RU2005107001A - CONTACT STRUCTURES - Google Patents

CONTACT STRUCTURES Download PDF

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RU2005107001A
RU2005107001A RU2005107001/15A RU2005107001A RU2005107001A RU 2005107001 A RU2005107001 A RU 2005107001A RU 2005107001/15 A RU2005107001/15 A RU 2005107001/15A RU 2005107001 A RU2005107001 A RU 2005107001A RU 2005107001 A RU2005107001 A RU 2005107001A
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Russia
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dispersing device
compound according
multicore
wire
catalytic
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RU2005107001/15A
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Russian (ru)
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RU2318590C2 (en
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Лоренс А. мл. СМИТ (US)
Лоренс А. мл. СМИТ
Абрахам П. ГЕЛБЕЙН (US)
Абрахам П. ГЕЛБЕЙН
Джон Р. АДАМС (US)
Джон Р. АДАМС
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Каталитик Дистиллейшн Текнолоджиз (Us)
Каталитик Дистиллейшн Текнолоджиз
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    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/248—Reactors comprising multiple separated flow channels
    • B01J19/2495—Net-type reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/009—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping in combination with chemical reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/32—Packing elements in the form of grids or built-up elements for forming a unit or module inside the apparatus for mass or heat transfer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B01J35/56—Foraminous structures having flow-through passages or channels, e.g. grids or three-dimensional monoliths
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    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G29/00—Refining of hydrocarbon oils, in the absence of hydrogen, with other chemicals
    • C10G29/20—Organic compounds not containing metal atoms
    • C10G29/205—Organic compounds not containing metal atoms by reaction with hydrocarbons added to the hydrocarbon oil
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G50/00—Production of liquid hydrocarbon mixtures from lower carbon number hydrocarbons, e.g. by oligomerisation
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    • B01J2219/322—Basic shape of the elements
    • B01J2219/32203—Sheets
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    • B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
    • B01J2219/322—Basic shape of the elements
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    • B01J2219/32224—Sheets characterised by the orientation of the sheet
    • B01J2219/32227—Vertical orientation
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    • B01J2219/322—Basic shape of the elements
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    • B01J2219/32289—Stretched materials
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    • B—PERFORMING OPERATIONS; TRANSPORTING
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    • B01J2219/32416—Metal fibrous
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    • B—PERFORMING OPERATIONS; TRANSPORTING
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    • B01J2219/32466—Composition or microstructure of the elements comprising catalytically active material
    • B—PERFORMING OPERATIONS; TRANSPORTING
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  • Chemical & Material Sciences (AREA)
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  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
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Claims (26)

1. Соединение вертикального реактора для осуществления каталитических реакций и диспергирующего устройства, расположенного в вертикальном реакторе, причем диспергирующее устройство содержит, по меньшей мере, 50 об.% открытого пространства.1. The connection of a vertical reactor for carrying out catalytic reactions and a dispersing device located in a vertical reactor, and the dispersing device contains at least 50 vol.% Open space. 2. Соединение по п.1, в котором открытое пространство составляет примерно до 97 об.%.2. The compound according to claim 1, in which the open space is up to about 97 vol.%. 3. Соединение по п.1, в котором диспергирующее устройство содержит проволоку в виде сетки, сплетенную с многожильным компонентом, или растянутый металл, переплетенный вместе с многожильным компонентом, причем многожильную нить выбирают из инертных полимеров, каталитических полимеров, каталитических металлов или их смесей.3. The compound according to claim 1, in which the dispersing device comprises a wire in the form of a mesh braided with a multicore component, or a stretched metal intertwined with a multicore component, wherein the multicore strand is selected from inert polymers, catalytic polymers, catalytic metals or mixtures thereof. 