RU94037492A - Method and plant for electron beam melting of titanium sponge - Google Patents

Method and plant for electron beam melting of titanium sponge

Info

Publication number
RU94037492A
RU94037492A RU94037492/02A RU94037492A RU94037492A RU 94037492 A RU94037492 A RU 94037492A RU 94037492/02 A RU94037492/02 A RU 94037492/02A RU 94037492 A RU94037492 A RU 94037492A RU 94037492 A RU94037492 A RU 94037492A
Authority
RU
Russia
Prior art keywords
intermediate tank
metal
ingot
titanium
guns
Prior art date
Application number
RU94037492/02A
Other languages
Russian (ru)
Other versions
RU2084549C1 (en
Inventor
А.А. Тур
В.А. Чернов
Original Assignee
Акционерное общество закрытого типа "Славянская компания"
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Акционерное общество закрытого типа "Славянская компания" filed Critical Акционерное общество закрытого типа "Славянская компания"
Priority to RU9494037492A priority Critical patent/RU2084549C1/en
Priority to UA95094263A priority patent/UA27069C2/en
Publication of RU94037492A publication Critical patent/RU94037492A/en
Application granted granted Critical
Publication of RU2084549C1 publication Critical patent/RU2084549C1/en

Links

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/02Details
    • H01J37/04Arrangements of electrodes and associated parts for generating or controlling the discharge, e.g. electron-optical arrangement, ion-optical arrangement
    • H01J37/06Electron sources; Electron guns
    • H01J37/077Electron guns using discharge in gases or vapours as electron sources
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/30Electron-beam or ion-beam tubes for localised treatment of objects
    • H01J37/305Electron-beam or ion-beam tubes for localised treatment of objects for casting, melting, evaporating or etching
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1295Refining, melting, remelting, working up of titanium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B9/00General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
    • C22B9/16Remelting metals
    • C22B9/22Remelting metals with heating by wave energy or particle radiation
    • C22B9/228Remelting metals with heating by wave energy or particle radiation by particle radiation, e.g. electron beams
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2237/00Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
    • H01J2237/30Electron or ion beam tubes for processing objects
    • H01J2237/31Processing objects on a macro-scale
    • H01J2237/3123Casting
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J2237/00Discharge tubes exposing object to beam, e.g. for analysis treatment, etching, imaging
    • H01J2237/30Electron or ion beam tubes for processing objects
    • H01J2237/31Processing objects on a macro-scale
    • H01J2237/3128Melting

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Plasma & Fusion (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

FIELD: special electrometallurgy, namely production of ingots and slabs of technical titanium having merchant purity degree in electron-beam plants with intermediate tank and with use of titanium sponge as initial charge. SUBSTANCE: method comprises steps of making consumable titanium container, filling it by titanium sponge, feeding container had been filled to zone of action of electron beam, heating and fusing its end over intermediate tank, refining metal in intermediate tank upon continuous heating power, draining melt metal to crystallizer for forming ingot. Novelty is feed of consumable container with linear motion speed equal to linear speed of distribution of front of melting temperature or less than that valve in order to provide degassing and evaporation of magnesium or sodium chlorides at sustaining value of reduced melting power for metal refining in intermediate tank and for ingot forming in crystallizer over range 3-10 kWt.h/kg.square meter and 0.5-2.5 kWt.h/kg.square meter respectively. Plant for performing the method includes electron-beam guns with deflection systems as heating sources, consumable container, intermediate tank and crystallizer. Novelty is using as heating sources gas discharge electron beam guns level of working pressure into which is higher than pressure in melting chamber, particularly high-voltage glow discharge electron beam guns upon ratio of distance between deflection systems of guns and intermediate tank to its surface area no less than 3 l/m. EFFECT: increased metal yielding to ingot, enhanced efficiency of plant upon lowered specific energy consumption, high quality of metal in ingots, stable manufacturing process.

Claims (1)

