RU96111117A - METHOD FOR PRODUCING 4-AMINOBENZAMIDE - Google Patents

METHOD FOR PRODUCING 4-AMINOBENZAMIDE

Info

Publication number
RU96111117A
RU96111117A RU96111117/04A RU96111117A RU96111117A RU 96111117 A RU96111117 A RU 96111117A RU 96111117/04 A RU96111117/04 A RU 96111117/04A RU 96111117 A RU96111117 A RU 96111117A RU 96111117 A RU96111117 A RU 96111117A
Authority
RU
Russia
Prior art keywords
aminobenzamide
producing
nitrobenzamide
reduction
isolation
Prior art date
Application number
RU96111117/04A
Other languages
Russian (ru)
Other versions
RU2102383C1 (en
Inventor
А.А. Конарев
Л.С. Помогаева
В.Н. Ждамарова
С.Г. Потапенко
Original Assignee
Государственный научный центр Российской Федерации "НИОПИК"
Filing date
Publication date
Application filed by Государственный научный центр Российской Федерации "НИОПИК" filed Critical Государственный научный центр Российской Федерации "НИОПИК"
Priority to RU96111117A priority Critical patent/RU2102383C1/en
Priority claimed from RU96111117A external-priority patent/RU2102383C1/en
Application granted granted Critical
Publication of RU2102383C1 publication Critical patent/RU2102383C1/en
Publication of RU96111117A publication Critical patent/RU96111117A/en

Links

Claims (1)

Способ получения 4-аминобензамида восстановлением 4-нитробензамида в водной среде с последующим выделением продукта из раствора высаливанием, отличающийся тем, что восстановление 4-нитробензамида осуществляют электрохимически в присутствии гептаэтиленгликолевого эфира-2-нафтол-сульфоновой кислоты при плотности тока 5 - 10А/дм2 и температуре 50-60oC.A method of producing 4-aminobenzamide by reduction of 4-nitrobenzamide in an aqueous medium followed by isolation of the product from the solution by salting out, characterized in that the reduction of 4-nitrobenzamide is carried out electrochemically in the presence of heptaethylene glycol ether-2-naphthol sulfonic acid at a current density of 5-10A / dm 2 and a temperature of 50-60 o C.
RU96111117A 1996-06-03 1996-06-03 Method of preparing 4-aminobenzamide RU2102383C1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU96111117A RU2102383C1 (en) 1996-06-03 1996-06-03 Method of preparing 4-aminobenzamide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU96111117A RU2102383C1 (en) 1996-06-03 1996-06-03 Method of preparing 4-aminobenzamide

Publications (2)

Publication Number Publication Date
RU2102383C1 RU2102383C1 (en) 1998-01-20
RU96111117A true RU96111117A (en) 1998-06-27

Family

ID=20181406

Family Applications (1)

Application Number Title Priority Date Filing Date
RU96111117A RU2102383C1 (en) 1996-06-03 1996-06-03 Method of preparing 4-aminobenzamide

Country Status (1)

Country Link
RU (1) RU2102383C1 (en)

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