RO85396B1 - Process for preparing 2-(diethylamine)-n-(2'-6'-dimethylphenyl)-acetamide - Google Patents

Process for preparing 2-(diethylamine)-n-(2'-6'-dimethylphenyl)-acetamide

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Publication number
RO85396B1
RO85396B1 RO109665A RO10966583A RO85396B1 RO 85396 B1 RO85396 B1 RO 85396B1 RO 109665 A RO109665 A RO 109665A RO 10966583 A RO10966583 A RO 10966583A RO 85396 B1 RO85396 B1 RO 85396B1
Authority
RO
Romania
Prior art keywords
dimethylphenyl
acetamide
diethylamine
preparing
chloro
Prior art date
Application number
RO109665A
Other languages
Romanian (ro)
Other versions
RO85396A2 (en
Inventor
Ferent Stefan Lozinschi
Nora Radulescu
Mariana Ionescu
Dumitru Manolache
Petre Panculescu
Lucian Harles
Mariana Simina Ionescu
Georgeta Filip
Mariana Zana
Original Assignee
Institutul De Cercetari Chimico-Farmaceutice
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Institutul De Cercetari Chimico-Farmaceutice filed Critical Institutul De Cercetari Chimico-Farmaceutice
Priority to RO109665A priority Critical patent/RO85396B1/en
Publication of RO85396A2 publication Critical patent/RO85396A2/en
Publication of RO85396B1 publication Critical patent/RO85396B1/en
Priority to RO84116875A priority patent/RO89961A3/en

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  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Inventia se refera la un procedeu de obtinere a 2(dietilamino)-N-(2', 6'-dimetilfenil) acetamidei (xilina) prin condensarea 2-clor-N-(2', 6'-dimetilfenil)acetamidei cu dietilamina în care reactia are loc la raporturi molare dietilamina: 2-clor-N-(2', 6'-dimetilfenil) acetamida 2,5...3:1 prin încalzirea în autoclava închisa la temperaturi de 80...125 degree C, timp de 5...10h, iar produsul se izoleaza prin turnare pe apa rece, filtrare si uscare. The invention relates to a process for the preparation of 2 (diethylamino) -N- (2 ', 6'-dimethylphenyl) acetamide (xylene) by condensing 2-chloro-N- (2', 6'-dimethylphenyl) acetamide with diethylamine in which reaction takes place at molar ratios of 2.5-3: 1 diethylamine: 2-chloro-N- (2 ', 6'-dimethylphenyl) acetamide by heating in the autoclave at temperatures of 80-125 ° C, for 5 to 10 hours, and the product is isolated by casting on cold water, filtration and drying.

RO109665A 1983-01-11 1983-01-11 Process for preparing 2-(diethylamine)-n-(2'-6'-dimethylphenyl)-acetamide RO85396B1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
RO109665A RO85396B1 (en) 1983-01-11 1983-01-11 Process for preparing 2-(diethylamine)-n-(2'-6'-dimethylphenyl)-acetamide
RO84116875A RO89961A3 (en) 1983-01-11 1984-12-25 PROCESS FOR OBTAINING 2- (DETYLAMINO) -N- (2 ', 6'-DIMETHYLPHENYL) -ACETAMIDE

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
RO109665A RO85396B1 (en) 1983-01-11 1983-01-11 Process for preparing 2-(diethylamine)-n-(2'-6'-dimethylphenyl)-acetamide

Publications (2)

Publication Number Publication Date
RO85396A2 RO85396A2 (en) 1984-10-31
RO85396B1 true RO85396B1 (en) 1984-11-30

Family

ID=20112521

Family Applications (2)

Application Number Title Priority Date Filing Date
RO109665A RO85396B1 (en) 1983-01-11 1983-01-11 Process for preparing 2-(diethylamine)-n-(2'-6'-dimethylphenyl)-acetamide
RO84116875A RO89961A3 (en) 1983-01-11 1984-12-25 PROCESS FOR OBTAINING 2- (DETYLAMINO) -N- (2 ', 6'-DIMETHYLPHENYL) -ACETAMIDE

Family Applications After (1)

Application Number Title Priority Date Filing Date
RO84116875A RO89961A3 (en) 1983-01-11 1984-12-25 PROCESS FOR OBTAINING 2- (DETYLAMINO) -N- (2 ', 6'-DIMETHYLPHENYL) -ACETAMIDE

Country Status (1)

Country Link
RO (2) RO85396B1 (en)

Also Published As

Publication number Publication date
RO89961A3 (en) 1986-08-30
RO85396A2 (en) 1984-10-31

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