SE537925C2 - Method and system for washing cellulose pulp - Google Patents

Method and system for washing cellulose pulp Download PDF

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Publication number
SE537925C2
SE537925C2 SE1300319A SE1300319A SE537925C2 SE 537925 C2 SE537925 C2 SE 537925C2 SE 1300319 A SE1300319 A SE 1300319A SE 1300319 A SE1300319 A SE 1300319A SE 537925 C2 SE537925 C2 SE 537925C2
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Sweden
Prior art keywords
washing
pulp
processing surface
washing apparatus
storage
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SE1300319A
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Swedish (sv)
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SE1300319A1 (en
Inventor
Anders Hedblom
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Valmet Oy
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Application filed by Valmet Oy filed Critical Valmet Oy
Priority to SE1300319A priority Critical patent/SE537925C2/en
Priority to PCT/SE2014/050510 priority patent/WO2014178780A1/en
Priority to CN201480025159.7A priority patent/CN105189859A/en
Priority to EP14792129.0A priority patent/EP2992136A4/en
Publication of SE1300319A1 publication Critical patent/SE1300319A1/en
Publication of SE537925C2 publication Critical patent/SE537925C2/en

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    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C9/00After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
    • D21C9/02Washing ; Displacing cooking or pulp-treating liquors contained in the pulp by fluids, e.g. wash water or other pulp-treating agents
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C9/00After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
    • D21C9/02Washing ; Displacing cooking or pulp-treating liquors contained in the pulp by fluids, e.g. wash water or other pulp-treating agents
    • D21C9/06Washing ; Displacing cooking or pulp-treating liquors contained in the pulp by fluids, e.g. wash water or other pulp-treating agents in filters ; Washing of concentrated pulp, e.g. pulp mats, on filtering surfaces
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C9/00After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
    • D21C9/18De-watering; Elimination of cooking or pulp-treating liquors from the pulp

Abstract

537 9 SAMMANDRAG En metod och ett system for tvattning av cellulosamassa tillhandahalls. Massan tvattas tva ganger i samma tvattutrymme i en tvattanordning (10) med en rorlig genomslapplig behandlingsyta (11), varvid filtrat fran massan passerar genom behandlingsytan medan massan transporteras tillsammans med behandlingsytan. Det finns en mellanliggande massalagring (20) anslutcn till tvattanordningen (10) och anordnad att lagra massan mcllan de tva tvattmomcnten (I, II). 537 9 SUMMARY A method and system for washing cellulosic pulp is provided. The pulp is washed twice in the same washing space in a washing device (10) with a movable permeable treatment surface (11), whereby filtrate from the pulp passes through the treatment surface while the pulp is transported together with the treatment surface. There is an intermediate mass storage (20) connected to the washing device (10) and arranged to store the mass between the two washing moments (I, II).

Description

537 9 METOD OCH SYSTEM FOR TVATTNING AV CELLULOSAMASSA TEKNISKT OMRADE Foreliggande uppfinning hanfOr sig till behandling av cellulosamassa och sarskilt till en metod och ett system for tvattning av cellulosamassa. TECHNICAL FIELD The present invention relates to the treatment of cellulose pulp and in particular to a method and system for washing cellulose pulp.

BAKGRUND Massatvattning (alien kallad fibertvdttning) är en nyckeloperation vid behandling av cellulosamassa. Tvdttning utfors pa flera stallen i massalinjen, sasom efter kokaren, i sileriet och efter syrgasreaktorer och blektom, fOr att avldgsna lut (med kemikalier, smuts, utlosta substanser, etc.) fran massan. BACKGROUND Pulp watering (alien called fiber washing) is a key operation in the treatment of cellulose pulp. Washing is carried out in several places in the pulp line, such as after the boiler, in the silage and after oxygen reactors and bleaches, in order to remove lye (with chemicals, dirt, discharged substances, etc.) from the pulp.

Marknaden erbjuder manga olika typer av tvdttar, inklusive tvittpressar, avvattningspressar, virapressar, skruvpressar, diffusorer, filter och trumtvdttar. En valkand tvattanordning är en valspress (twin-roll press) av den generella typ som till exempel visas i det amerikanska patentet US 3,980,518. En sadan valspress har tva mot varandra roterande valsar med perforerade ytterytor. Den inkommande massan fordelas pa respektive vats i ldngdriktningen. 2 0En massabana bildas pa respektive vals och transporteras i rotationsriktningen i ett trag som dclvis omslutcr valsarna, fram till dct sa kalladc pressnypct mcllan valsarna. Valspressen anvander tvattprinciperna fortrangning, da smutsig vatska (lut) i massan ersatts av renare tvattvdtska som tillsatts till traget, och pressning, da smutsig vatska pressas/kramas ut fran massan, i synnerhet vid pressnypet. The market offers many different types of washers, including washers, drainage presses, wire presses, screwdrivers, diffusers, filters and drum washers. A roller and washing device is a twin-roll press of the general type shown, for example, in U.S. Pat. No. 3,980,518. Such a roller press has two rotating rollers with perforated outer surfaces. The incoming mass is distributed on each water in the longitudinal direction. A pulp web is formed on the respective roller and is transported in the direction of rotation in a funnel which therefore encloses the rollers, until the so-called press nip between the rollers. The roller press uses the washing principles displacement, when dirty liquid (lye) in the pulp is replaced by cleaner washing liquid added to the hopper, and pressing, when dirty liquid is pressed / squeezed out of the mass, especially at the press nip.

En tvattanordning, som valspressen till exempel, har begransad prestanda. Ibland anordnas tva eller fler tvdttpressar i serie efter varandra i syfte att uppna onskad tvdtteffektivitet. A washing device, such as the roller press, has limited performance. Sometimes two or more washing presses are arranged in series one after the other in order to achieve the desired washing efficiency.

Tvdttanordningar sasom valspressar är emellertid dyra och utrymmeskrayande maskiner. De konsumerar ocksa mycket energi. Dessutom är det i allmanhet problematiskt att infora ytterligare maskiner i ett massabruk. 1 537 9 SAMMANFATTNING Ett syfte med uppfinningen är att tillhandahalla en forbdttrad metod for tvattning av cellulosamassa. Ett annat syfte är att tillhandahalla en effektiv metod for tvattning av cellulosamassa, vilken är forhallandevis billig och/eller kraver lite utrymme. However, television sets such as roller presses are expensive and space scraping machines. They also consume a lot of energy. In addition, it is generally problematic to introduce additional machines into a pulp mill. SUMMARY An object of the invention is to provide an improved method of washing cellulosic pulp. Another object is to provide an efficient method for washing cellulosic pulp, which is relatively inexpensive and / or requires little space.

Dessa syften uppnas i enlighet med bifogade patentkrav. These objects are achieved in accordance with the appended claims.

Foreliggande uppfinning baseras pa insikten att det är mojligt att uppna effektiv tvattning genom anvandning av en och samma tvattanordning for tva (eller fler) ickesimultana tvatmoment. Tvdttmomenten skiljs at tidsmassigt genom en mellanliggande massalagring, sa att massa tvdttas satsvis i tvattanordningen och lagras i den mellanliggande massalagringen mellan tvattmomenten. The present invention is based on the insight that it is possible to achieve efficient washing by using one and the same washing device for two (or more) non-simultaneous washing steps. The washing moments are separated in time by an intermediate mass storage, so that mass is washed batchwise in the washing device and stored in the intermediate mass storage between the washing moments.

Narmare bestamt tillhandahalls en metod for tvattning av cellulosamassa, ndmnda metod innefattande tvattning, i ett forsta tvattmoment, av massan under en forsta forutbestamd tidsperiod genom anvandning av en tvattanordning med en rorlig genomslapplig behandlingsyta. Filtrat fran massan passerar genom behandlingsytan medan massan 2 0transporteras tillsammans med behandlingsytan. Massan som tvattas i det forsta tvdttmomentet mottages av en mellanliggande massalagring ansluten till tvattanordningen och lagras i den mellanliggande massalagringen. Massan tvattas sedan i ett andra tvdttmoment under en andra forutbestdmd tidsperiod genom anvandning av tvdttanordningen, varvid massan mottages fran den mellanliggande massalagringen och pafOrs pa tvattanordningens behandlingsyta, sa att massan tvattas igen i samma tvattutrymme i tvdttanordningen. More specifically, there is provided a method of washing cellulosic pulp, said method comprising washing, in a first wash step, the pulp for a first predetermined period of time by using a washing device with a movable permeable treatment surface. The filtrate from the pulp passes through the treatment surface while the pulp is transported together with the treatment surface. The pulp washed in the first washing step is received by an intermediate pulp storage connected to the washing device and stored in the intermediate pulp storage. The pulp is then washed in a second washing step for a second predetermined period of time by using the washing device, the pulp being received from the intermediate pulp storage and applied to the treatment surface of the washing device, so that the pulp is washed again in the same washing space in the washing device.

