RU94023597A - Method of preparing polycrystalline diamond of a specified shape - Google Patents

Method of preparing polycrystalline diamond of a specified shape

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Publication number
RU94023597A
RU94023597A RU94023597/26A RU94023597A RU94023597A RU 94023597 A RU94023597 A RU 94023597A RU 94023597/26 A RU94023597/26 A RU 94023597/26A RU 94023597 A RU94023597 A RU 94023597A RU 94023597 A RU94023597 A RU 94023597A
Authority
RU
Russia
Prior art keywords
temperature
zirconium
titanium
carbide
specified shape
Prior art date
Application number
RU94023597/26A
Other languages
Russian (ru)
Other versions
RU2060933C1 (en
Inventor
Н.С. Каличкина
В.А. Боровикова
Н.А. Бенделиани
Original Assignee
Институт высоких давлений им. Л.Ф.Верещагина РАН
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Институт высоких давлений им. Л.Ф.Верещагина РАН filed Critical Институт высоких давлений им. Л.Ф.Верещагина РАН
Priority to RU94023597A priority Critical patent/RU2060933C1/en
Application granted granted Critical
Publication of RU2060933C1 publication Critical patent/RU2060933C1/en
Publication of RU94023597A publication Critical patent/RU94023597A/en

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  • Carbon And Carbon Compounds (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

FIELD: production of artificial diamonds. SUBSTANCE: carbon- containing material of a specified shape is surrounded with a powdered catalyst containing, %: 60-70 tungsten carbide, 10-12 titanium carbide, 2.4-2.6 cobalt, 2.4-2.6 titanium boride and 15-21 zirconium, and high pressure and temperature are then applied, the velocity of the temperature rise being 1400-1600 deg/s. The material is kept at high temperature for 1-2 s, and its subsequent treatment with a mixture of nitric acid and HF is carried out at room temperature. EFFECT: new method elaborated.

Claims (1)

Изобретение относится к области производства искусственных алмазов, в частности к получению поликристаллических алмазов заданной формы. Способ заключается в том, что углеродсодержащий материал заданной формы окружают порошкообразным катализатором, содержащим карбид вольфрама, карбид титана, кобальт, борид титана и цирконий, и воздействуют высокими давлением и температурой. Новым в способе являются дополнительно взятые в качестве катализатора порошки борида титана и циркония при соотношении компонентов, мас.%: карбид вольфрама 60 - 70; карбид титана 10 - 12; кобальт 2,4-2,6; борид титана 2,4-2,6; цирконий 15 - 21. Скорость повышения температуры 1400-1600 град/с. Выдержка 1-2 с и последующая химическая обработка смесью кислот НNO3 и HF при комнатной температуре.The invention relates to the field of production of artificial diamonds, in particular to the production of polycrystalline diamonds of a given shape. The method consists in the fact that a carbon-containing material of a given shape is surrounded by a powdery catalyst containing tungsten carbide, titanium carbide, cobalt, titanium boride and zirconium, and is exposed to high pressure and temperature. New in the method are additionally taken as a catalyst, powders of titanium boride and zirconium with a ratio of components, wt.%: Tungsten carbide 60 - 70; titanium carbide 10-12; cobalt 2.4-2.6; titanium boride 2.4-2.6; zirconium 15 - 21. The rate of temperature increase is 1400-1600 degrees / s. Exposure 1-2 s and subsequent chemical treatment with a mixture of acids НNO 3 and HF at room temperature.
RU94023597A 1994-06-22 1994-06-22 Method for production of polycrystalline diamond having predetermined shape RU2060933C1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
RU94023597A RU2060933C1 (en) 1994-06-22 1994-06-22 Method for production of polycrystalline diamond having predetermined shape

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RU94023597A RU2060933C1 (en) 1994-06-22 1994-06-22 Method for production of polycrystalline diamond having predetermined shape

Publications (2)

Publication Number Publication Date
RU2060933C1 RU2060933C1 (en) 1996-05-27
RU94023597A true RU94023597A (en) 1996-07-27

Family

ID=20157538

Family Applications (1)

Application Number Title Priority Date Filing Date
RU94023597A RU2060933C1 (en) 1994-06-22 1994-06-22 Method for production of polycrystalline diamond having predetermined shape

Country Status (1)

Country Link
RU (1) RU2060933C1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2611633C2 (en) * 2015-06-29 2017-02-28 Открытое акционерное общество "Научно-исследовательский институт природных, синтетических алмазов и инструмента" - ОАО "ВНИИАЛМАЗ" Method of diamond tool making

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8505654B2 (en) 2009-10-09 2013-08-13 Element Six Limited Polycrystalline diamond
RU2735087C1 (en) * 2020-03-12 2020-10-28 Федеральное государственное бюджетное учреждение науки Институт физики высоких давлений им. Л.Ф. Верещагина Российской академии наук (ИФВД РАН) Method of producing polycrystalline diamond material with a hole
RU2740599C1 (en) * 2020-03-12 2021-01-15 Федеральное государственное бюджетное учреждение науки Институт физики высоких давлений им. Л.Ф. Верещагина Российской академии наук (ИФВД РАН) Method of producing polycrystalline diamond material

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2611633C2 (en) * 2015-06-29 2017-02-28 Открытое акционерное общество "Научно-исследовательский институт природных, синтетических алмазов и инструмента" - ОАО "ВНИИАЛМАЗ" Method of diamond tool making

Also Published As

Publication number Publication date
RU2060933C1 (en) 1996-05-27

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