RU2015116523A - METHOD FOR POST-PRODUCTION THERMAL PROCESSING OF ADDITIVELY PRODUCED PRODUCTS FROM STRENGTHENED GAMMA PRIMA PHASE OF SUPER ALLOYS - Google Patents
METHOD FOR POST-PRODUCTION THERMAL PROCESSING OF ADDITIVELY PRODUCED PRODUCTS FROM STRENGTHENED GAMMA PRIMA PHASE OF SUPER ALLOYS Download PDFInfo
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- RU2015116523A RU2015116523A RU2015116523A RU2015116523A RU2015116523A RU 2015116523 A RU2015116523 A RU 2015116523A RU 2015116523 A RU2015116523 A RU 2015116523A RU 2015116523 A RU2015116523 A RU 2015116523A RU 2015116523 A RU2015116523 A RU 2015116523A
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- Prior art keywords
- product
- temperature
- post
- heat treatment
- heating
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Links
- 238000000034 method Methods 0.000 title claims abstract 13
- 238000004519 manufacturing process Methods 0.000 title claims abstract 7
- 229910000601 superalloy Inorganic materials 0.000 title claims abstract 3
- 238000010438 heat treatment Methods 0.000 claims abstract 18
- 238000001513 hot isostatic pressing Methods 0.000 claims abstract 2
- 238000001953 recrystallisation Methods 0.000 claims abstract 2
- 235000006679 Mentha X verticillata Nutrition 0.000 abstract 1
- 235000002899 Mentha suaveolens Nutrition 0.000 abstract 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 abstract 1
Classifications
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/16—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of other metals or alloys based thereon
- C22F1/18—High-melting or refractory metals or alloys based thereon
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
- B22F10/60—Treatment of workpieces or articles after build-up
- B22F10/64—Treatment of workpieces or articles after build-up by thermal means
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/12—Both compacting and sintering
- B22F3/14—Both compacting and sintering simultaneously
- B22F3/15—Hot isostatic pressing
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/12—Both compacting and sintering
- B22F3/16—Both compacting and sintering in successive or repeated steps
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/24—After-treatment of workpieces or articles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B33—ADDITIVE MANUFACTURING TECHNOLOGY
- B33Y—ADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
- B33Y40/00—Auxiliary operations or equipment, e.g. for material handling
- B33Y40/20—Post-treatment, e.g. curing, coating or polishing
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- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D6/00—Heat treatment of ferrous alloys
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C19/00—Alloys based on nickel or cobalt
- C22C19/03—Alloys based on nickel or cobalt based on nickel
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C19/00—Alloys based on nickel or cobalt
- C22C19/07—Alloys based on nickel or cobalt based on cobalt
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/10—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of nickel or cobalt or alloys based thereon
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
- B22F10/20—Direct sintering or melting
- B22F10/28—Powder bed fusion, e.g. selective laser melting [SLM] or electron beam melting [EBM]
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F3/00—Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
- B22F3/24—After-treatment of workpieces or articles
- B22F2003/248—Thermal after-treatment
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F5/00—Manufacture of workpieces or articles from metallic powder characterised by the special shape of the product
- B22F5/009—Manufacture of workpieces or articles from metallic powder characterised by the special shape of the product of turbine components other than turbine blades
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/25—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Thermal Sciences (AREA)
- Physics & Mathematics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Powder Metallurgy (AREA)
- Turbine Rotor Nozzle Sealing (AREA)
- Health & Medical Sciences (AREA)
- Child & Adolescent Psychology (AREA)
- Heat Treatment Of Articles (AREA)
- Laser Beam Processing (AREA)
- Forging (AREA)
Abstract