Tvdttningen och lagringen upprepas foretradesvis sâ att massan tvattas satsvis genom anvandning av den mellanliggande massalagringen, varvid varje sats massa tvdttas i tva separata tvattmoment, vilka ager rum i samma tvattutrymme i samma tvattanordning men är tidsmassigt atskilda. The washing and storage are preferably repeated so that the pulp is washed batchwise using the intermediate pulp storage, each batch of pulp being washed in two separate washing steps, which take place in the same washing space in the same washing device but are separated in time.

Enligt en annan aspekt av uppfmningen tillhandahalls ett system for tvattning av cellulosamassa. 2 537 9 En allman uppfattning inom massaindustrin är att man alltid ska strava efter ett kontinuerligt massaflode och stabila forhallanden i massalinjen. Uppfinningen foreslar, i rak motsats till detta, att avbryta massaflodet och utfora tvattning i en loop pa satsvis sat. According to another aspect of the invention, there is provided a system for washing cellulosic pulp. 2 537 9 A general view in the pulp industry is that one should always strive for a continuous pulp flow and stable conditions in the pulp line. The invention proposes, in direct contrast to this, to interrupt the mass flow and carry out washing in a loop in batchwise manner.

Prestandan/resultatet blir forvanande nog tillfredstallande trots det ickekontinuerliga flodet genom tvattanordningen. Surprisingly, the performance / result is satisfactory despite the non-continuous flow through the washing device.

Tva (eller fler) konventionella tvattanordningar kan ersattas med en stone tvattanordning och en mellanliggande massalagring anordnade enligt uppfinningen. Tvattanordningarna som 1 0ersatts kan vara anordnade intill varandra i massalinjen eller komma fran olika delar av massalinjen forknippade med liknande processforhallanden. Uppfinningen innebar ocksa att krav pa okad tvatteffektivitet kan hanteras utan att en extra tvattanordning behovs. Den foreslagna losningen är forhallandevis billig och konsumerar mindre energi an konventionell tvattning med seriekopplade pressar. Den kraver dessutom mindre utrymme i massabruket. Two (or more) conventional washing devices can be replaced with a stone washing device and an intermediate pulp storage arranged according to the invention. The washing devices that have been replaced can be arranged next to each other in the pulp line or come from different parts of the pulp line associated with similar process conditions. The invention also meant that requirements for increased washing efficiency can be handled without the need for an additional washing device. The proposed solution is relatively inexpensive and consumes less energy than conventional washing with series-connected presses. It also requires less space in the pulp mill.

KORTFATTAD FIGURBESKRIVNING Uppfmningen, samt ytterligare syften och fordelar darmed, forstas bast genom hanvisning till efterfoljande beskrivning och bifogade ritningar, dar: Fig. 1 är ett schematiskt blockdiagram over ett system for tvattning av cellulosamassa enligt en exemplifierande utforingsform av uppfinningen; Fig. 2 är ett schematiskt blockdiagram over ett system fOr tvattning av cellulosamassa enligt en ann an exemplifierande utforingsform av uppfinningen; Fig. 3 är ett schematiskt blockdiagram over ett system for tvattning av cellulosamassa enligt ytterligare en annan exemplifierande utforingsform av uppfinningen; Fig. 4 är en schematisk tvarsnittsvy som illustrerar en valspress som anvands i en exemplifierande utforingsform av uppfinningen; och 3 537 9 Fig. 5 är ett flodesdiagram over en metod for tvattning av cellulosamassa enligt en exemplifierande utforingsform av uppfinningen. BRIEF DESCRIPTION OF THE DRAWINGS The invention, and further objects and advantages thereof, will be best understood by reference to the following description and accompanying drawings, in which: Fig. 1 is a schematic block diagram of a cellulosic pulp washing system according to an exemplary embodiment of the invention; Fig. 2 is a schematic block diagram of a cellulosic pulp washing system according to another exemplary embodiment of the invention; Fig. 3 is a schematic block diagram of a cellulosic pulp washing system according to still another exemplary embodiment of the invention; Fig. 4 is a schematic cross-sectional view illustrating a roller press used in an exemplary embodiment of the invention; and Fig. 5 is a flow diagram of a method for washing cellulosic pulp according to an exemplary embodiment of the invention.

DETALJERAD BESKRIVNING I ritningarna bctecknas liknande eller motsvarande dclar mcd samma hanvisningssiffror. DETAILED DESCRIPTION In the drawings, similar or corresponding parts are denoted by the same reference numerals.

Fig. 1 är ett schematiskt blockdiagram over ett system for tvattning av cellulosamassa enligt en 1 0exemplifierande utforingsform av uppfinningen. Det illustrerade systemet 100 innefattar en tvattanordning 10, en mellanliggande massalagring 20, ett forsta och ett andra processkarl 30, 40 anslutna till tvattanordningen 10, samt en forsta och en andra filtrattank 51, 52. Nar systemet är i drift, sker ett ffirsta tvattmoment I, dà massa fran det forsta processkarlet 30 tvattas i tvattanordningen 10 under transport tillsammans med en rorlig genomslapplig behandlingsyta 11 (t.ex. en roterbar yta, sasom den perforerade ytterytan hos en pressvals 15), och sedan leds till den mellanliggande massalagringen 20. I ett efterfoljande andra tvattmoment II tvattas massa frail den mellanliggande massalagringen 20 i samma tvattutrymme i samma tvattanordning 10 som i det forsta tvattmomentet I och fors sedan ut till det andra processkarlet 40. Fig. 1 is a schematic block diagram of a cellulosic pulp washing system according to an exemplary embodiment of the invention. The illustrated system 100 comprises a washing device 10, an intermediate pulp storage 20, a first and a second process vessel 30, 40 connected to the washing device 10, and a first and a second filter tank 51, 52. When the system is in operation, a first washing step takes place. , then pulp from the first process vessel 30 is washed in the washing device 10 during transport together with a movable permeable treatment surface 11 (e.g. a rotatable surface, such as the perforated outer surface of a press roll 15), and then led to the intermediate pulp storage 20. a subsequent second washing step II, mass frail is washed from the intermediate mass storage 20 in the same washing space in the same washing device 10 as in the first washing step I and is then carried out to the second process vessel 40.

Under det forsta tvattmomentet I uppsamlas filtrat som passerar genom den genomslappliga behandlingsytan 11 i den forsta filtrattanken 51. Under det andra tvattmomentet II uppsamlas filtrat som passerar genom den genomslappliga behandlingsytan 11 i den andra filtrattanken 52. I en fciredragen utforingsform aterfors filtrat fran det andra tvattmomentet II till det forsta tvattmomentet I och anvands som tvattvatska. Filtrat kan ocksâ anvandas for spadning av massan. During the first wash step I, filtrate passing through the permeable treatment surface 11 is collected in the first filtrate tank 51. During the second wash step II, filtrate passing through the permeable treatment surface 11 is collected in the second filtrate tank 52. In a preferred embodiment, filtrate is returned from the second filtrate from the second filtrate tank. II to the first washing step I and is used as washing water. The filtrate can also be used for spreading the pulp.

Nar systemet 100 är i drift finns normalt sett ett kontinuerligt massaflode in till forsta processkarlet 30 och ut fran det andra processkarlet 40 men ett ickekontinuerligt massaflode inom systemet (pilar I respektive II). Massan tvattas foretradesvis satsvis genom anvandning av den mellanliggande massalagringen 20, sa att varje sats massa tvattas i tva separata 4 537 9 tvdttmoment I, II, vilka dger rum i samma tvdttutrymme i samma tvdttanordning 10 men är tidsmassigt atskilda. When the system 100 is in operation, there is normally a continuous mass flow in to the first process vessel 30 and out of the second process vessel 40 but a non-continuous mass flow within the system (arrows I and II, respectively). The pulp is preferably washed batchwise using the intermediate pulp storage 20, so that each batch of pulp is washed in two separate washing steps I, II, which take place in the same washing space in the same washing device 10 but are separated in time.

