PL97302B1 - CRYSTATE FOR INTERMEDIATE TEMPERATURES - Google Patents

CRYSTATE FOR INTERMEDIATE TEMPERATURES Download PDF

Info

Publication number
PL97302B1
PL97302B1 PL18463875A PL18463875A PL97302B1 PL 97302 B1 PL97302 B1 PL 97302B1 PL 18463875 A PL18463875 A PL 18463875A PL 18463875 A PL18463875 A PL 18463875A PL 97302 B1 PL97302 B1 PL 97302B1
Authority
PL
Poland
Prior art keywords
insert
parts
cryostat
thermal conductivity
temperature
Prior art date
Application number
PL18463875A
Other languages
Polish (pl)
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Priority to PL18463875A priority Critical patent/PL97302B1/en
Publication of PL97302B1 publication Critical patent/PL97302B1/en

Links

Landscapes

  • Measuring Temperature Or Quantity Of Heat (AREA)

Description

Przedmiotem wynalazku jest kriostat dla temperatur posrednich znajdujacy zastosowanie zwlaszcza dla malych próbek w fizyce i chemii ciala stalego.Znany stan techniki. Konwencjonalne kriostaty zawieraja z reguly elektroniczne uklady regulacji, które na podstawie wskazan termopary steruja czlonem wykonawczym zmieniajacym doplyw ciepla. Sa to urzadzenia o rozbudowanej konstrukcji i zlozonym systemem sterowania. W praktyce laboratoryjnej stosuje sie czasem wkladki miedziane, których zakonczenie zanurzone jest w czynniku chlodzacym, np. w cieklym azocie.Wkladka taka pozwala osiagnac temperature okolo 10-15° wyzsza od temperatury czynnika chlodzacego.Istota wynalazku. W kriostacie wedlug wynalazku wkladka wykonana z materialu o dobrym przewodnictwie cieplnym sklada sie z dwóch czesci, pomiedzy którymi umieszczony jest wymieniony element z materialu o zlym przewodnictwie cieplnym. Obie czesci wkladki z materialu o dobrym przewodnictwie cieplnym polaczone jest z elementem wykonanym z materialu o zlym przewodnictwie cieplnym w sposób rozlaczny umozliwiajacy zmiane grubosci tej warstwy.Korzystne skutki techniczne wynalazku. Kriostat wedlug wynalazku rozszerza w sposób istotny zakres stosowalnosci typowych, masowo produkowanych naczyn Dewara. Dzieki prostej konstrukcji kriostat wykazuje duza niezawodnosc oraz stabilnosc pracy. Poczatkowy okres ustalania sie warunków pracy kriostatu mozna wykorzystac dla pracy w rezimie regulowanego narastania lub spadku temperatury co w konwencjonalnych kriostatach wymaga dodatkowego elektronicznego bloku programowania zmian temperatury w czasie. Mozliwosc róznorodnego doboru materialów i zmian ksztaltu elementów kriostatu zapewnia swobodny wybór optymalnych parametrów eksploatacyjnych urzadzenia w szerokim zakresie.Objasnienie rysunku. Wynalazek w przykladzie wykonania uwidoczniono na rysunku przedstawiajacym kriostat w przekroju podluznymi, Przyklad wykonania wynalazku. Wkladka wykonana z miedzi sklada sie z dwóch czesci 1 i 2, polaczonych ze soba elementem 3 wykonanym ze stopu Wooda. Gwint 4 umozliwia zmiane odleglosci pomiedzy czesciami 1 i 2 wkladki miedzianej. W czesci górnej 1 znajduje sie przestrzen robocza 5 zamykana korkiem 6, w której umieszcza sie badana próbke.2 97 302 Dla okreslenia zaleznosci temperatury w,pf*estrzenl roboczej 5 od odleglosci pomiedzy czesciami 1 i 2 przeprowadza sie cechowanie kriostatu przy pomocy termopary, Jednoczesnie okresla sie szybkosc spadku temperatury w okresie poczatkowym. Nastepnie w celu osiagniecia zadane) temperatury próbki reguluje sie gwintem 4 odleglosc pomiedzy czesciami 1 I 2 wkladki miedzianej. Kriostat wraz z próbka umieszcza sie w naczyniu De wara a czesc dolna 2 wkladki miedzianej zanurza sie w czynniku chlodzacym. Spadek temperatur w czesciach 1 i 2 jest niewielki, natomiast gwaltowny spadek temperatury nastepuje w elemencie 3 wykonanym ze stopu Wooda, który charakteryzuje sie niskim wspólczynnikiem przewodnictwa cieplnego, PLThe subject of the invention is an intermediate temperature cryostat which is used especially for small samples in solid state physics and chemistry. The known state of the art. Conventional cryostats normally contain electronic control systems which, based on the indicated thermocouples, control the actuator that changes the heat supply. These are devices with an extensive structure and a complex control system. In laboratory practice, copper inserts are sometimes used, the ends of which are immersed in a cooling medium, e.g. in liquid nitrogen. Such an insert allows to achieve a temperature of about 10-15 ° higher than the temperature of the cooling agent. Summary of the invention. In the cryostat according to the invention, the insert made of a material with good thermal conductivity consists of two parts, between which the said element of material with a bad thermal conductivity is placed. Both parts of the insert made of a material with a good thermal conductivity are connected to an element made of a material with a bad thermal conductivity in a removable manner enabling the thickness of this layer to be changed. Advantageous technical effects of the invention. The cryostat according to the invention significantly extends the range of applicability of typical mass-produced dewar vessels. Due to its simple construction, the cryostat is highly reliable and stable in operation. The initial period of establishing the operating conditions of the cryostat can be used for the operation in the regime of regulated rise or fall of temperature, which in conventional cryostats requires an additional electronic block for programming temperature changes over time. The possibility of a variety of materials and changes in the shape of the cryostat elements ensures a free choice of optimal operating parameters of the device in a wide range. The invention is illustrated in an exemplary embodiment by a drawing showing a cryostat in longitudinal section, Embodiment of the invention. The insert made of copper consists of two parts 1 and 2, connected with each other by an element 3 made of a Wood alloy. The thread 4 makes it possible to vary the distances between parts 1 and 2 of the copper insert. In the upper part 1 there is a working space 5 closed with a plug 6, in which the tested sample is placed. 2 97 302 To determine the temperature dependence w, pf * ester 5 on the distance between parts 1 and 2, the cryostat is calibrated with a thermocouple. the rate of temperature drop in the initial period is determined. Then, in order to achieve the desired sample temperature, the distance between the parts 1 and 2 of the copper insert is adjusted with the thread 4. The cryostat and the sample are placed in the De wara vessel and the lower part of the 2 copper insert is immersed in the coolant. The temperature drop in parts 1 and 2 is small, while a sharp drop in temperature occurs in element 3 made of Wood's alloy, which has a low thermal conductivity coefficient, PL

