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Application filed by Institutul De Cercetari Chimico-FarmaceuticefiledCriticalInstitutul De Cercetari Chimico-Farmaceutice
Priority to RO83111898ApriorityCriticalpatent/RO87519A2/en
Publication of RO87519B1publicationCriticalpatent/RO87519B1/en
Publication of RO87519A2publicationCriticalpatent/RO87519A2/en
Organic Low-Molecular-Weight Compounds And Preparation Thereof
(AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts
(AREA)
Abstract
Inventia se refera la un procedeu de obtinere a malonatului de difenil prin esterificare cu fenol în prezenta oxiclorurii de fosfor, conform caruia se supune esterificarii malonatul de sodiu, la raportul molar malonat de sodiu: fenol: POCl3 de 1: 2: 1,25 la 65-70 degree C timp de 6 h.The invention relates to a process for the preparation of diphenyl malonate by esterification with phenol in the presence of phosphorus oxychloride according to which the sodium malonate is esterified to the molar ratio of sodium: phenol: POCl3 of 1: 2: 1.25 to 65-70 ° C for 6 hours.
RO83111898A1983-08-181983-08-18
PROCESS OF OBTAINING THE MILLION OF DIFFERENCE
RO87519A2
(en)
SINGLE STAGE FERMENTATION PROCEDURE FOR THE PREPARATION OF 9-HYDROXY-3-BONE-4,17 (20) -PREGNADIEN-20-CARBOXYLIC ACID, USEFUL AS INTERMEDIATE FOR THE PRODUCTION OF STERROIDS