"Tvdttutrymme" syflar hdr pa ett utrymme inuti tvdttanordningen 10 ddr massan transporteras pa behandlingsytan 11 och tvattas eller avvattnas. Behandlingsytan 11, d.v.s. den genomslappliga yta som massan pafors pa, är identisk i det forsta och andra tvatmomentet I, II. Foretradesvis anvands tvdttanordningens fulla axiella langd. I fallet med en valspress 10 (twin-roll press), anvands alltsa vasentligen hela langden hos pressvalsarna 15 i varje tvdttmoment I, II. 10 Inmatningsomfadet hos tvdttanordningen 10, ddr massan fordelas pa behandlingsytan 11, är vasentligen detsamma i tvdttmoment I och II. Pa liknande salt är utmatningsomradet hos tvdttanordningen 10, d.v.s. ddr massan avldgsnas fran behandlingsytan 11, vasentligen detsamma i tvdttmoment I och II. "Laundry space" refers to a space inside the washing device 10 where the pulp is transported on the treatment surface 11 and washed or dewatered. The treatment surface 11, i.e. the permeable surface on which the mass is applied is identical in the first and second washing steps I, II. Preferably, the full axial length of the washing device is used. In the case of a roller press 10 (twin-roll press), then essentially the entire length of the press rollers 15 is used in each torque I, II. The feed circumference of the washing device 10, where the pulp is distributed on the treatment surface 11, is essentially the same in washing steps I and II. On similar salt is the discharge area of the washing device 10, i.e. where the pulp is removed from the treatment surface 11, essentially the same in steps I and II.

Den mellanliggande massalagringen 20 är typiskt sett en tank/ett kart med en lagringsvolym Overskridande volymen massa producerad i respektive tvdttmoment I, II. Med andra ord är den mellanliggande massalagringen 20 dimensionerad for att lagra massa mellan tvdttmoment I och II. Den mellanliggande massalagringen 20 kan vara en ren massalagring/buffert eller, 2 0alternativt, dven fungera som behandlingstank/kdr1 med kemikalietillsats, temperaturstyrning, spadning, eller annan behandling av massan. Exempel inbegriper en medelkoncentrationstank (MC) en hogkoncentrationstank (HC), ett surt steg (A) och blektorn/blekreaktorer, t.ex. klordioxid (D), syrgas (0), peroxid (P), behandling med komplexbildare (Q), alkali-syrgas (E0), eller alkali-syrgas-peroxid (EOP). I tillampningar med forhallandevis korta tvdttcykler kan det dven vara mojligt aft anvanda en forstorad standpipe eller liknande. The intermediate mass storage 20 is typically a tank / cart with a storage volume exceeding the volume of mass produced in the respective two-step steps I, II. In other words, the intermediate mass storage 20 is dimensioned to store mass between torques I and II. The intermediate pulp storage 20 may be a pure pulp storage / buffer or, alternatively, may act as a treatment tank / kdr1 with chemical addition, temperature control, spading, or other treatment of the pulp. Examples include an average concentration tank (MC), a high concentration tank (HC), an acid step (A) and bleach / bleach reactors, e.g. chlorine dioxide (D), oxygen (0), peroxide (P), treatment with complexing agent (Q), alkali oxygen (E0), or alkali oxygen peroxide (EOP). In applications with relatively short wash cycles, it may also be possible to use an enlarged standpipe or the like.

Den mellanliggande massalagringen 20 är extern i forhallande till tvdttanordningen 10, d.v.s. en separat fysisk enhet. Massan ldmnar alltsa tvatanordningen 10 mellan tvatningen i tvdttmoment I resp. II. Utforanden ddr den mellanliggande massalagringen 20 irmefattar tva eller fler parallella tankar är tankbara. 537 9 Processkarlen 30, 40 är karl/tankar i massaprocessen (d.v.s. massalinjen) som matar ut eller tar emot massa som tvattas i enlighet med uppfinningen. Varje processkarl 30, 40 kan vara ett behandlingstom/en reaktor/tank eller, altemativt, en ren massalagring. Exempel innefattar en blastank (BT), en MC/HC-tank, ett A-steg, samt ett blektorn/en blekreaktor, t.ex. D, 0, P, Q, EO, EOP. The intermediate pulp storage 20 is external in relation to the washing device 10, i.e. a separate physical unit. The mass thus leaves the washing device 10 between the washing in the washing step I resp. II. The embodiments where the intermediate mass storage 20 comprises two or more parallel tanks are tankable. The process vessels 30, 40 are vessels / tanks in the pulp process (i.e. the pulp line) which discharge or receive pulp which is washed in accordance with the invention. Each process vessel 30, 40 may be a treatment plant / reactor / tank or, alternatively, a pure pulp storage. Examples include a blast tank (BT), an MC / HC tank, an A stage, and a bleach tower / bleach reactor, e.g. D, 0, P, Q, EO, EOP.

Den mellanliggande massalagringen 20 fungerar som en massabuffert som vaxlar mellan ett paTyllningslage, under det forsta tvattmomentet 1, och ett tomningslage, under det andra tvdttmomentet II. Det forsta och andra processkarlet 30, 40 är ocksa anordnade att vaxla 1 0mellan ett tomningslage och ett pafyllningslage men tomningslaget hor till det forsta tvdttmomentet I och pafyllningslaget hor till det andra tvattmomentet II. The intermediate pulp storage 20 acts as a pulp buffer which alternates between a filling layer, during the first washing step 1, and an emptying layer, during the second washing step II. The first and second process vessels 30, 40 are also arranged to alternate between an emptying layer and a filling layer, but the emptying layer belongs to the first washing step I and the filling layer belongs to the second washing step II.

Det bor noteras att "tomningslage" inte nodvandigtvis innebar att kdrlet är fullstandigt tomt efter tvdttmomentet. I synnerhet for processkarlen 30, 40 firms ofta en minimumniva. massa som kravs i kdrlet for aft hela processen ska ga jamnt. Dessutom firms eft massaflode in till det forst processkarlet 30 aven i tomningslage men det utgaende flodet är stone. Pa motsvarande satt firms ett massaflode ut fran det andra processkdrlet 40 alien i fyllningslage men det inkommande flodet är stone. 2 0I Fig. 1 indikerar ventiler att flodena i forsta och andra tvdttmomentet I, II inte är kontinuerliga. En pump 21 visas ocksa., anordnad att mata ut massa fran den mellanliggande massalagringen 20 under det andra tvdttmomentet II. Massan kan spadas med ett lampligt spadorgan sa att den kan pumpas fran den mellanliggande massalagringen 20. Systemet enligt uppfinningen kan implementeras genom anvandning av konventionell utrustning, sasom rorledningar, ventiler, pumpar, spadskruvar, etc. Detaljer, sasom var ventiler behovs, är rutinatgarder, vilka inte kraver flagon uppfinnarkompetens. It should be noted that "emptying" did not necessarily mean that the boiler is completely empty after the washing step. In particular for the process man 30, 40 firms often have a minimum level. mass as required in the vessel for aft the whole process should go smoothly. In addition, after mass flow into the first process vessel 30 is also emptied, but the outgoing flow is stone. Correspondingly, there is a mass flow out of the second process vessel 40 alien in fill layer, but the incoming flow is stone. In Fig. 1, valves indicate that the rivers in the first and second washing moments I, II are not continuous. A pump 21 is also shown, arranged to discharge pulp from the intermediate pulp storage 20 during the second washing step II. The pulp can be shoveled with a suitable shovel means so that it can be pumped from the intermediate pulp storage 20. The system according to the invention can be implemented by using conventional equipment, such as pipelines, valves, pumps, shovel screws, etc. Details such as where valves are needed are routine guards. which do not require flaw inventor competence.

Det fcirsta tvattmomentet I ager rum under en fOrsta forutbestamd tidsperiod, medan det andra tvdttmomentet II ager rum under en andra forutbestamd tidsperiod. Dessa forutbestamda tidsperioder behover inte vara fasta tidsintervall, utan kan ocksà till exempel bestdmmas som tiden det tar for en viss volym massa aft passera genom tvattanordningen 10. Ett mojligt tillvagagangssatt är att bestamma tidsperioden baserat pa atminstone en processparameter, 6 537 9 t.ex. sà att nivan massa i en viss processtank inte hamnar utanfor ett maximum- eller minimumvarde. Eller sa kan tidsperioden bestammas baserat pa processparametrar som indikerar massakvalitet, blekningsgrad, systemprestanda, etc. Olika styrstrategier är mojliga. The first washing moment I takes place during a first predetermined time period, while the second washing moment II takes place during a second predetermined time period. These predetermined time periods need not be fixed time intervals, but can also be determined, for example, as the time it takes for a certain volume of mass to pass through the washing device 10. A possible approach is to determine the time period based on at least one process parameter, e.g. so that the level of pulp in a given process tank does not fall outside a maximum or minimum value. Or the time period can be determined based on process parameters that indicate pulp quality, degree of bleaching, system performance, etc. Different control strategies are possible.

