RO84436B1 - Procedeu de preparare a(e)-8-(e)-10-dodecadien-1-01-olului - Google Patents
Procedeu de preparare a(e)-8-(e)-10-dodecadien-1-01-oluluiInfo
- Publication number
- RO84436B1 RO84436B1 RO107408A RO10740882A RO84436B1 RO 84436 B1 RO84436 B1 RO 84436B1 RO 107408 A RO107408 A RO 107408A RO 10740882 A RO10740882 A RO 10740882A RO 84436 B1 RO84436 B1 RO 84436B1
- Authority
- RO
- Romania
- Prior art keywords
- dodecadien
- dodecadiene
- tert
- sulfuric acid
- preparing
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 2
- 229910021592 Copper(II) chloride Inorganic materials 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 abstract 1
- 238000010511 deprotection reaction Methods 0.000 abstract 1
- 238000010790 dilution Methods 0.000 abstract 1
- 239000012895 dilution Substances 0.000 abstract 1
- PSLIMVZEAPALCD-UHFFFAOYSA-N ethanol;ethoxyethane Chemical compound CCO.CCOCC PSLIMVZEAPALCD-UHFFFAOYSA-N 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- 238000000622 liquid--liquid extraction Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000003208 petroleum Substances 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000010992 reflux Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 238000000638 solvent extraction Methods 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Inventia se refera la un procedeu de preparare a (E)-8-(E)-10-dodecadien-1-olului, conform caruia se cupleaza 1-acetoxi-(E)-2, (E)-4-hexadiena cu compusul magnezian al 1-Cl-6-tert-butoxi-hexanului, la un raport molar de 1/1...1,5 în mediu de eter etilic, în prezenta catalizatorului de Li2(CuCl2), la temperatura de -10...+5 degree C, raportul molar catalizator/1-actoxi-(E)-2, (E)-4-hexadiena fiind 0,02...0,04 deprotejarea 1-tert-butoxi-(E)-8, (E)-10-dodecadienei obtinute realizîndu-se prin hidroliza în solutie etanolica de acid sulfuric 5...15%, la reflux, timp de 2...15h, la un raport de dilutie produs/acid sulfuric etanolic = 1/20...35, dupa care se purifica (E)-8-(E)-10-dodecadien-1-olul brut, obtinut prin extractie lichid-lichid cu eter de petrol-etanol 50%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RO107408A RO84436B1 (ro) | 1982-05-03 | 1982-05-03 | Procedeu de preparare a(e)-8-(e)-10-dodecadien-1-01-olului |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RO107408A RO84436B1 (ro) | 1982-05-03 | 1982-05-03 | Procedeu de preparare a(e)-8-(e)-10-dodecadien-1-01-olului |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RO84436A2 RO84436A2 (ro) | 1984-06-21 |
| RO84436B1 true RO84436B1 (ro) | 1984-08-30 |
Family
ID=20111463
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RO107408A RO84436B1 (ro) | 1982-05-03 | 1982-05-03 | Procedeu de preparare a(e)-8-(e)-10-dodecadien-1-01-olului |
Country Status (1)
| Country | Link |
|---|---|
| RO (1) | RO84436B1 (ro) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102030617A (zh) * | 2010-11-16 | 2011-04-27 | 北京颖新泰康国际贸易有限公司 | 昆虫性信息素型化合物以及昆虫性信息素醚系和酯系化合物的制备方法 |
-
1982
- 1982-05-03 RO RO107408A patent/RO84436B1/ro unknown
Also Published As
| Publication number | Publication date |
|---|---|
| RO84436A2 (ro) | 1984-06-21 |
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