RU2013152578A - METHOD FOR CHEMICAL CLEANING AND DEACTIVATION OF CIRCUITS OF RESEARCH AND ENERGY REACTORS COOLED WITH PRESSURE WATER - Google Patents

METHOD FOR CHEMICAL CLEANING AND DEACTIVATION OF CIRCUITS OF RESEARCH AND ENERGY REACTORS COOLED WITH PRESSURE WATER Download PDF

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RU2013152578A
RU2013152578A RU2013152578/06A RU2013152578A RU2013152578A RU 2013152578 A RU2013152578 A RU 2013152578A RU 2013152578/06 A RU2013152578/06 A RU 2013152578/06A RU 2013152578 A RU2013152578 A RU 2013152578A RU 2013152578 A RU2013152578 A RU 2013152578A
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Russia
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research
circuits
chemical cleaning
oedp
ammonia
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RU2013152578/06A
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Russian (ru)
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RU2558732C2 (en
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Александр Брониславович Гелбутовский
Игорь Константинович Степанов
Петр Иванович Черемисин
Андрей Игоревич Степанов
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Закрытое акционерное общество "Экомет-С"
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  • Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
  • Preventing Corrosion Or Incrustation Of Metals (AREA)

Abstract

Способ химической очистки и дезактивации контуров исследовательских и энергетических реакторов, охлаждаемых водой под давлением, водными растворами оксиэтилидендифосфоновой (ОЭДФ) кислоты, отличающийся тем, что обработку контура в сборе осуществляют 5÷20%-ными растворами ОЭДФ кислоты, нейтрализованными до величин рН 2,0÷2,9 аммиаком, или калиевой, или натриевой щелочью при температурах 55÷95°C, а по достижению постоянного значения величины рН (что соответствует окончанию процесса растворения рыхлой части железоокисных отложений) в контур вводят при циркуляции концентраты калиевой или натриевой щелочи или аммиака для создания в растворе величины рН 8,0÷8,5.The method of chemical cleaning and decontamination of the circuits of research and power reactors, cooled with water under pressure, with aqueous solutions of hydroxyethylidene diphosphonic (OEDP) acid, characterized in that the complete circuit is treated with 5-20% OEDP solutions of acid, neutralized to pH 2.0 ÷ 2.9 ammonia, or potassium, or sodium alkali at temperatures of 55 ÷ 95 ° C, and upon reaching a constant pH value (which corresponds to the end of the dissolution of the loose part of the iron oxide deposits) into the circuit in odyat while circulating concentrates potassium or sodium hydroxide or ammonia in solution to create a pH 8.0 ÷ 8.5.

Claims (1)

Способ химической очистки и дезактивации контуров исследовательских и энергетических реакторов, охлаждаемых водой под давлением, водными растворами оксиэтилидендифосфоновой (ОЭДФ) кислоты, отличающийся тем, что обработку контура в сборе осуществляют 5÷20%-ными растворами ОЭДФ кислоты, нейтрализованными до величин рН 2,0÷2,9 аммиаком, или калиевой, или натриевой щелочью при температурах 55÷95°C, а по достижению постоянного значения величины рН (что соответствует окончанию процесса растворения рыхлой части железоокисных отложений) в контур вводят при циркуляции концентраты калиевой или натриевой щелочи или аммиака для создания в растворе величины рН 8,0÷8,5. The method of chemical cleaning and decontamination of the circuits of research and power reactors, cooled with water under pressure, with aqueous solutions of hydroxyethylidene diphosphonic (OEDP) acid, characterized in that the complete circuit is treated with 5-20% OEDP solutions of acid, neutralized to pH 2.0 ÷ 2.9 ammonia, or potassium, or sodium alkali at temperatures of 55 ÷ 95 ° C, and upon reaching a constant pH value (which corresponds to the end of the dissolution of the loose part of the iron oxide deposits) into the circuit in odyat while circulating concentrates potassium or sodium hydroxide or ammonia in solution to create a pH 8.0 ÷ 8.5.
RU2013152578/06A 2013-11-26 2013-11-26 Method for chemical treatment and deactivation of pressured water-cooled research and power reactor circuits RU2558732C2 (en)

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RU2013152578/06A RU2558732C2 (en) 2013-11-26 2013-11-26 Method for chemical treatment and deactivation of pressured water-cooled research and power reactor circuits

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RU2013152578/06A RU2558732C2 (en) 2013-11-26 2013-11-26 Method for chemical treatment and deactivation of pressured water-cooled research and power reactor circuits

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RU2558732C2 RU2558732C2 (en) 2015-08-10

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Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH386450A (en) * 1961-05-13 1965-01-15 Borg Holding Ag Process for the chemical cleaning and treatment of devices, in particular steam generators
SU1366857A1 (en) * 1986-07-03 1988-01-15 Производственное Энергетическое Объединение "Алтайэнерго" Method of regenerating washing solution on the basis of ethylenediaminetetraacetic acid or salts thereof
SU1746203A1 (en) * 1990-06-04 1992-07-07 Всесоюзный Научно-Исследовательский Институт Горной Механики Им.М.М.Федорова Method of cleaning heat exchange surfaces from carbonate deposits
RU2303226C1 (en) * 2005-11-01 2007-07-20 Федеральное государственное унитарное предприятие "Научно-исследовательский технологический институт им. А.П. Александрова" Method for washing a steam generator
RU2313053C1 (en) * 2006-05-18 2007-12-20 Открытое акционерное общество "Всероссийский дважды ордена Трудового Красного Знамени теплотехнический научно-исследовательский институт" (ОАО "ВТИ") Method for steam-chemical cleaning of internal surfaces of boiler pipes from precipitations

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Effective date: 20181127