RU97106736A -
METHOD FOR PRODUCING 1-ETHYL-2,3-FULLERENALUMUM CYCLOPENTANES
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METHOD FOR PRODUCING 1-ETHYL-2,3-FULLERENALUMUM CYCLOPENTANES
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Publication number
RU97106736A
RU97106736ARU97106736/04ARU97106736ARU97106736ARU 97106736 ARU97106736 ARU 97106736ARU 97106736/04 ARU97106736/04 ARU 97106736/04ARU 97106736 ARU97106736 ARU 97106736ARU 97106736 ARU97106736 ARU 97106736A
Способ получения 1-этил-2,3-фуллереналюмациклопентанов, отличающийся тем, что фуллерен (C60) взаимодействует с избытком триэтилалюминия (AlEt3) в молярном соотношении C60 : AlEt3 = 1 : (50 - 350) соответственно, в присутствии катализатора цирконацендихлорида (Cp2ZrCl2) в количестве 1 - 3 мол. % по отношению к триэтилалюминию и толуола в качестве растворителя в атмосфере аргона при нормальных условиях в течение 24 - 48 ч.The method of obtaining 1-ethyl-2,3-fullerenalumacyclopentanes, characterized in that fullerene (C 60 ) interacts with an excess of triethylaluminum (AlEt 3 ) in a molar ratio of C 60 : AlEt 3 = 1: (50 - 350), respectively, in the presence of a catalyst zirconacene dichloride (Cp 2 ZrCl 2 ) in an amount of 1 to 3 mol. % with respect to triethylaluminum and toluene as a solvent in an argon atmosphere under normal conditions for 24 to 48 hours
RU97106736A1997-04-241997-04-24Method of synthesis of 1-ethyl-2,3-fullerenealuminocyclo- -pentanes
RU2132332C1
(en)
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