Processforhallandena, sasom pH och temperatur, bar foretradesvis vara ungefar samma eller liknande i den forsta och det andra tvattmomentet. I fall da den mellanliggande massalagringen 20 inbegriper behandling av massan, och inte enbart lagring, ska behandlingen saledes foretradesvis vara av liknande slag som behandlingen av massan i processkarlet 30 innan forsta tvattmomentet I. I synnerhet är det fordelaktigt att dela en tvattanordning mellan processteg 1 0med liknande halt korrosiva amnen, sasom klorider. En hog halt klorider innebar att de delar hos tvattanordningen som kommer i kontakt med massan maste tillverkas av ett bestandigt, dyrt material. The process conditions, such as pH and temperature, should preferably be approximately the same or similar in the first and second washing steps. In cases where the intermediate pulp storage 20 involves treatment of the pulp, and not only storage, the treatment should thus preferably be of a similar nature to the treatment of the pulp in the process vessel 30 before the first washing step I. In particular, it is advantageous to divide a washing device between process steps similar content of corrosive substances, such as chlorides. A high content of chlorides meant that the parts of the washing device which come into contact with the pulp must be made of a durable, expensive material.

Exempel pa kombinationer av mellanliggande massalagringar 20 och forsta och andra processkarl 30, 40 i enlighet med uppfinningen tillhandahalls i Tabell 1. (D1 och D2 är klordioxidsteg, P1 och P2 peroxidsteg, osv.) Beroende pa tillampning kan tankar/karl i en konventionell massalinje antingen anvandas i alla tre positionema, eller sâ behover atminstone en ny tank/nytt karl introduceras. HC-tankar kan, beroende pa tillampning, anvandas i stallet for MC-tankar. Examples of combinations of intermediate pulp storages 20 and first and second process vessels 30, 40 in accordance with the invention are provided in Table 1. (D1 and D2 are chlorine dioxide stages, P1 and P2 peroxide stages, etc.) Depending on the application, tanks / vessels in a conventional pulp line may either used in all three positions, or at least one new tank / new man needs to be introduced. HC tanks can, depending on the application, be used instead of motorcycle tanks.

I Exempel 2 är det forsta processkarlet 30, den mellanliggande massalagringen 20 och det andra processkarlet 40 rena lagringstankar. I de andra exemplen tillsatts syra eller blekkemikalier till atminstone ett av det forsta processkarlet 30, den mellanliggande massalagringen 20 och det andra processkarlet 40. In Example 2, the first process vessel 30, the intermediate pulp storage 20 and the second process vessel 40 are pure storage tanks. In the other examples, acid or bleaching chemicals are added to at least one of the first process vessel 30, the intermediate pulp storage 20 and the second process vessel 40.

Tabell 1. Table 1.

Exempel # la processkarl Mellanliggande massalagring 2 processkarl 1 BT MC A 2 BT MC MC 3 D1 D2 MC 4 MC MC 02 P1 P2 MC 7 537 9 6POMC I princip kan tva konventionella tvattningsmaskiner, var och en med pro duktionsvolym V, ersattas av en stor tvdttningsmaskin med produktionsvolym V+V, som kors enligt uppfinningen. Uppfirmingen krdver rorledningar, ventiler etc. och i vissa fall en extra tank/ett extra kart med tillhOrande pump. Icke desto mindre medfor det ffireslagna systemet minskade kostnader, eftersom en storre tvdttningsmaskin är mycket billigare per producerad massavolym an tvd mindre tvdttningsmaskiner. En annan viktig fordel är att mindre energi konsumeras av systemet enligt uppfinningen an av konventionella system for tvdttning. Example # la process vessel Intermediate mass storage 2 process vessel 1 BT MC A 2 BT MC MC 3 D1 D2 MC 4 MC MC 02 P1 P2 MC 7 537 9 6POMC In principle, two conventional washing machines, each with production volume V, can be replaced by a large washing machine with production volume V + V, which crosses according to the invention. The invention requires pipelines, valves, etc. and in some cases an extra tank / an extra card with an associated pump. Nevertheless, the proposed system reduces costs, since a larger washing machine is much cheaper per mass of mass produced than two smaller washing machines. Another important advantage is that less energy is consumed by the system according to the invention than by conventional washing systems.

Typiskt sett kors var och en av den forsta och det andra tvdttmomentet I, II under en tidsperiod pa 0,03 till 2 timmar. I allmanhet är en kort tvdttcykel att foredra, dA volymen massa i bufferten(buffertarna) annars kan bli svarhanterlig. Det är ocksa bra for filtrathanteringen med en kort tvdttcykel. En tidsperiod pa omkring 3-5 min per tvdttmoment kan till exempel anvandas. Vid tillampningar som anvander blekreaktorer som massabuffertar, skulle en langre tidsperiod vara mojlig pA grund av storre tankstorlek. Tvdttcykeln kan emellertid inte vara for lang, emedan massans uppehallstid dd. kommer att variera fOr mycket Mom reaktorn. En tidsperiod pA omkring 10-30 min per tvdttmoment kan till exempel anvdndas. Sdledes ligger en foredragen tidsperiod for varje tvdttmoment Mom omradet ca 3 till 30 min. Typically, each of the first and second washing steps I, II crosses over a period of 0.03 to 2 hours. In general, a short wash cycle is preferable, as the volume of pulp in the buffer (s) can otherwise be responsive. It is also good for filtrate handling with a short wash cycle. For example, a time period of about 3-5 minutes per torque can be used. For applications that use bleach reactors as pulp buffers, a longer period of time would be possible due to the larger tank size. However, the television cycle can not be too long, since the residence time of the pulp dd. will vary too much Mom reactor. For example, a time period of about 10-30 minutes per torque can be used. Thus, a preferred time period for each torque Mom is in the range of about 3 to 30 minutes.

Aterigen gar uppfinningen mot radande uppfattning inom massaindustrin att stabila forhallanden i massalinjen alltid är mdlet. I linje med det traditionella synsdttet skulle tvdttcykeln vara sA lang som mojligt pa grund av systemstabiliteten men hdr foreslas i stdllet en kort tidsperiod. Again, the invention goes against the prevailing view in the pulp industry that stable conditions in the pulp line are always the means. In line with the traditional visual acuity, the wash cycle should be as long as possible due to system stability, but this is proposed instead for a short period of time.

FOr att erhalla ett effektivitet system fOr tviittning kan organ tillhandahallas for att Lindra tvdttanordningens 10 instdllningar mellan tvdttmoment I och II. Sdrskilt kan mdngden tvdttvaska (visas ej i ritningarna) som tillsatts till massan pa behandlingsytan 11 anpassas till respektive tvdttmoment I, II. En annan parameter som kan justeras är rotationshastigheten hos den rorliga genomsldppliga behandlingsytan 11. En annan parameter som kan anpassas till respektive tvdttmoment I, II är mangden tillsatt spddvdtska, som spdder massan till pumpbar koncentration efter tvdttningen i tvattanordningen 10. Anpassning av dessa parametrar 8 537 9 (forandring av installningar eller intervall) kan t.ex. vara ldmplig om massakoncentrationema är olika i tvdttmoment I och II. In order to obtain an efficient system for washing, means can be provided for relieving the settings of the washing device 10 between washing steps I and II. In particular, the amount of laundry (not shown in the drawings) added to the pulp on the treatment surface 11 can be adapted to the respective washing steps I, II. Another parameter that can be adjusted is the rotational speed of the movable permeable treatment surface 11. Another parameter that can be adapted to the respective washing steps I, II is the amount of added diluent, which dilutes the mass to pumpable concentration after washing in the washing device 10. Adjustment of these parameters 8 537 9 (change of installations or intervals) can e.g. be exemplary if the pulp concentrations are different in steps I and II.

Det ska forstas att aven om tvattanordningen 10 illustreras som en valspress (twin-roll press) är detta bara ett exempel. En annan tvdttanordning, sasom en diffusor, ett filter, en trumtvdtt (t.ex. trumfOrtrangningstvatt), eller en annan typ av press (t.ex. en virapress), kan ocksa anvandas i enlighet med uppfinningen. Den rorliga genomslappliga behandlingsytan 11 kan fOljaktligen innefatta en perforerad pressvals eller trumyta, en vim, eller en silplat hos en diffusor. It is to be understood that although the washing device 10 is illustrated as a twin-roll press, this is only an example. Another washing device, such as a diffuser, a filter, a drum washing (e.g., drum displacement wash), or another type of press (e.g., a wire press), may also be used in accordance with the invention. The movable permeable treatment surface 11 may consequently comprise a perforated press roll or drum surface, a vim, or a sieve plate of a diffuser.

