RU2009143206A - CALCIUM-PHOSPHATE BIOLOGICALLY ACTIVE COATING ON THE IMPLANT AND METHOD OF ITS APPLICATION - Google Patents
CALCIUM-PHOSPHATE BIOLOGICALLY ACTIVE COATING ON THE IMPLANT AND METHOD OF ITS APPLICATION Download PDFInfo
- Publication number
- RU2009143206A RU2009143206A RU2009143206/15A RU2009143206A RU2009143206A RU 2009143206 A RU2009143206 A RU 2009143206A RU 2009143206/15 A RU2009143206/15 A RU 2009143206/15A RU 2009143206 A RU2009143206 A RU 2009143206A RU 2009143206 A RU2009143206 A RU 2009143206A
- Authority
- RU
- Russia
- Prior art keywords
- calcium
- compounds
- base
- spark
- implant
- Prior art date
Links
Landscapes
- Materials For Medical Uses (AREA)
Abstract
1. Кальций-фосфатное биологически активное покрытие на имплантате, основа которого выполнена из конструкционного материала, в частности из нержавеющей стали, содержащее нанесенный на основу промежуточный слой металла вентильной группы, в частности титана толщиной 5-50 мкм и последующий слой кальций-фосфатных соединений, нанесенный электрохимическим методом анодирования титана в режиме искрового или дугового разрядов. ! 2. Способ нанесения покрытия по п.1, в котором промежуточный слой вентильного металла на материал основы наносят в плазме непрерывного вакуумно-дугового разряда, а последующий слой кальций-фосфатных соединений формируют методом анодирования импульсным или постоянным током в условиях искрового или дугового разрядов в растворе фосфорной кислоты концентрацией 5-33% с добавлением соединений кальция до сверхпересыщенного состояния. ! 3. Способ нанесения покрытия по п.2, отличающийся тем, что в качестве соединений кальция выбирают СаО и дополнительно добавляют в раствор 5-10% порошка гидроксиапатита дисперсностью не более 70 мкм. 1. Calcium-phosphate biologically active coating on the implant, the base of which is made of a structural material, in particular stainless steel, containing an intermediate layer of a valve group deposited on the base, in particular titanium with a thickness of 5-50 μm and a subsequent layer of calcium phosphate compounds, deposited by the electrochemical method of anodizing titanium in the mode of spark or arc discharges. ! 2. The coating method according to claim 1, in which the intermediate layer of the valve metal on the base material is applied in a plasma of a continuous vacuum arc discharge, and the subsequent layer of calcium phosphate compounds is formed by anodizing by pulsed or direct current in the conditions of spark or arc discharges in solution phosphoric acid with a concentration of 5-33% with the addition of calcium compounds to a supersaturated state. ! 3. The coating method according to claim 2, characterized in that CaO is selected as calcium compounds and 5-10% hydroxyapatite powder with a dispersion of not more than 70 μm is additionally added to the solution.
Claims (3)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RU2009143206/15A RU2423150C1 (en) | 2009-11-23 | 2009-11-23 | Calcium-phosphate biologically active coating of implant and method of deposition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RU2009143206/15A RU2423150C1 (en) | 2009-11-23 | 2009-11-23 | Calcium-phosphate biologically active coating of implant and method of deposition |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2009143206A true RU2009143206A (en) | 2011-05-27 |
| RU2423150C1 RU2423150C1 (en) | 2011-07-10 |
Family
ID=44734554
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2009143206/15A RU2423150C1 (en) | 2009-11-23 | 2009-11-23 | Calcium-phosphate biologically active coating of implant and method of deposition |
Country Status (1)
| Country | Link |
|---|---|
| RU (1) | RU2423150C1 (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2523410C1 (en) * | 2013-04-09 | 2014-07-20 | Федеральное государственное бюджетное образовательное учреждение высшего профессионального образования "Новосибирский государственный технический университет" | Method for preparing nanostructured calcium-phosphate coating for medical implants |
| RU2572004C1 (en) * | 2014-10-31 | 2015-12-27 | Федеральное государственное унитарное предприятие "ЭКСПЕРИМЕНТАЛЬНО-ПРОИЗВОДСТВЕННЫЕ МАСТЕРСКИЕ" Федерального медико-биологического агентства | Method of treating delayed union and unfused fractures of long bones |
| RU2598626C1 (en) * | 2015-06-11 | 2016-09-27 | Федеральное государственное автономное образовательное учреждение высшего профессионального образования "Белгородский государственный национальный исследовательский университет" (НИУ "БелГУ") | Method of forming a bioactive coating on surface of major joint endoprosthesis |
