RU1803407C - Method of 2,3,6,7 - difurazano -4,5- diaza -1,8,11, -trioxacyclotridecatriene -2,4,6 - synthesis - Google Patents

Method of 2,3,6,7 - difurazano -4,5- diaza -1,8,11, -trioxacyclotridecatriene -2,4,6 - synthesis

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Publication number
RU1803407C
RU1803407C SU914927512A SU4927512A RU1803407C RU 1803407 C RU1803407 C RU 1803407C SU 914927512 A SU914927512 A SU 914927512A SU 4927512 A SU4927512 A SU 4927512A RU 1803407 C RU1803407 C RU 1803407C
Authority
RU
Russia
Prior art keywords
difurazano
diaza
trioxacyclotridecatriene
synthesis
oxacyclotridecatriene
Prior art date
Application number
SU914927512A
Other languages
Russian (ru)
Inventor
Алексей Борисович Шереметев
Ольга Викторовна Харитонова
Татьяна Семеновна Новикова
Ленор Иванович Хмельницкий
Original Assignee
Институт органической химии им.Н.Д.Зелинского
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Институт органической химии им.Н.Д.Зелинского filed Critical Институт органической химии им.Н.Д.Зелинского
Priority to SU914927512A priority Critical patent/RU1803407C/en
Application granted granted Critical
Publication of RU1803407C publication Critical patent/RU1803407C/en

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Abstract

Использование: в качестве катализатора гетерофазных реакций. Сущность изобре- тени :2,3,6,7-дифуразано-4,5-диаза-1,8,11-три- оксациклотридекатриен-2,4,6. БФ CsHeNeOs, выход 52%, т.пл. 94-95°С. Соединение получают взаимодействием бис-(3-аминофура- занилового) эфира диэтиленгликол  с М,М-дибромизоциануратом в среде инертного органического растворител  при 20-40°С.Usage: as a catalyst for heterophase reactions. SUMMARY OF THE INVENTION: 2,3,6,7-difurazano-4,5-diaza-1,8,11-tri-oxacyclotridecatriene-2,4,6. BP CsHeNeOs, yield 52%, mp. 94-95 ° C. The compound is prepared by reacting diethylene glycol bis (3-aminofuranosanil) ether with M, M-dibromisocyanurate in an inert organic solvent at 20-40 ° C.

Description

Изобретение относитс  к способу получени  новой гетероциклической системы - 2,3,6,7-дифуразано-4,5-диаза-1,8,11-триок- сациклотридекатриена-2,4,6 формулы IThe invention relates to a method for producing a new heterocyclic system - 2,3,6,7-difurazano-4,5-diaza-1,8,11-trioxacyclotridecatriene-2,4,6 of the formula I

НО ОН ,WBUT HE W

Nf4)N+0(CH2CH2C1)2Nf4) N + 0 (CH2CH2C1) 2

NOOHNooh

SU914927512A 1991-04-18 1991-04-18 Method of 2,3,6,7 - difurazano -4,5- diaza -1,8,11, -trioxacyclotridecatriene -2,4,6 - synthesis RU1803407C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU914927512A RU1803407C (en) 1991-04-18 1991-04-18 Method of 2,3,6,7 - difurazano -4,5- diaza -1,8,11, -trioxacyclotridecatriene -2,4,6 - synthesis

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU914927512A RU1803407C (en) 1991-04-18 1991-04-18 Method of 2,3,6,7 - difurazano -4,5- diaza -1,8,11, -trioxacyclotridecatriene -2,4,6 - synthesis

Publications (1)

Publication Number Publication Date
RU1803407C true RU1803407C (en) 1993-03-23

Family

ID=21569760

Family Applications (1)

Application Number Title Priority Date Filing Date
SU914927512A RU1803407C (en) 1991-04-18 1991-04-18 Method of 2,3,6,7 - difurazano -4,5- diaza -1,8,11, -trioxacyclotridecatriene -2,4,6 - synthesis

Country Status (1)

Country Link
RU (1) RU1803407C (en)

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Авторское свидетельство СССР № 1756320, кл. 1756320, кл. С 07 D 498/14, 1990. *

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