Изобретение относится к специальной электрометаллургии и может найти применение при получении слитков и слябов технического титана коммерческой чистоты в электронно-лучевых установках с промежуточной емкостью и с использованием в качестве исходной шихты губчатого титана. Способ включает изготовление расходуемого титанового контейнера, заполнение его губчатым титаном, подачу заполненного расходуемого контейнера в зону действия электронных лучей, нагрев и оплавление его торца над промежуточной емкостью, рафинирование металла в промежуточной емкости при постоянной мощности нагрева, слив жидкого металла в кристаллизатор и формирование в нем слитка. Новизна способа заключается в том, что подачу расходуемого контейнера осуществляют с линейной скоростью перемещения, равной или меньшей линейной скорости распространения фронта температуры плавления, обеспечивающей дегазацию и испарение хлоридов магния или натрия, поддерживая при этом величину приведенной энергии плавки на рафинирование металла в промежуточной емкости и на формирование слитка в кристаллизаторе в пределах 3-10 и 0,5-2,5 кВт ч/кг м2 соответственно. Установка для осуществления способа содержит в качестве источников нагрева электронные пушки с отклоняющими системами, расходуемый контейнер, промежуточную емкость и кристаллизатор. Новым в установке является то, что в качестве источников нагрева установлены газоразрядные электронные пушки, уровень рабочего давления которых выше давления в камере плавки, в частности, электронные пушки высоковольтного тлеющего разряда, причем отношение расстояния между отклоняющими системами пушек и промежуточной емкостью к ее площади не менее 3 м-1. Изобретение позволяет повысить выход годного металла в слиток и производительность установки при снижении удельного расхода электроэнергии, обеспечении высокого качества металла в слитке и стабильности технологического процесса.The invention relates to special electrometallurgy and may find application in the preparation of commercial-grade ingots and slabs of commercial grade titanium in electron beam installations with an intermediate capacity and using sponge titanium as the initial charge. The method includes the manufacture of a consumable titanium container, filling it with sponge titanium, feeding the filled consumable container into the zone of electron rays, heating and melting its end above the intermediate tank, refining the metal in the intermediate tank with constant heating power, draining the liquid metal into the mold and forming it ingot. The novelty of the method lies in the fact that the supply of the consumable container is carried out with a linear velocity of movement equal to or lower than the linear velocity of propagation of the front of the melting temperature, which provides degassing and evaporation of magnesium or sodium chlorides, while maintaining the magnitude of the reduced melting energy for refining the metal in an intermediate tank and the formation of the ingot in the mold in the range of 3-10 and 0.5-2.5 kW h / kg m 2, respectively. The installation for implementing the method comprises, as heat sources, electron guns with deflecting systems, a consumable container, an intermediate tank and a mold. New in the installation is that gas-discharge electron guns are installed as heating sources, the level of the working pressure of which is higher than the pressure in the melting chamber, in particular, electron guns of a high-voltage glow discharge, and the ratio of the distance between the deflecting systems of the guns and the intermediate capacity to its area is not less than 3 m -1 . The invention improves the yield of metal in the ingot and the performance of the installation while reducing the specific energy consumption, ensuring high quality metal in the ingot and the stability of the process.
RU9494037492A 1994-09-28 1994-09-28 Method of electron-beam remelting of titanium sponge and installation for its realization RU2084549C1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
RU9494037492A RU2084549C1 (en) 1994-09-28 1994-09-28 Method of electron-beam remelting of titanium sponge and installation for its realization
UA95094263A UA27069C2 (en) 1994-09-28 1995-09-22 Method for electron-beam remelting of spongy titanium and plant for realization the same

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU9494037492A RU2084549C1 (en) 1994-09-28 1994-09-28 Method of electron-beam remelting of titanium sponge and installation for its realization

Publications (2)

Publication Number Publication Date
RU94037492A true RU94037492A (en) 1996-07-10
RU2084549C1 RU2084549C1 (en) 1997-07-20

Family

ID=20161369

Family Applications (1)

Application Number Title Priority Date Filing Date
RU9494037492A RU2084549C1 (en) 1994-09-28 1994-09-28 Method of electron-beam remelting of titanium sponge and installation for its realization

Country Status (2)

Country Link
RU (1) RU2084549C1 (en)
UA (1) UA27069C2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115855745A (en) * 2022-12-16 2023-03-28 贵州航天新力科技有限公司 Method for measuring melting speed of 7-series aluminum alloy material in melting process

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2443789C2 (en) * 2010-04-19 2012-02-27 Открытое акционерное общество "Чепецкий механический завод" Method for obtaining hafnium ingots in electron beam furnace
RU2469115C1 (en) * 2011-05-24 2012-12-10 Федеральное государственное бюджетное учреждение науки Институт физики твердого тела Российской академии наук (ИФТТ РАН) Method of electron-beam melting of product from high-melting metal or alloy, and device for its implementation
CN108883447B (en) * 2016-03-11 2020-03-24 日本制铁株式会社 Titanium material and method for producing same

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115855745A (en) * 2022-12-16 2023-03-28 贵州航天新力科技有限公司 Method for measuring melting speed of 7-series aluminum alloy material in melting process
CN115855745B (en) * 2022-12-16 2023-06-16 贵州航天新力科技有限公司 Method for measuring melting speed of 7-series aluminum alloy material in melting process

Also Published As

Publication number Publication date
RU2084549C1 (en) 1997-07-20
UA27069C2 (en) 2000-02-28

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Legal Events

Date Code Title Description
MM4A The patent is invalid due to non-payment of fees

Effective date: 20080929