RU2014119880A - METHOD FOR PRODUCING A LOW TEMPERATURE ORGANIC HEAT CARRIER BASED ON PHENYLALKANE AND A DEVICE FOR ITS IMPLEMENTATION - Google Patents
METHOD FOR PRODUCING A LOW TEMPERATURE ORGANIC HEAT CARRIER BASED ON PHENYLALKANE AND A DEVICE FOR ITS IMPLEMENTATION Download PDFInfo
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- RU2014119880A RU2014119880A RU2014119880/05A RU2014119880A RU2014119880A RU 2014119880 A RU2014119880 A RU 2014119880A RU 2014119880/05 A RU2014119880/05 A RU 2014119880/05A RU 2014119880 A RU2014119880 A RU 2014119880A RU 2014119880 A RU2014119880 A RU 2014119880A
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- phenylalkane
- mixture
- phenyl compound
- alkylation
- acyclic paraffin
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Abstract
1. Способ получения низкотемпературного органического теплоносителя на основе фенилалкана, заключающийся в том, что ациклический парафин смешивают с фенильным соединением, полученную смесь нагревают, добавляют катализатор алкилирования, алкилируют смесь и выделяют фенилалкан путем дистилляции, отличающийся тем, что на смесь ациклического парафина и фенильного соединения в процессе операции алкилирования воздействуют ультразвуковыми колебаниями, при этом смесь нагревают до температуры 150-180°C и выдерживают в течение 50-70 минут.2. Устройство для получения низкотемпературного органического теплоносителя на основе фенилалкана по п. 1, содержащее емкость для ациклического парафина, емкость для фенильного соединения, смеситель, нагреватель, реактор алкилирования, дистиллятор, емкость сбора фенилалкана, причем выходы емкостей для ациклического парафина и фенильного соединения соединены параллельно и подключены последовательно к смесителю, нагревателю, реактору алкилирования, дистиллятору, емкости сбора фенилалкана, отличающееся тем, что оно снабжено волноводом с ультразвуковым излучателем, установленным внутри реактора алкилирования и генератором ультразвуковых колебаний, соединенным с ультразвуковым излучателем.1. A method of obtaining a low-temperature organic heat carrier based on phenylalkane, which consists in the fact that acyclic paraffin is mixed with a phenyl compound, the resulting mixture is heated, an alkylation catalyst is added, the mixture is alkylated and phenylalkane is isolated by distillation, characterized in that a mixture of acyclic paraffin and phenyl compound during the alkylation operation, they are affected by ultrasonic vibrations, while the mixture is heated to a temperature of 150-180 ° C and held for 50-70 minutes. 2. A device for producing a low-temperature organic phenylalkane-based coolant according to claim 1, comprising a container for acyclic paraffin, a container for phenyl compound, a mixer, a heater, an alkylation reactor, a distiller, a collection vessel for phenylalkane, and the outputs of the containers for acyclic paraffin and phenyl compound are connected in parallel and connected in series to a mixer, heater, alkylation reactor, distiller, phenylalkane collection tank, characterized in that it is equipped with a waveguide with ltrazvukovym emitter installed inside the alkylation reactor and the ultrasonic vibration generator connected with the ultrasonic transducer.
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RU2014119880/05A RU2014119880A (en) | 2014-05-19 | 2014-05-19 | METHOD FOR PRODUCING A LOW TEMPERATURE ORGANIC HEAT CARRIER BASED ON PHENYLALKANE AND A DEVICE FOR ITS IMPLEMENTATION |
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RU2014119880/05A RU2014119880A (en) | 2014-05-19 | 2014-05-19 | METHOD FOR PRODUCING A LOW TEMPERATURE ORGANIC HEAT CARRIER BASED ON PHENYLALKANE AND A DEVICE FOR ITS IMPLEMENTATION |
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RU2014119880A true RU2014119880A (en) | 2015-11-27 |
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RU2014119880/05A RU2014119880A (en) | 2014-05-19 | 2014-05-19 | METHOD FOR PRODUCING A LOW TEMPERATURE ORGANIC HEAT CARRIER BASED ON PHENYLALKANE AND A DEVICE FOR ITS IMPLEMENTATION |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2709889C1 (en) * | 2019-08-23 | 2019-12-23 | Акционерное общество "Акустический институт имени академика Н.Н. Андреева" | Method for continuous ultrasonic preparation of low-temperature organic heat carrier based on phenylalkane and device for its implementation |
RU2712456C1 (en) * | 2019-08-23 | 2020-01-29 | Акционерное общество "Акустический институт имени академика Н.Н. Андреева" | Method for continuous ultrasonic preparation of low-temperature organic heat carrier based on phenylalkane and device for its implementation |
-
2014
- 2014-05-19 RU RU2014119880/05A patent/RU2014119880A/en not_active Application Discontinuation
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2709889C1 (en) * | 2019-08-23 | 2019-12-23 | Акционерное общество "Акустический институт имени академика Н.Н. Андреева" | Method for continuous ultrasonic preparation of low-temperature organic heat carrier based on phenylalkane and device for its implementation |
RU2712456C1 (en) * | 2019-08-23 | 2020-01-29 | Акционерное общество "Акустический институт имени академика Н.Н. Андреева" | Method for continuous ultrasonic preparation of low-temperature organic heat carrier based on phenylalkane and device for its implementation |
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Legal Events
Date | Code | Title | Description |
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FA92 | Acknowledgement of application withdrawn (lack of supplementary materials submitted) |
Effective date: 20151028 |