Fig. 2 illustrerar ett annat exemplifierande system enligt uppfinningen med tre tvattmoment I, II, III i samma tvdttanordning. Detta system 200 inbegriper en andra mellanliggande massalagring 60 forutom den mellanliggande massalagringen 20 i Fig. 1. Den andra mellanliggande massalagringen 60 är ansluten till tvattanordningen 10. Under det andra tvattmomentet II leds den tvattade massan till den andra mellanliggande massalagringen 60 och i ett tredje tvattmoment III tvattas massan en tredje gang pa behandlingsytan 11 i samma tvattutrymme i tvattanordningen 10. Fig. 2 illustrates another exemplary system according to the invention with three washing steps I, II, III in the same washing device. This system 200 includes a second intermediate pulp storage 60 in addition to the intermediate pulp storage 20 in Fig. 1. The second intermediate pulp storage 60 is connected to the washing device 10. During the second washing step II, the washed pulp is led to the second intermediate pulp storage 60 and in a third washing step III, the pulp is washed a third time on the treatment surface 11 in the same washing space in the washing device 10.

Det tredje tvdttmomentet III har en tillhorande tredje fdrutbestamd tidsperiod. Vad som sagts 2 0ovan om de forsta och andra forutbestdmda tidsperiodema kan appliceras dven pa den tredje tidsperioden. Processforhallandena, sasom pH och temperatur, ska foretradesvis vara ungefdr samma eller liknande i alla tre tvattmomenten I, II, III. The third torque III has an associated third predetermined time period. What has been said above about the first and second predetermined time periods can also be applied to the third time period. The process conditions, such as pH and temperature, should preferably be approximately the same or similar in all three washing steps I, II, III.

Det finns foretradesvis en filtrattank 51, 52, 53 for valje tvattmoment och filtrat kan anvandas som tvattvdtska i ett foregdende tvdttmoment. There is preferably a filtrate tank 51, 52, 53 for selecting the torque and the filtrate can be used as a washing liquid in a previous washing torque.

Tvattprinciperna enligt Fig. 2 kan anyandas for att ersatta tre konventionella tvdttanordningar med en enda, stOrre tvdttanordning. I princip kan tre tvdttningmaskiner var och en med produktionsvolym V ersattas av en enda tvattningsmaskin med produktionsvolym V+V+V, vilket innebar att totala nyttan blir annu stOrre an i fallet med endast tva tvattmoment I, II. 9 537 9 Fig. 3 illustrerar ett annat exemplifierande system 300 enligt uppfinningen med tva tvattmoment I, II i samma tvattanordning 10. Tvattanordningen 10 är ansluten till den mellanliggande massalagringen 20 via ytterligare processutrustning 70, sa att ytterligare behandling, sasom blekning, utfors mellan den forsta tvattningen i tvattanordningen 10 och lagringen i den mellanliggande massalagringen 20. The washing principles of Fig. 2 can be used to replace three conventional washing devices with a single, larger washing device. In principle, three washing machines each with production volume V can be replaced by a single washing machine with production volume V + V + V, which meant that the total benefit will be even greater than in the case of only two washing steps I, II. Fig. 3 illustrates another exemplary system 300 according to the invention with two washing steps I, II in the same washing device 10. The washing device 10 is connected to the intermediate pulp storage 20 via further processing equipment 70, so that further treatment, such as bleaching, is carried out between the the first washing in the washing device 10 and the storage in the intermediate pulp storage 20.

Den ytterligare processutrustningen 70 kan till exempel innefatta eft blektom med en tillhorande tvatt och annan tillhorande utrustning sasom en pump, spadskruv, osv. I ett sadant fall finns ett massaflode genom tvatten hos den ytterligare processutrustningen 70 (d.v.s. tvatten anordnad efter blektomet) under bagge tvattmomenten I, II. Blektomet hos den ytterligare processutrustningen 70 fungerar som en ytterligare massabuffert, anordnad att vaxla mellan ett pafyllningslage, under det forsta tvattmomentet I, och ett tomningslage, under det andra tvattmomentet II. The additional process equipment 70 may include, for example, after the bleacher with an associated wash and other associated equipment such as a pump, paddle screw, etc. In such a case, a mass flow through the water of the additional process equipment 70 (i.e., water arranged after the bleach atom) is present under the ram washing moments I, II. The bleach atom of the further processing equipment 70 functions as an additional pulp buffer, arranged to alternate between a filling layer, during the first washing step I, and an emptying layer, during the second washing step II.

Genom anvandande av principema enligt Fig. 3, kan en tvattanordning delas mellan processteg, t.ex. bleksteg, som inte ligger direkt efter varandra i massalinjen. Processforhallandena ska foretradesvis vara ungefar samma eller liknande i det forsta och det andra tvattmomentet I, II. By applying the principles according to Fig. 3, a washing device can be divided between process steps, e.g. pale steps, which do not lie directly one after the other in the mass line. The process conditions should preferably be approximately the same or similar in the first and second washing steps I, II.

Exempel pa kombinationer av mellanliggande massalagringar 20 och fcirsta och andra 2 0processkarl 30, 40 i utforingsformer med ytterligare processutrustning 70 tillhandahalls i Tabell 2. Examples of combinations of intermediate pulp storages 20 and first and second process vessels 30, 40 in embodiments with additional process equipment 70 are provided in Table 2.

Tabell 2. Table 2.

Exempel # la processkarl Ytterligare behandling Mellanliggande massalagring 2 processkarl 7 DO EOP D1 D2 8 MC DO EO D1 Exempel 7 avser en massalinje som innefattar bleksekvensen DO EOP D1 D2 (i allmanhet med tvatt efter varje blektom). Stegen DO och D1 delar samma tvattanordning, som kors enligt uppfinningens principer. Med andra ord utfors tvattning i en och samma tvattanordning 10 mellan DO- och EOP-tomen och mellan D1- och D2-tornen. Att dela tvattanordning mellan tva. 10 537 9 D-steg, som i Exempel 7, har fordelen är processforhallandena hos de tva tvattmomenten I, II i tvattanordning är mycket lika (samma pH, osv.). Example # la process vessel Additional treatment Intermediate pulp storage 2 process vessel 7 DO EOP D1 D2 8 MC DO EO D1 Example 7 relates to a pulp line comprising the bleaching sequence DO EOP D1 D2 (generally with wash after each bleach atom). Steps D0 and D1 share the same washing device, which crosses according to the principles of the invention. In other words, washing is performed in one and the same washing device 10 between the DO and EOP atoms and between the D1 and D2 towers. Sharing washing device between two. D-step, as in Example 7, has the advantage that the process conditions of the two washing steps I, II in the washing device are very similar (same pH, etc.).

Exempel 8 avser en massalinje som innefattar bleksekvensen MC DO EO D1 (i allmanhet med tvatt efter varje blektorn). MC-tornet kan beroende pa tillampning ersattas av ett HC-torn. Example 8 relates to a pulp line comprising the bleaching sequence MC DO EO D1 (generally with wash after each bleaching tower). Depending on the application, the motorcycle tower can be replaced by an HC tower.

MC/HC-tornet och EO delar samma tvattanordning, som kOrs enligt uppfinningens principer. I detta exempel, liksom i Exempel 7, kan befintliga karl/tankar i blekstegen anvandas och det finns inget behov av att introducera flagon ny tank/karl som massabuffert. 1 0Vidare kan principerna enligt Fig. 2 och 3 kombineras till ett system med tre tvattmoment I, II, III, ddr forsta och andra tvattmomentet I, II och/eller andra och tredje tvattmomentet II, III inte behover utforas direkt efter varandra. I princip kan tre tvattningmaskiner fran olika delar av massalinjen och var och en med tillhorande produktionsvolym V pa detta satt ersattas av en enda tvattningsmaskin med produktionsvolym V+V+V. The MC / HC tower and the EO share the same washing device as the cross according to the principles of the invention. In this example, as in Example 7, existing tanks / tanks in the bleaching stages can be used and there is no need to introduce a new tank / tank as a pulp buffer. Furthermore, the principles according to Figs. 2 and 3 can be combined into a system with three washing steps I, II, III, ddr first and second washing steps I, II and / or the second and third washing steps II, III do not need to be performed directly one after the other. In principle, three washing machines from different parts of the pulp line and each with an associated production volume V can thus be replaced by a single washing machine with a production volume V + V + V.