4. Соединение по п.3, в котором диспергирующее устройство содержит сплетенную сетку из проволоки и полимерную сетку.4. The compound according to claim 3, in which the dispersing device comprises a woven wire mesh and a polymer network. 5. Соединение по п.3, в котором диспергирующее устройство содержит сплетенные вместе проволоку в виде сетки и стекловолокно.5. The compound according to claim 3, in which the dispersing device comprises woven together a wire in the form of a mesh and fiberglass. 6. Соединение по п.3, в котором диспергирующее устройство содержит сетку их сплетенных вместе проволоки и многожильного компонента, включающего тефлон, стальную шерсть, полипропилен, PVDF, полиэстер или их сочетание.6. The compound according to claim 3, in which the dispersing device comprises a grid of their wire braided together and a multicore component comprising Teflon, steel wool, polypropylene, PVDF, polyester, or a combination thereof. 7. Соединение по п.3, в котором диспергирующее устройство расположено в виде множества размещенных вертикально поперечных матов внутри и поперек вертикального реактора.7. The compound according to claim 3, in which the dispersing device is located in the form of many vertically placed transverse mats inside and across the vertical reactor. 8. Соединение по п.3, в котором проволочная сетка обеспечивает структурную целостность системы, и открытое пространство в реакторе требуется для перемещения паров и жидкостей через него.8. The compound according to claim 3, in which the wire mesh ensures the structural integrity of the system, and open space in the reactor is required to move vapors and liquids through it. 9. Соединение по п.3, в котором диспергирующее устройство содержит листы, пучки или пакеты из сплетенных вместе проволоки и многожильного компонента или их сочетания.9. The compound according to claim 3, in which the dispersing device comprises sheets, bundles or packets of woven together wire and a multicore component or a combination thereof. 10. Соединение по п.3, в котором диспергирующее устройство содержит многожильный каталитический материал из сульфонированной виниловой смолы, Ni, R, Co, Mo, Ag или их смесей.10. The compound according to claim 3, in which the dispersing device contains a multicore catalytic material from sulfonated vinyl resin, Ni, R, Co, Mo, Ag, or mixtures thereof. 11. Соединение для осуществления каталитических реакций в совмещенном нисходящем потоке, содержащее вертикальный реактор, диспергирующее устройство, расположенное в вертикальном реакторе, содержащее, по меньшей мере, один частично жидкий реагент, катализатор и реакционные условия для поддержания частично жидкого реагента при температуре кипения.11. Compound for carrying out catalytic reactions in a combined downward stream containing a vertical reactor, a dispersing device located in a vertical reactor containing at least one partially liquid reagent, catalyst and reaction conditions for maintaining a partially liquid reagent at a boiling point. 12. Соединение по п.11, в котором диспергирующее устройство содержит проволоку в виде сетки, сплетенную вместе с многожильным компонентом, или растянутый металл, переплетенный вместе с многожильным компонентом, причем многожильную нить выбирают из инертных полимеров, каталитических полимеров, каталитических металлов или их смесей.12. The compound according to claim 11, in which the dispersing device comprises a wire in the form of a mesh, woven together with a multicore component, or a stretched metal interwoven together with a multicore component, the multicore string being selected from inert polymers, catalytic polymers, catalytic metals or mixtures thereof . 13. Соединение по п.11, в котором диспергирующее устройство содержит сплетенные вместе сетку из проволоки и полимерную сетку.13. The compound of claim 11, wherein the dispersing device comprises a wire mesh and a polymer network woven together. 14. Соединение по п.11, в котором диспергирующее устройство содержит сплетенные вместе проволоку в виде сетки и стекловолокно.14. The compound according to claim 11, in which the dispersing device comprises woven together a wire in the form of a mesh and fiberglass. 15. Соединение по п.11, в котором диспергирующее устройство содержит сетку из сплетенных вместе проволоки и многожильного компонента, включающего тефлон, стальную шерсть, полипропилен, PVDF, полиэстер или их сочетание.15. The compound according to claim 11, in which the dispersing device comprises a grid of woven together wire and a multicore component comprising Teflon, steel wool, polypropylene, PVDF, polyester, or a combination thereof. 