1. Способ послепроизводственной термической обработки аддитивно изготовленного изделия из упрочненного гамма-прим-фазой (γ′) суперсплава на основе Ni или Со или Fe или их сочетания, состоящий из следующих стадий:a) обеспечение аддитивно изготовленного изделия в послепроизводственном состоянии, затемb) нагревание изделия от комнатной температуры (RT) до температуры T, причем Tявляется на 50-100°С меньшей, чем температура T, при которой начинается падение коэффициента теплового расширения, затемc) выдерживание изделия в течение времени t1 при Tдля достижения равномерной температуры изделия, затемd) нагревание изделия путем применения быстрого нагрева со скоростью нагрева vпо меньшей мере 25°С/мин от Тдо температуры Т≥850°С, чтобы исключить или по меньшей мере уменьшить выделение гамма-прим-фазы, затемe) применение к изделию дополнительных стадий с длительностью/температурой в зависимости от цели термической обработки.2. Способ по п. 1, отличающийся тем, что на стадии (d) скорость нагрева v=25-60°C/мин.3. Способ по п. 1, отличающийся тем, что на стадии (е) осуществляют изотермическую выдержку tв течение 2 часов для уменьшения остаточных напряжений.4. Способ по п. 1, отличающийся тем, что на стадии (е) применяют иные или дополнительные времена выдержки при температурах Т>Тдля дальнейшего уменьшения остаточных напряжений и/или перекристаллизации микроструктуры.5. Способ по п. 1, отличающийся тем, что термическую обработку осуществляют под давлением в течение горячего изостатического прессования (ГИП).6. Способ по любому из пп. 1-5, отличающийся следующими параметрами послепроизводственной термической обработки аддитивно изготовленного изделия, выполненного из IN 738LC:T=400°Cv=5°C/минv=35°C/минT=1050°Ct=2 чT=1120°C/2 ч или 1200°C/4 ч или 1250°C/3 1. A method of post-production heat treatment of an additively manufactured product from a gamma-prim-phase (γ ′) hardened superalloy based on Ni or Co or Fe or a combination thereof, consisting of the following stages: a) providing the additively manufactured product in the post-production state, then b) heating products from room temperature (RT) to temperature T, and T is 50-100 ° C lower than temperature T at which the thermal expansion coefficient begins to fall, then c) keeping the product for a time t1 at T for d achieving a uniform temperature of the product, then d) heating the product by applying rapid heating with a heating rate v of at least 25 ° C / min from Tdo temperature T≥850 ° C to eliminate or at least reduce the emission of gamma-prim phase, then e) application to the product of additional stages with a duration / temperature depending on the purpose of the heat treatment. 2. The method according to claim 1, characterized in that in step (d) the heating rate is v = 25-60 ° C / min. 3. The method according to claim 1, characterized in that at the stage (e) isothermal exposure t for 2 hours is carried out to reduce residual stresses. A method according to claim 1, characterized in that at the stage (e), other or additional holding times are used at temperatures T> T to further reduce the residual stresses and / or recrystallization of the microstructure. The method according to claim 1, characterized in that the heat treatment is carried out under pressure during hot isostatic pressing (GUI) .6. The method according to any one of paragraphs. 1-5, characterized by the following parameters of post-production heat treatment of an additively manufactured product made of IN 738LC: T = 400 ° Cv = 5 ° C / minv = 35 ° C / minT = 1050 ° Ct = 2 hT = 1120 ° C / 2 h or 1200 ° C / 4 h or 1250 ° C / 3
Claims (6)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP14167904.3 | 2014-05-12 | ||
EP14167904.3A EP2944402B1 (en) | 2014-05-12 | 2014-05-12 | Method for post-built heat treatment of additively manufactured components made of gamma-prime strengthened superalloys |
Publications (3)
Publication Number | Publication Date |
---|---|
RU2015116523A true RU2015116523A (en) | 2016-11-20 |
RU2015116523A3 RU2015116523A3 (en) | 2018-11-12 |
RU2684989C2 RU2684989C2 (en) | 2019-04-16 |
Family
ID=50693512
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
RU2015116523A RU2684989C2 (en) | 2014-05-12 | 2015-04-29 | Method of following production thermal treatment of additively made articles from super-hardened gamma-type super fell charts |
Country Status (7)
Country | Link |
---|---|
US (1) | US9670572B2 (en) |
EP (1) | EP2944402B1 (en) |
JP (1) | JP2015227505A (en) |
KR (1) | KR20150129616A (en) |
CN (1) | CN105088119B (en) |
CA (1) | CA2890977A1 (en) |
RU (1) | RU2684989C2 (en) |
Families Citing this family (28)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2944402B1 (en) | 2014-05-12 | 2019-04-03 | Ansaldo Energia IP UK Limited | Method for post-built heat treatment of additively manufactured components made of gamma-prime strengthened superalloys |
US10378087B2 (en) | 2015-12-09 | 2019-08-13 | General Electric Company | Nickel base super alloys and methods of making the same |
DE102016203901A1 (en) | 2016-03-10 | 2017-09-14 | MTU Aero Engines AG | Method and device for producing at least one component region of a component |
JP6826821B2 (en) * | 2016-05-12 | 2021-02-10 | 三菱重工業株式会社 | Manufacturing method of metal parts |
CN110520273A (en) * | 2017-02-02 | 2019-11-29 | 英默里斯滑石美国有限公司 | Improve the adherency of the road plastic part Zhong Kua and coalescence manufactured in 3D printing |
WO2018216067A1 (en) * | 2017-05-22 | 2018-11-29 | 川崎重工業株式会社 | High temperature component and method for producing same |
EP3406371A1 (en) * | 2017-05-22 | 2018-11-28 | Siemens Aktiengesellschaft | Method of relieving mechanical stress in additive manufacturing |