For enkelhets skull visas inga ventiler, pumpar, spadorgan, etc. i Fig. 2 och 3. En fackman pa omradet forstar att uppfinningen kan implementeras genom anvandning av konventionell utrustning anordnad enligt beskrivna principer. 2 0Fig. 4 är en schematisk tvarsnittsvy over en exemplifierande tvattanordning, en valspress (twin-roll press) 10, i ett foredraget system enligt uppfinningen. Valspressen 10 innefattar tva samverkande cylindriska pressvalsarltrummor 15. De tva pressvalsarna 15 är anordnade att rotera i motsatta riktningar D1 under drift och har var och en en genomslapplig ytteryta 11, narmare bestamt cn perforcrad mctallplat. Pressvalsarna omsluts dclvis av ett trag 16 som bildas av styrytor anordnade pa avstand fran den perforerade ytterytan 11 hos respektive pressvals 15 sa att pressvalsen delvis omsluts i omkretsriktningen. For the sake of simplicity, no valves, pumps, spade means, etc. are shown in Figs. 2 and 3. A person skilled in the art understands that the invention can be implemented by using conventional equipment arranged according to the described principles. 2 0Fig. 4 is a schematic cross-sectional view of an exemplary washing device, a twin-roll press, 10, in a preferred system according to the invention. The roll press 10 comprises two cooperating cylindrical press roll rollers 15. The two press rolls 15 are arranged to rotate in opposite directions D1 during operation and each has a transparent outer surface 11, more specifically a perforated metal plate. The press rollers are therefore enclosed by a funnel 16 formed by guide surfaces arranged at a distance from the perforated outer surface 11 of the respective press roll 15 so that the press roll is partially enclosed in the circumferential direction.

Till varje pressvals 15 hor en massafordelningsanordning 12. Massafordelningsanordningen 12 är anordnad vid pressvalsens 15 ovre del for fordelning av massa pa den perforerade valsytan 11. Den innefattar ett avlangt holje 18, som &tracker sig langs en vasentlig del av pressvalsen 15 i langdriktningen och är ansluten till traget 16. Vid drift kommer massan in i 11 537 9 massafordelningsanordningen 12 via dess inlopp, vilket till exempel kan vara anordnat pa mitten av valspressen 10 sett i langsgaende riktning. To each press roll 15 belongs a mass distribution device 12. The mass distribution device 12 is arranged at the upper part of the press roll 15 for distributing mass on the perforated roll surface 11. It comprises an elongate housing 18 which extends along a substantial part of the press roll 15 in the longitudinal direction and is connected to the hopper 16. During operation, the pulp enters the pulp distribution device 12 via its inlet, which may, for example, be arranged in the middle of the roller press 10 seen in the longitudinal direction.

I massafordelningsanordningen 12 fOrdelas massan i langsgaende riktning och fors ut genom utloppet 13 sa aft en massabana bildas pa den perforerade valsytan 11. Massabanan transporteras, styrd av traget 16, i rotationsriktningen D1 och pressas i ett nyp 17 dar avstandet mellan pressvalsama 15 är som minst. Pressvalsarna 15 kan innefatta axiella filtratkanaler (visas ej) vilka tar emot filtratet som passerar genom den perforerade valsytan 11 och transporterar det mot pressvalsamas 15 andar, dar det tas ut. Tvattvatska kan t.ex. tillforas till massabanan i traget 16. 10Massan fors ut med hjalp av en utmatarskruv 19. In the pulp distribution device 12, the pulp is distributed in the longitudinal direction and carried out through the outlet 13 so that a pulp web is formed on the perforated roll surface 11. The pulp web is transported, guided by the trough 16, in the direction of rotation D1 and pressed in a nip 17. . The press rolls 15 may comprise axial filtrate channels (not shown) which receive the filtrate which passes through the perforated roll surface 11 and transports it towards the spirits of the press rolls 15, where it is taken out. Tvattvatska can e.g. is fed to the pulp web in the hopper 16. 10The pulp is lifted out with the aid of a discharge screw 19.

I Fig. 4 är tva pressvalsar 15 anordnade intill varandra med rotationscentra i samma horisontella plan. Uppfinningen lampar sig aven for tvatt- och/eller avvattningsanordningar dar valsama till exempel är annorlunda anordnade eller bara en perforerad vals anvands, liksom for andra anordningar dar massan avvattnas pa en rorlig genomslapplig yta. In Fig. 4, two press rollers 15 are arranged next to each other with centers of rotation in the same horizontal plane. The invention also applies to washing and / or dewatering devices where the rollers are arranged differently, for example, or only a perforated roller is used, as well as to other devices where the mass is dewatered on a movable permeable surface.

Ett annat exemplifierande system enligt uppfinningen innefattar en valspress 10 med ett ickekonvergerande trag 16, d.v.s. ett trag som är parallellt eller divergerar frail positionen dar massan paTcirs pa pressvalsen 15 till pressnypet 17. Det ickekonvergerande traget 16 Or 2 0systemet enligt uppfinningen mindre kansligt for variationer i processforhallandena, sasom varierande massakoncentration och flode. Another exemplary system according to the invention comprises a roller press 10 with a non-converging trough 16, i.e. a trough which is parallel or diverges from the free position where the mass is applied on the press roll 15 to the press nip 17. The non-converging trough 16 system according to the invention is less susceptible to variations in the process conditions, such as varying mass concentration and flow.

Ett annat fordelaktigt system enligt uppfinningen innefattar en valspress 10 med organ for justering av avstandet mellan pressvalsarna 15 som svar pa varierande driftsforhallanden hos de respektive tvattmomenten I, II, III. Det kan till exempel vara sâ att nypet andras (d.v.s. andras mellan ett forsta och andra intervall) om massakoncentrationen är olika i tvattmoment I och II. Pressnypet 17 varieras foretradesvis automatiskt under drift, mellan tvattmomenten I, II, III och fOretradesvis aven under varje tvattmoment. Med hjalp av nypstyrning blir tvattningen i valspressen 10 mer effektiv och pressen 10 blir mindre kanslig for varierande last. Another advantageous system according to the invention comprises a roller press 10 with means for adjusting the distance between the press rollers 15 in response to varying operating conditions of the respective washing steps I, II, III. For example, it may be that the nip is different (i.e. different between a first and second interval) if the pulp concentration is different in washing steps I and II. The press nip 17 is preferably varied automatically during operation, between the washing steps I, II, III and preferably also during each washing step. With the aid of nip control, the washing in the roller press 10 becomes more efficient and the press 10 becomes less susceptible to varying loads.

Ytterligare ett annat fordelaktigt system enligt uppfinningen inbegriper en valspress 10, vars pressvalsar 15 har en diameter i omradet 0,8-3m, foretradesvis 1,5-3m och en langd i omradet 12 537 9 1,2-11m, foretradesvis 4-11m. Genom anvandning av en stor valspress kan produktionsvolymen bibehallas fastan pressen anordnas att hantera tva olika tvattmoment. Tva konventionella pressar 10, vardera med produktionsvolym V, kan ersattas av en stor press med pro duktionsvolym V+V som kors enligt uppfinningen. Yet another advantageous system according to the invention comprises a roller press 10, whose press rollers 15 have a diameter in the range 0.8-3m, preferably 1.5-3m and a length in the range 12 537 9 1.2-11m, preferably 4-11m . By using a large roller press, the production volume can be maintained even though the press is arranged to handle two different washing steps. Two conventional presses 10, each with production volume V, can be replaced by a large press with production volume V + V which crosses according to the invention.

Ytterligare ett annat fordelaktigt system enligt uppfinningen innefattar en tvattanordning med en oppen massafordelningsanordning, sasom massafordelningsanordningen 12 illustrerad i Fig. 4. Massafordelningsanordningen 12 innefattar ett roterbart fordelningsorgan 14 anordnat att fordela massa pa den rorliga genomslappliga behandlingsytan 11 och ett utlopp 13 som oppnar sig mot massabanan, vilken under drift bildas pa den genomslappliga behandlingsytan 11. Yet another advantageous system according to the invention comprises a washing device with an open pulp distribution device, such as the pulp distribution device 12 illustrated in Fig. 4. The pulp distribution device 12 comprises a rotatable distribution means 14 arranged to distribute pulp on the movable transparent treatment surface 11 and an outlet 13 , which during operation is formed on the permeable treatment surface 11.

Utloppet har en langd som motsvarar massabanans bredd och det roterbara fordelningsorganet 14 är anordnat att fordela massa langs vasentligen hela utloppets 13 langd. Det finns inga flodeshindrande delar mellan det roterbara fordelningsorganet 14 och den genomslappliga behandlingsytan 11 i Fig. 4. The outlet has a length corresponding to the width of the pulp web and the rotatable distributing means 14 is arranged to distribute pulp along substantially the entire length of the outlet 13. There are no flow preventing parts between the rotatable distributor 14 and the permeable treatment surface 11 in Fig. 4.