| RU2593346C1 (en) * | 2015-07-24 | 2016-08-10 | Александр Анатольевич Марков | Synthetic bioactive calcium-phosphate mineral complex |
| RU2617252C2 (en) * | 2015-08-14 | 2017-04-24 | федеральное государственное бюджетное образовательное учреждение высшего образования "Тюменский государственный медицинский университет" Министерства здравоохранения Российской Федерации (ФГБОУ ВО Тюменский ГМУ Минздрава России) | Method of calcium-phosphate coatings processing on implants |
| US10537661B2 (en) * | 2017-03-28 | 2020-01-21 | DePuy Synthes Products, Inc. | Orthopedic implant having a crystalline calcium phosphate coating and methods for making the same |
| US10537658B2 (en) | 2017-03-28 | 2020-01-21 | DePuy Synthes Products, Inc. | Orthopedic implant having a crystalline gallium-containing hydroxyapatite coating and methods for making the same |
-
2009
- 2009-11-23 RU RU2009143206/15A patent/RU2423150C1/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| RU2423150C1 (en) | 2011-07-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| RU2009143206A (en) | CALCIUM-PHOSPHATE BIOLOGICALLY ACTIVE COATING ON THE IMPLANT AND METHOD OF ITS APPLICATION | |
| Anada et al. | Dose-dependent osteogenic effect of octacalcium phosphate on mouse bone marrow stromal cells | |
| Gupta et al. | Status of surface treatment in endosseous implant: a literary overview | |
| Durdu et al. | Characterization and formation of hydroxyapatite on Ti6Al4V coated by plasma electrolytic oxidation | |
| Suh et al. | Effect of hydrothermally treated anodic oxide films on osteoblast attachment and proliferation | |
| Schumacher et al. | Strontium substitution in apatitic CaP cements effectively attenuates osteoclastic resorption but does not inhibit osteoclastogenesis | |
| Kim et al. | Anodically nanostructured titanium oxides for implant applications | |
| ES2385770T3 (en) | Method to form a bioactive coating | |
| Oya et al. | Calcification by MC3T3-E1 cells on RGD peptide immobilized on titanium through electrodeposited PEG | |
| Bai et al. | One-step approach for hydroxyapatite-incorporated TiO2 coating on titanium via a combined technique of micro-arc oxidation and electrophoretic deposition | |
| Park et al. | Bioactivity evaluation of porous TiO2 surface formed on titanium in mixed electrolyte by spark anodization | |
| Hu et al. | Preparation and in vitro evaluation of nanostructured TiO2/TCP composite coating by plasma electrolytic oxidation | |
| Shin et al. | In vitro biological response to the oxide layer in pure titanium formed at different current densities by plasma electrolytic oxidation | |
| Park et al. | Surface characteristics and primary bone marrow stromal cell response of a nanostructured strontium‐containing oxide layer produced on a microrough titanium surface | |
| WO2013159500A1 (en) | Micro-arc oxidized, self-closing-pore, active coating of magnesium-based implant material and preparation method therefor | |
| Liu et al. | Enhanced bioactive and osteogenic activities of titanium by modification with phytic acid and calcium hydroxide | |
| CN101138652A (en) | Preparation method of high-bioactivity surface stephanoporate implant composite material | |
| Guan et al. | Enhanced cytocompatibility of Ti6Al4V alloy through selective removal of Al and V from the hierarchical micro-arc oxidation coating | |
| Sandrini et al. | In vitro assessment of the osteointegrative potential of a novel multiphase anodic spark deposition coating for orthopaedic and dental implants | |
| Fuentes et al. | Advanced surface treatments on titanium and titanium alloys focused on electrochemical and physical technologies for biomedical applications | |
| Liu et al. | Enhancing biological properties of porous coatings through the incorporation of manganese | |
| Gu et al. | Degradation and biocompatibility of a series of strontium substituted hydroxyapatite coatings on magnesium alloys | |
| BR112014010980A2 (en) | thin electrolyte for biocompatible plasma electroplating coatings in implant magnesium material | |
| Li et al. | Evaluation of the osteo-inductive potential of hollow three-dimensional magnesium-strontium substitutes for the bone grafting application | |
| Bernhardt et al. | In vitro osteogenic potential of human bone marrow stromal cells cultivated in porous scaffolds from mineralized collagen |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM4A | The patent is invalid due to non-payment of fees |
Effective date: 20111124 |
|
| NF4A | Reinstatement of patent |
Effective date: 20130410 |
|
| MM4A | The patent is invalid due to non-payment of fees |
Effective date: 20181124 |