CN108914029A (en) * | 2017-06-13 | 2018-11-30 | 刘红宾 | A method of preventing different metal materials zigzag Interface Cracking |
GB201709540D0 (en) * | 2017-06-15 | 2017-08-02 | Rolls Royce Plc | Processing method |
GB2565063B (en) | 2017-07-28 | 2020-05-27 | Oxmet Tech Limited | A nickel-based alloy |
US10889872B2 (en) | 2017-08-02 | 2021-01-12 | Kennametal Inc. | Tool steel articles from additive manufacturing |
WO2019099000A1 (en) * | 2017-11-15 | 2019-05-23 | Siemens Energy, Inc. | Method of repairing gamma prime strengthened superalloys |
US11097348B2 (en) | 2017-12-08 | 2021-08-24 | General Electric Company | Structures and components having composite unit cell matrix construction |
EP3521804A1 (en) * | 2018-02-02 | 2019-08-07 | CL Schutzrechtsverwaltungs GmbH | Device for determining at least one component parameter of a plurality of, particularly additively manufactured, components |
GB201808824D0 (en) * | 2018-05-30 | 2018-07-11 | Rolls Royce Plc | Crack reduction for additive layer manufacturing |
DE102018210397A1 (en) * | 2018-06-26 | 2020-01-02 | Siemens Aktiengesellschaft | Method for additive manufacturing of a structure with coolant guidance, component and device |
CN108994304B (en) * | 2018-07-27 | 2019-07-26 | 中南大学 | A method of it eliminating metal material increasing material manufacturing crackle and improves mechanical property |
US10577679B1 (en) | 2018-12-04 | 2020-03-03 | General Electric Company | Gamma prime strengthened nickel superalloy for additive manufacturing |
US11077512B2 (en) * | 2019-02-07 | 2021-08-03 | General Electric Company | Manufactured article and method |
US11807929B2 (en) | 2019-03-14 | 2023-11-07 | Unison Industries, Llc | Thermally stabilized nickel-cobalt materials and methods of thermally stabilizing the same |
US11235405B2 (en) | 2019-05-02 | 2022-02-01 | General Electric Company | Method of repairing superalloy components using phase agglomeration |
GB2584654B (en) | 2019-06-07 | 2022-10-12 | Alloyed Ltd | A nickel-based alloy |
GB2587635B (en) * | 2019-10-02 | 2022-11-02 | Alloyed Ltd | A Nickel-based alloy |
CN110964992B (en) * | 2019-11-28 | 2021-06-01 | 西安航天发动机有限公司 | Heat treatment method for additive manufacturing high-temperature alloy working in low-temperature environment |
CN111390180A (en) * | 2020-04-27 | 2020-07-10 | 南京国重新金属材料研究院有限公司 | Method for improving endurance quality of GH3536 alloy manufactured by selective laser melting technology |
CN112828310B (en) * | 2020-12-31 | 2023-01-24 | 湖北三江航天红阳机电有限公司 | Method for improving toughness of 3D printing nickel-based high-temperature alloy part |
CN113584294B (en) * | 2021-06-25 | 2023-03-14 | 西安热工研究院有限公司 | Post-weld stress relief treatment method for precipitation-strengthened high-temperature alloy |
CN114109044B (en) * | 2021-11-25 | 2022-08-23 | 浙江大学 | 3D weaves and prints integration structure construction equipment |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100377830C (en) * | 2002-08-28 | 2008-04-02 | P.O.M.集团公司 | Part-geometry independant real time closed loop weld pool temperature control system for multi-layer DMD process |
US7854064B2 (en) | 2006-06-05 | 2010-12-21 | United Technologies Corporation | Enhanced weldability for high strength cast and wrought nickel superalloys |
US8313593B2 (en) * | 2009-09-15 | 2012-11-20 | General Electric Company | Method of heat treating a Ni-based superalloy article and article made thereby |
US9175373B2 (en) * | 2011-02-15 | 2015-11-03 | Siemens Energy, Inc. | Inertia friction weld of superalloy with enhanced post weld heat treatment |
CH705750A1 (en) | 2011-10-31 | 2013-05-15 | Alstom Technology Ltd | A process for the production of components or portions, which consist of a high-temperature superalloy. |
CH705662A1 (en) * | 2011-11-04 | 2013-05-15 | Alstom Technology Ltd | Process for producing articles of a solidified by gamma-prime nickel-base superalloy excretion by selective laser melting (SLM). |
EP2944402B1 (en) | 2014-05-12 | 2019-04-03 | Ansaldo Energia IP UK Limited | Method for post-built heat treatment of additively manufactured components made of gamma-prime strengthened superalloys |
-
2014
- 2014-05-12 EP EP14167904.3A patent/EP2944402B1/en active Active
-
2015
- 2015-04-29 RU RU2015116523A patent/RU2684989C2/en active
- 2015-05-06 US US14/705,264 patent/US9670572B2/en active Active
- 2015-05-08 KR KR1020150064623A patent/KR20150129616A/en unknown
- 2015-05-11 CA CA2890977A patent/CA2890977A1/en not_active Abandoned
- 2015-05-12 JP JP2015097096A patent/JP2015227505A/en active Pending
- 2015-05-12 CN CN201510239365.4A patent/CN105088119B/en active Active
Also Published As
Publication number | Publication date |
---|---|
CA2890977A1 (en) | 2015-11-12 |
CN105088119B (en) | 2019-05-10 |
CN105088119A (en) | 2015-11-25 |
KR20150129616A (en) | 2015-11-20 |
JP2015227505A (en) | 2015-12-17 |
US20150322557A1 (en) | 2015-11-12 |
RU2684989C2 (en) | 2019-04-16 |
RU2015116523A3 (en) | 2018-11-12 |
EP2944402A1 (en) | 2015-11-18 |
EP2944402B1 (en) | 2019-04-03 |
US9670572B2 (en) | 2017-06-06 |
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