFFFAOYSA-N 0.000 abstract 1
- WWNBZGLDODTKEM-UHFFFAOYSA-N sulfanylidenenickel Chemical compound [Ni]=S WWNBZGLDODTKEM-UHFFFAOYSA-N 0.000 abstract 1
- XCUPBHGRVHYPQC-UHFFFAOYSA-N sulfanylidenetungsten Chemical compound [W]=S XCUPBHGRVHYPQC-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J33/00—Protection of catalysts, e.g. by coating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
- C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Materials Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Catalysts (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
- Steering Control In Accordance With Driving Conditions (AREA)
Abstract
1508021 Passivating catalysts SHELL INTERNATIONALE RESEARCH MAATSCHAPPIJ BV 22 April 1975 [25 April 1974 27 Feb 1975] 16588/75 Headings B1E and B1F A process for taking out of operation a catalyst-filled reactor in which the pyrophoric character of the catalyst is entirely removed, the reactor being used for the catalytic hydrogenation of a liquid or gaseous feed by passing the feed over the catalyst in the presence of added hydrogen comprises (a) if the temperature in the reactor is above 300‹C it is reduced to below 300‹C and kept at below 300‹C until the reactor is opened, (b) the supply of feed is discontinued and the added hydrogen is replaced by an inert gas, before, after or during the said reduction in temperature if the temperature is reduced, (c) the reactor is purged with a purge gas consisting of the inert gas for some time, (d) subsequently an oxygen-comprising gas is introduced into the purge gas in such a quantity that the oxygen content thereof is below 1% by volume whilst the temperature in the reactor is increasing as a result of the presence of oxygen therein, whereby the temperature in the reactor is maintained below 300‹C, (e) when the temperature in the reactor no longer increases as a result of the presence of oxygen therein, the oxygen content of the purge gas is increased and the supply of purge gas is continued until no further appreciable heat generation in the reactor is found to occur, (f) the oxygen partial pressure of the purge gas is brought to at least 0.2 kg/cm<SP>2</SP>, and (g) the reactor is opened. The feed may consist of off-gas from a Claus plant for the preparation of elemental sulphur from sulphur compounds-containing gases or the reactor may have been used for the catalytic desulphurization of liquid hydrocarbon feed. The catalyst may consist of cobalt sulphide and/or nickel sulphide combined with molybdenum sulphide and/or tungsten sulphide, on a carrier at least the greater part of which consists of silica and/or alumina.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NLAANVRAGE7405565,A NL184371C (en) | 1974-04-25 | 1974-04-25 | METHOD FOR DECOMMISSIONING A HYDROGENATION REACTOR, AND A METHOD FOR THE CATALYTIC HYDROGENATION OF A SULFUR COMPOUNDS. |
| NL7502315A NL7502315A (en) | 1975-02-27 | 1975-02-27 | Interrupting operation in catalytic hydrogenation reactors - by cooling purging and slowly introducing oxygen before opening |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| SE7504666L true SE7504666L (en) | 1975-10-27 |
| SE416817B SE416817B (en) | 1981-02-09 |
Family
ID=26644986
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SE7504666A SE416817B (en) | 1974-04-25 | 1975-04-22 | SET FOR COMMISSIONING OF A CATALYST-FILLED REACTOR FOR CATALYTIC HYDRAULATION OF A LIQUID OR GAS-INPUT MATERIAL |
Country Status (10)
| Country | Link |
|---|---|
| JP (1) | JPS5854854B2 (en) |
| CA (1) | CA1062641A (en) |
| DE (1) | DE2517869A1 (en) |
| DK (1) | DK172475A (en) |
| ES (1) | ES436838A1 (en) |
| FR (1) | FR2268859B1 (en) |
| GB (1) | GB1508021A (en) |
| IT (1) | IT1037563B (en) |
| NO (1) | NO146893C (en) |
| SE (1) | SE416817B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3003185B1 (en) * | 2013-03-14 | 2016-06-03 | Air Liquide | PROCESS FOR PROCESSING A CATALYTIC REACTOR |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1144863B (en) * | 1956-01-11 | 1963-03-07 | Exxon Research Engineering Co | Process for the regeneration of catalysts containing molybdenum |
| US3033802A (en) * | 1959-05-22 | 1962-05-08 | Chemetron Corp | Stabilization of reduced metal catalyst and apparatus therefor |
| NL283488A (en) * | 1961-09-21 | |||
| BE757482R (en) * | 1969-04-01 | 1971-03-16 | Chemetron Corp | PROCESS FOR THE PRODUCTION OF REDUCED AND STABILIZED COPPER OXIDE-ZINC OXIDE CATALYZERS FOR THE REACTION OF TRANSFORMATION OF GAS TO WATER AND NEW PRODUCTS THUS OBTAINED |
| NL7104842A (en) * | 1971-04-10 | 1972-10-12 | Passivating pyrophoric powder - by suspending in org liquid and treating with oxygen | |
| US3764558A (en) * | 1971-06-24 | 1973-10-09 | Sun Oil Co Pennsylvania | Constant low oxygen concentration gas regeneration of refining catalysts |
| US3838066A (en) * | 1971-10-01 | 1974-09-24 | Standard Oil Co | Method for stabilizing pyrophoric materials in a catalyst bed |
-
1975
- 1975-03-11 CA CA221,839A patent/CA1062641A/en not_active Expired
- 1975-04-21 IT IT22600/75A patent/IT1037563B/en active
- 1975-04-22 DE DE19752517869 patent/DE2517869A1/en active Granted
- 1975-04-22 FR FR7512474A patent/FR2268859B1/fr not_active Expired
- 1975-04-22 JP JP50048269A patent/JPS5854854B2/en not_active Expired
- 1975-04-22 NO NO751432A patent/NO146893C/en unknown
- 1975-04-22 SE SE7504666A patent/SE416817B/en not_active IP Right Cessation
- 1975-04-22 GB GB16588/75A patent/GB1508021A/en not_active Expired
- 1975-04-22 ES ES436838A patent/ES436838A1/en not_active Expired
- 1975-04-22 DK DK172475A patent/DK172475A/en active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| ES436838A1 (en) | 1976-12-01 |
| JPS5854854B2 (en) | 1983-12-07 |
| DE2517869A1 (en) | 1975-11-13 |
| IT1037563B (en) | 1979-11-20 |
| DE2517869C2 (en) | 1988-02-18 |
| DK172475A (en) | 1975-10-26 |
| JPS50154177A (en) | 1975-12-11 |
| NO751432L (en) | 1975-10-28 |
| NO146893B (en) | 1982-09-20 |
| FR2268859B1 (en) | 1977-04-15 |
| SE416817B (en) | 1981-02-09 |
| CA1062641A (en) | 1979-09-18 |
| FR2268859A1 (en) | 1975-11-21 |
| AU8034175A (en) | 1976-10-28 |
| NO146893C (en) | 1982-12-29 |
| GB1508021A (en) | 1978-04-19 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| NUG | Patent has lapsed |
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