Utloppet 13 hos en oppen massafordelningsanordning 12 är oppet i den bemarkelsen att ingen vagg eller annan flodeshindrande del av betydelse finns anordnad i utloppsoppningen. Det oppna utloppet 13 skapar ett fritt massaflode frail massafordelningsanordningen 12 mot den genomslappliga behandlingsytan 11. The outlet 13 of an open mass distribution device 12 is open in the sense that no cradle or other significant obstacle is provided in the outlet opening. The open outlet 13 creates a free mass flow from the mass distribution device 12 towards the permeable treatment surface 11.

Den oppna massafordelningsanordningen 12 kan med fordel vara av den typ som beskrivs i det svenska patentet SE 532 366, i synnerhet med avseende pa positionen hos det roterbara fordelningsorganet 14. En sadan anordning tillhandahaller bade fordelning och formering av massan pa pressvalsen 15. The open mass distribution device 12 can advantageously be of the type described in the Swedish patent SE 532 366, in particular with respect to the position of the rotatable distribution means 14. Such a device provides both distribution and formation of the mass on the press roll 15.

Den oppna designen hos massafordelningsanordningen 12 medfor att systemet enligt uppfinningen kan hantera varierande processforhallanden, sasom variationer i massakoncentration och flode. The open design of the pulp distribution device 12 means that the system according to the invention can handle varying process conditions, such as variations in pulp concentration and flow.

En Open massafordelningsanordning 12 kan anvandas i en dubbelvalspress 10 men den kan aven anvandas for aft pafora massa till den rorliga genomslappliga behandlingsytan 11 hos en annan tvattanordning 10 som kors enligt uppfmningen. 13 537 9 Fig. 5 är ett flodesdiagram over en metod for tvdttning av cellulosamassa enligt en exemplifierande utforingsform av uppfinningen. I steg Si tvdttas massa i ett forsta tvdttmoment I genom anvandning av en tvdttanordning 10 med en rOrlig genomslapplig behandlingsyta 11. An open pulp distribution device 12 can be used in a double roll press 10, but it can also be used to apply pulp to the movable permeable treatment surface 11 of another washing device 10 which crosses according to the invention. Fig. 5 is a flow chart of a method of washing cellulosic pulp according to an exemplary embodiment of the invention. In step Si, pulp is washed in a first washing step I by using a washing device 10 with a movable permeable treatment surface 11.

Massans ingaende koncentration är foretrddesvis i omrAdet 2-13%. Darefter transporteras massan till en mellanliggande massalagring 20 (steg S2). Kemikalier kan tillsattas till massan i den mellanliggande massalagringen 20. Steg S3 fragar om tvdttmoment I är fardigt, d.v.s. om ett forutbestamt villkor som bestammer tiden for tvdttmoment I är uppfyllt. Om nej, gar processen tillbaka till steg Si. Om ja, kan installningarna hos tvattanordningen 10 eller dess 1 0tillhorande utrustning, sasom ventiler, spddorgan, osv., justeras i steg S4 (icke-obligatoriskt) sâ att de passar for nasta tvdttmoment. MAngden tvdttvdtska kan till exempel Andras. I steg S5 tvdttas lagrad massa i ett andra tvdttmoment II genom anvandning av samma tvdttanordning 10 med den rorliga genomslappliga behandlingsytan 11. Massans ingaende koncentration är foretradesvis i omradet 2-13%. Steg S6 fragar om tvdttmoment II är fardigt. Om nej, gar processen tillbaka till steg S5. Om ja, kan installningama hos tvdttanordningen 10 justeras i steg S7 (icke-obligatoriskt) for att passa nasta tvdttmoment. Processen gar ddrefter tillbaka till steg Si. The initial concentration of the pulp is preferably in the range 2-13%. The pulp is then transported to an intermediate pulp storage 20 (step S2). Chemicals can be added to the pulp in the intermediate pulp storage 20. Step S3 asks if the torque I is finished, i.e. if a predetermined condition determining the time for tvdttmoment I is met. If not, the process returns to step Si. If so, the installations of the washing device 10 or its associated equipment, such as valves, spouts, etc., can be adjusted in step S4 (optional) to suit the next washing steps. The amount of tvdttvdtska can, for example, Andras. In step S5, stored pulp is washed in a second washing step II by using the same washing device 10 with the movable permeable treatment surface 11. The solids concentration of the pulp is preferably in the range 2-13%. Step S6 asks if torque II is complete. If not, the process returns to step S5. If so, the installations of the washing device 10 can be adjusted in step S7 (optional) to suit the next washing steps. The process then returns to step Si.

I enlighet med Fig. 5 upprepas foretradesvis tvdtt- och lagringsstegen Si, S2, S5 sà att massan 2 0tvdttas satsvis genom anvandning av den mellanliggande massalagringen 20, varvid varje sats massa tvdttas i tva separata tvdttmoment I, II, vilka Ager rum i samma tvdttutrymme i samma tvdttanordning 10 men är tidsmassigt atskilda. According to Fig. 5, the washing and storage steps S1, S2, S5 are preferably repeated so that the pulp is washed batchwise using the intermediate pulp storage 20, each batch of mass being washed in two separate washing steps I, II, which take place in the same washing space. in the same washing device 10 but are separated in time.

Justeringen i steg S4 kan till exempel innefatta justering av atminstone en parameter av: ett flode tillsatt tvdttvdtska, en rotationshastighet, ett flode tillsatt spadvdtska och ett avstand mellan pressvalsarna 15. The adjustment in step S4 may, for example, comprise adjusting at least one parameter of: a flood added TV, a rotational speed, a flood of sod and a distance between the press rollers 15.

Uppfinningen är inte begransad till de illustrerade utfOringsformerna, utan tacker Aven ekvivalenter till visade sardrag och kan varieras Mom patentkravens skyddsomfang. Det kan till exempel fmnas utforingsformer med mer an tre tvdttmoment i samma tvdttanordning. Det ar dven mojligt att ha ett system ddr en tvdttanordning an anordnad sâ att den kan koras bade konventionellt, med ett massaflode genom tvdttanordningen, och enligt uppfinningen, med tva 14 537 9 massafloden, tidsmassigt atskilda, genom tvattanordningen. Detta kan till exempel vara anvandbart nar en massalinje kors med tva olika massatyper med olika krav pa tvattresultat och/eller mycket olika massafloden. The invention is not limited to the illustrated embodiments, but also owes equivalents to the features shown and can be varied within the scope of the patent claims. For example, there may be embodiments with more than three washing torques in the same washing device. It is also possible to have a system in which a washing device is arranged so that it can be operated both conventionally, with a mass flow through the washing device, and according to the invention, with two mass flows, temporally separated, through the washing device. This can be useful, for example, when a mass line crosses with two different mass types with different requirements for water results and / or very different mass flows.

Claims (29)