16. Соединение по п.11, в котором диспергирующее устройство расположено в виде множества расположенных вертикально поперечных матов, внутри и поперек вертикального реактора.16. The compound according to claim 11, in which the dispersing device is located in the form of a plurality of vertically arranged transverse mats, inside and across the vertical reactor. 17. Соединение по п.11, в котором проволочная сетка обеспечивает структурную целостность системы, и открытое пространство в реакторе требуется через него для перемещения паров и жидкостей.17. The compound according to claim 11, in which the wire mesh ensures the structural integrity of the system, and open space in the reactor is required through it to move vapors and liquids. 18. Соединение по п.11, в котором диспергирующее устройство содержит листы, пучки или пакеты из сплетенных вместе проволоки и многожильного компонента или их сочетания.18. The compound according to claim 11, in which the dispersing device comprises sheets, bundles or packets of woven together wire and a multicore component, or a combination thereof. 19. Соединение по п.11, в котором диспергирующее устройство содержит многожильный каталитический материал из сульфонированной виниловой смолы, Ni, R, Co, Mo, Ag или их смесей.19. The compound according to claim 11, in which the dispersing device contains a multicore catalytic material from sulfonated vinyl resin, Ni, R, Co, Mo, Ag, or mixtures thereof. 20. Соединение по п.11, в котором присутствуют, по меньшей мере, две фазы.20. The compound according to claim 11, in which at least two phases are present. 21. Диспергирующее устройство, содержащее проволоку в виде сетки или растянутый металл, сплетенный вместе с многожильным материалом, выбранным из каталитических полимеров, каталитических металлов или их смесей.21. Dispersing device containing a wire in the form of a mesh or a stretched metal, woven together with a multicore material selected from catalytic polymers, catalytic metals or mixtures thereof. 22. Диспергирующее устройство по п.21, которое содержит многожильный каталитический материал из сульфонированной виниловой смолы, Ni, R, Co, Mo, Ag или их смесей.22. The dispersing device according to item 21, which contains a multicore catalytic material from sulfonated vinyl resin, Ni, R, Co, Mo, Ag or mixtures thereof. 23. Диспергирующее устройство по п.21, которое содержит, по меньшей мере, 50 об.% открытого пространства.23. The dispersing device according to item 21, which contains at least 50 vol.% Open space. 24. Диспергирующее устройство по п.21, в котором диспергирующее устройство содержит примерно до 97 об.% открытого пространства.24. The dispersing device according to item 21, in which the dispersing device contains up to about 97 vol.% Open space. 25. Соединение по п.1, в котором диспергирующее устройство содержит структуру, которая имеет жесткую рамку, изготовленную из двух по существу вертикальных двойных решеток, расположенных на расстоянии друг от друга и удерживаемых в жестком состоянии посредством множества по существу горизонтальных жестких элементов и множества по существу горизонтальных трубок из проволочной сетки, прикрепленных к решеткам для формирования множества проходов для текучих сред между трубками, причем трубки являются пустыми или содержат каталитические или некаталитические материалы.25. The compound according to claim 1, in which the dispersing device comprises a structure that has a rigid frame made of two essentially vertical double gratings located at a distance from each other and held in a rigid state by a plurality of essentially horizontal rigid elements and a plurality of essentially horizontal tubes of wire mesh attached to the gratings to form a plurality of fluid passages between the tubes, the tubes being empty or containing catalytic sludge non-catalytic materials. 26. Соединение по п.1, в котором диспергирующее устройство содержит структуру, содержащую множество листов проволочной сетки, сформированной в виде изгибов V-образной формы, имеющих плоские участки между V-образными выступами, причем множество листов имеет по существу однородный размер, и они имеют выступы, ориентированные в одном направлении и по существу совмещенные друг с другом, при этом листы разделены множеством жестких элементов, ориентированных по нормали к V-образным выступам и находящихся на них.26. The compound according to claim 1, in which the dispersing device comprises a structure comprising a plurality of sheets of wire mesh formed in the form of bends of a V-shape having flat sections between the V-shaped protrusions, and the many sheets have a substantially uniform size, and they they have protrusions oriented in one direction and essentially aligned with each other, while the sheets are separated by many rigid elements oriented normal to the V-shaped protrusions and located on them.
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