RU97106736A - METHOD FOR PRODUCING 1-ETHYL-2,3-FULLERENALUMUM CYCLOPENTANES - Google Patents

METHOD FOR PRODUCING 1-ETHYL-2,3-FULLERENALUMUM CYCLOPENTANES

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Publication number
RU97106736A
RU97106736A RU97106736/04A RU97106736A RU97106736A RU 97106736 A RU97106736 A RU 97106736A RU 97106736/04 A RU97106736/04 A RU 97106736/04A RU 97106736 A RU97106736 A RU 97106736A RU 97106736 A RU97106736 A RU 97106736A
Authority
RU
Russia
Prior art keywords
ethyl
fullerenalumum
cyclopentanes
producing
alet
Prior art date
Application number
RU97106736/04A
Other languages
Russian (ru)
Other versions
RU2132332C1 (en
Inventor
У.М. Джемилев
А.Г. Ибрагимов
З.А. Юсупов
М.Ф. Ахметов
Л.М. Халилов
М.Ф. Чегодаева
Original Assignee
Институт нефтехимии и катализа с опытным заводом АН РБ
Filing date
Publication date
Application filed by Институт нефтехимии и катализа с опытным заводом АН РБ filed Critical Институт нефтехимии и катализа с опытным заводом АН РБ
Priority to RU97106736A priority Critical patent/RU2132332C1/en
Priority claimed from RU97106736A external-priority patent/RU2132332C1/en
Publication of RU97106736A publication Critical patent/RU97106736A/en
Application granted granted Critical
Publication of RU2132332C1 publication Critical patent/RU2132332C1/en

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Claims (1)

Способ получения 1-этил-2,3-фуллереналюмациклопентанов, отличающийся тем, что фуллерен (C60) взаимодействует с избытком триэтилалюминия (AlEt3) в молярном соотношении C60 : AlEt3 = 1 : (50 - 350) соответственно, в присутствии катализатора цирконацендихлорида (Cp2ZrCl2) в количестве 1 - 3 мол. % по отношению к триэтилалюминию и толуола в качестве растворителя в атмосфере аргона при нормальных условиях в течение 24 - 48 ч.The method of obtaining 1-ethyl-2,3-fullerenalumacyclopentanes, characterized in that fullerene (C 60 ) interacts with an excess of triethylaluminum (AlEt 3 ) in a molar ratio of C 60 : AlEt 3 = 1: (50 - 350), respectively, in the presence of a catalyst zirconacene dichloride (Cp 2 ZrCl 2 ) in an amount of 1 to 3 mol. % with respect to triethylaluminum and toluene as a solvent in an argon atmosphere under normal conditions for 24 to 48 hours
RU97106736A 1997-04-24 1997-04-24 Method of synthesis of 1-ethyl-2,3-fullerenealuminocyclo- -pentanes RU2132332C1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU97106736A RU2132332C1 (en) 1997-04-24 1997-04-24 Method of synthesis of 1-ethyl-2,3-fullerenealuminocyclo- -pentanes

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU97106736A RU2132332C1 (en) 1997-04-24 1997-04-24 Method of synthesis of 1-ethyl-2,3-fullerenealuminocyclo- -pentanes

Publications (2)

Publication Number Publication Date
RU97106736A true RU97106736A (en) 1999-04-27
RU2132332C1 RU2132332C1 (en) 1999-06-27

Family

ID=20192370

Family Applications (1)

Application Number Title Priority Date Filing Date
RU97106736A RU2132332C1 (en) 1997-04-24 1997-04-24 Method of synthesis of 1-ethyl-2,3-fullerenealuminocyclo- -pentanes

Country Status (1)

Country Link
RU (1) RU2132332C1 (en)

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