1. A method for Washing of cellulose pulp, comprising the steps of Washing, in a first Washing operation (I), the pulp for a first predetermined period oftime using a Washing apparatus (10) With a movable penneable processing surface (11),filtrate from the pulp passing through the processing surface as the pulp is transported togetherwith the processing surface, storing the pulp in an interrnediate pulp storage (20) connected to the Washing apparatus(10) and arranged to receive the pulp washed in the first Washing operation, and Washing, in a second Washing operation (II), the pulp for a second predeterrnined periodof time using the Washing apparatus (10), the pulp being received from the intermediate pulpstorage (20) and applied onto the processing surface (11) of the Washing apparatus, such thatthe pulp is washed again in the same Washing space of the Washing apparatus, the Washing and storing steps being repeated such that the pulp is washed batch-wiseusing the intermediate pulp storage (20), each batch of pulp being washed in two separateWashing operations (I, II), which occur in the same Washing space of the same Washing apparatus (10) but are separate in time.
2. The method of claim 1, wherein the input area of the Washing apparatus ( 10), where thepulp is distributed onto the processing surface (11), is the same in the first and second Washing operation (I, II), and the output area of the Washing apparatus ( 10), Where the pulp is withdrawn from the processing surface ( 11), is the same in the first and second Washing operation (I, II).
3. The method of claim 1 or 2, comprising the further step of adding chemicals to the pulp inthe interrnediate pulp storage (20).
4. The method of any of previous claims, comprising the further steps of receiving the pulp to be washed in the first Washing operation (I) from a first processvessel (30) connected to the Washing apparatus (10), and outputting the pulp washed in the second Washing operation (II) to a second processvessel (40) connected to the Washing apparatus (10), the first process vessel (30) and thesecond process vessel (40) being arranged to altemate between an emptying mode, during the first Washing operation (I), and a filling mode, during the second Washing operation (II).
5. The method of any of previous claims, wherein the first process vessel (30), the interrnediate pulp storage (20), and the second process vessel (40) are pure storage tanks.
6. The method of any of claims 1-4, wherein at least one of the first process vessel (30), the interrnediate pulp storage (20), and the second process vessel (40) is a bleaching reactor.
7. The method of any of previous claims, comprising additional processing of the pulpbetween the Washing of the first Washing operation (I) and the storing in the interrnediate pulp storage (20).
8. The method of any of previous claims, comprising the further steps of collecting, during the first Washing operation (I), filtrate passing through the movablepermeable processing surface (11) into a first filtrate tank (51), and collecting, during the second Washing operation (II), filtrate passing through the movable permeable processing surface (11) into a second filtrate tank (52).
9. The method of claim 8, wherein the filtrate collected during the second Washing operation (II) is used as Washing liquid in the first Washing operation (I).
10. The method of any of previous claims, comprising the further steps of storing the pulp in a second interrnediate pulp storage (60) connected to the Washingapparatus (10) and arranged to receive the pulp washed in the second Washing operation (II),and Washing, in a third Washing operation (III), the pulp for a third predetermined period of time using the Washing apparatus (10), the pulp being received from the second interrnediate pulp storage (60) and applied onto the processing surface (11) of the Washing apparatus, such that the pulp is washed again in the same Washing space of the Washing apparatus.
11. The method of any of previous claims, wherein the Washing operations (I, II, III) are associated with similar process conditions.
12. The method of any of previous claims, wherein each Washing operation (I, II, III) is run during a period of time in the range of about 3 to 30 min.
13. The method of any of previous claims, comprising the further step of adjusting a pararneter of the Washing apparatus (10) or its associated equipment to therespective Washing operation (I, II, III), the parameter being selected from the group of: a flowof added Washing liquid; a rotation speed; a flow of added dilution liquid; and a distance between press rolls (15).
14. A system (100) for Washing of cellulose pulp, comprising a Washing apparatus (10) with a movable perrneable processing surface (11), arrangedfor Washing, in a first Washing operation (I), the pulp for a first predetermined period of time,filtrate from the pulp passing through the processing surface as the pulp is transpoited togetherwith the processing surface, and an interrnediate pulp storage (20), connected to the Washing apparatus (10) and arrangedto receive and store the pulp washed in the first Washing operation, and wherein the Washing apparatus (10) is further arranged for receiving the pulp from theinterrnediate pulp storage (20) and Washing, in a second Washing operation (II), for a secondpredetennined period of time, the pulp again on the processing surface (ll) in the sameWashing space of the Washing apparatus, the system further comprising means for repetition of the Washing operations ( I, II) and the storing in the interrnediatepulp storage (20), such that the system is arranged for batch-Wise operation, each batch ofpulp being washed in two separate Washing operations (I, II), which occur in the same Washing space of the Washing apparatus (10) but are separate in time.
15. The system of claim 14, wherein the input area of the washing apparatus ( 10), where thepulp is distributed onto the processing surface (11), is the same in the first and secondwashing operation (I, II), and the output area of the washing apparatus ( 10), where the pulp is Withdrawn from the processing surface ( 11), is the same in the first and second washing operation (I, II). .
16. The system of claim 14 or 15, further comprising means for adding chemicals to the pulp in the interrnediate pulp storage (20).
17. The system of any of claims 14-16, further comprising a first process vessel (30) connected to the washing apparatus (10), means for receiving, at the washing apparatus (10), the pulp to be washed in the firstwashing operation (I) from the first process vessel (3 0), a second process vessel (40) connected to the washing apparatus (10), and means for outputting, from the washing apparatus (10), the pulp washed in the secondwashing operation (II) to the second process vessel (40), the first process vessel (30) and thesecond process vessel (40) being arranged to alternate between an emptying mode, during the first washing operation (I), and a filling mode, during the second washing operation (II).
18. The system of any of claims 14-17, wherein the first process vessel (30), the intermediate pulp storage (20), and the second process vessel (40) are pure storage tanks.
19. The system of any of claims 14-17, wherein at least one of the first process vessel (30), the intermediate pulp storage (20), and the second process vessel (40) is a bleaching reactor.
20. The system of any of claims 14-19, further comprising means (70) for additionalprocessing of the pulp arranged between the first washing in the washing apparatus (10) and the interrnediate pulp storage (20).
21. The system of any of claims 14-20, further comprising a first filtrate tank (51) arranged to collect filtrate passing through the movableperrneable processing surface (11) during the first Washing operation (I), and a second filtrate tank (52), arranged to collect filtrate passing through the movable permeable processing surface (11) during the second Washing operation (II).
22. The system of claim 21, further comprising means for using the filtrate collected during the second Washing operation (II) as Washing liquid in the first Washing operation (I).
23. The system of any of claims 14-22, further comprising a second intermediate pulp storage (60) connected to the Washing apparatus (10) andarranged to receive and store the pulp washed in the second Washing operation (II), andwherein the Washing apparatus (10) is further arranged for receiving the pulp from theintermediate pulp storage (60) and Washing, in a third Washing operation (III), for a thirdpredetermined period of time, the pulp again on the processing surface (11) in the same Washing space of the Washing apparatus.
24. The system of any of claims 14-23, adapted for operating each Washing operation (I, II, III) during a period of time in the range of about 3 to 30 min.
25. The system of any of claims 14-24, further comprising adjustment means for adjusting a parameter of the Washing apparatus (10) or itsassociated equipment to the respective Washing operation (I, II, III), the parameter beingselected from the group of: a flow of added Washing liquid; a rotation speed; a flow of added dilution liquid; and a distance between press rolls (15).
26. The system of any of claims 14-25, wherein the Washing apparatus (10) comprises an openpulp distribution device (12) with a rotatable distribution means (14) and an outlet (13) which opens towards the movable permeable processing surface (11).
27. The system of any of claims 14-26, wherein the Washing apparatus (10) is a roll press withtwo co-operating press rolls (15) and the movable permeable processing surface (11) is arotatable perforated outer surface of the press roll, a pulp web in operation being formed onthe respective rolls and transported in the direction of rotation in a non-converging vat (16) partially surrounding the press rolls, until the press nip (17) between the rolls.
28. The system of claim 27, wherein the press rolls (15) have a diameter in the range of 1.5- 3m and a length in the range of 4-1 lm.
29. The system of any of claims 27 or 28, further comprisingmeans for automatically varying the distance between the press rolls (15) in response tovarying operating conditions between the first and second Washing operation (I, II), respectively.
SE1300319A 2013-05-03 2013-05-03 Method and system for washing cellulose pulp SE537925C2 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
SE1300319A SE537925C2 (en) 2013-05-03 2013-05-03 Method and system for washing cellulose pulp
PCT/SE2014/050510 WO2014178780A1 (en) 2013-05-03 2014-04-25 Method and system for washing of cellulose pulp
CN201480025159.7A CN105189859A (en) 2013-05-03 2014-04-25 Method and system for washing of cellulose pulp
EP14792129.0A EP2992136A4 (en) 2013-05-03 2014-04-25 Method and system for washing of cellulose pulp

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SE1300319A SE537925C2 (en) 2013-05-03 2013-05-03 Method and system for washing cellulose pulp

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SE537925C2 true SE537925C2 (en) 2015-11-24

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WO (1) WO2014178780A1 (en)

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Publication number Priority date Publication date Assignee Title
US3416668A (en) * 1967-08-23 1968-12-17 D & S Engineering Internat Ltd Table filter washer
US3587257A (en) * 1967-10-16 1971-06-28 Stadler Hurter International L Bleaching system including a single,triple-deck table washer
US5015333A (en) * 1983-07-20 1991-05-14 Beloit Corporation Multi-stage pulp washing within a batch digester
FI83841C (en) * 1989-04-07 1991-09-10 Salomans Oy Process for continuous exchange of the liquid in a suspension of a fibrous or fine-grained material
US5275024A (en) * 1992-05-04 1994-01-04 The Black Clawson Company Paper pulp washing
US6006554A (en) * 1998-06-03 1999-12-28 Beloit Technologies, Inc. Two stage counter current drum washer
FI122775B (en) * 2004-09-07 2012-06-29 Andritz Oy Apparatus and method for treating pulp
FI20041518A (en) * 2004-11-25 2006-05-26 Andritz Oy Method and apparatus for treating mesa
SE0602268L (en) * 2006-10-27 2008-04-15 Metso Paper Inc Washing press comprising separation of filtrate
EP2152960B1 (en) * 2007-05-25 2017-06-28 Valmet Technologies, Inc. Arrangement for washing and dewatering cellulose pulp

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EP2992136A4 (en) 2016-12-21
SE1300319A1 (en) 2014-11-04
EP2992136A1 (en) 2016-03-09
WO2014178780A1 (en) 2014-11-06
CN105189859A (en) 2015-12-23

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