Claims (1)

1. Zastrzezenie patentowe Kriostat dla temperatur posrednich, w którym wkladka wykonana z materialu o dobrym przewodnictwie cieplnym zanurzona jest czesciowo w czynniku chlodzacym, znamienny tym, ze wkladka sklada sie z dwóch czesci (1 i 2), pomiedzy którymi umieszczony jest wymienny element (3) wykonany z materialu o zlym przewodnictwie cieplnym przy czym obie czesci (1, 2) wkladki polaczone sa z elementem (3) w sposób rozlaczny umozliwiajacy regulacje odleglosci pomiedzy czesciami (1 i,2) wkladki. Prac. Poligraf. UP PRL naklad 120+18 Cena 45 zl PL1. Claim Cryostat for intermediate temperatures, in which the insert made of a material with good thermal conductivity is partially immersed in a coolant, characterized in that the insert consists of two parts (1 and 2), between which a replaceable element (3 ) made of a material with bad thermal conductivity, whereby both parts (1, 2) of the insert are connected to the element (3) in a separable way, enabling the adjustment of the distance between the parts (1 and 2) of the insert. Wash. Typographer. UP PRL, circulation 120 + 18 Price PLN 45 PL
PL18463875A 1975-11-11 1975-11-11 CRYSTATE FOR INTERMEDIATE TEMPERATURES PL97302B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL18463875A PL97302B1 (en) 1975-11-11 1975-11-11 CRYSTATE FOR INTERMEDIATE TEMPERATURES

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL18463875A PL97302B1 (en) 1975-11-11 1975-11-11 CRYSTATE FOR INTERMEDIATE TEMPERATURES

Publications (1)

Publication Number Publication Date
PL97302B1 true PL97302B1 (en) 1978-02-28

Family

ID=19974210

Family Applications (1)

Application Number Title Priority Date Filing Date
PL18463875A PL97302B1 (en) 1975-11-11 1975-11-11 CRYSTATE FOR INTERMEDIATE TEMPERATURES

Country Status (1)

Country Link
PL (1) PL97302B1 (en)

Similar Documents

Publication Publication Date Title
US5005985A (en) Method of determining thermal coefficient of materials
Magrini et al. On the influence of the thickness and thermal properties of heating walls on the heat transfer coefficients in nucleate pool boiling
Bald The relative efficiency of cryogenic fluids used in the rapid quench cooling of biological samples
Hallman Experimental Study of Combined Forced and Free-laminar Convection in a Vertical Tube
US2588355A (en) Method and apparatus for measuring dew point
Wunderlich et al. A study of transition temperature standards by DTA
Nagendra et al. Free convection heat transfer from vertical cylinders and wires
Braga et al. Effect of density extremum on the solidification of water on a vertical wall of a rectangular cavity
PL97302B1 (en) CRYSTATE FOR INTERMEDIATE TEMPERATURES
DE3034667C2 (en)
Müller-Steinhagen et al. Effect of dissolved gases on subcooled flow boiling heat transfer
Omaraa et al. Modified T-history method for measuring thermophysical properties of phase change materials at high temperature
Khvostantsev et al. Kinetic properties and phase transitions in Sb2Te3 under hydrostatic pressure up to 9 GPa
Mishra et al. Experimental lumped analysis of different solid geometries
Sugawara et al. Experimental studies on the melting of a horizontal ice layer
Sagert et al. Thermal diffusion of ammonium salts in aqueous solution
Findlay et al. Temperature measurements of a graphite furnace used in flameless atomic absorption
Jensen et al. A thermal investigation of some inorganic salts
NEVINS JR The cooling power of an impinging jet
Harrison Magnetic properties of the magnetite-spinel solid solution
SU819652A1 (en) Method of investigation of crystal optical properties
US3257840A (en) Apparatus for comparative determination of thermal conductivity
Woodall The direct measurement of the Peltier coefficient
Kamotani et al. Effect of cold wall temperature on onset of oscillatory thermocapillary flow
Lezak et al. Light induced cooling of a heated solid immersed in liquid helium I