PL85397B1 - - Google Patents
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- Publication number
- PL85397B1 PL85397B1 PL16454273A PL16454273A PL85397B1 PL 85397 B1 PL85397 B1 PL 85397B1 PL 16454273 A PL16454273 A PL 16454273A PL 16454273 A PL16454273 A PL 16454273A PL 85397 B1 PL85397 B1 PL 85397B1
- Authority
- PL
- Poland
- Prior art keywords
- weight
- sie
- kwasu
- alfa
- octowego
- Prior art date
Links
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 claims 8
- 238000000034 method Methods 0.000 claims 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims 2
- IGODOXYLBBXFDW-UHFFFAOYSA-N alpha-Terpinyl acetate Chemical compound CC(=O)OC(C)(C)C1CCC(C)=CC1 IGODOXYLBBXFDW-UHFFFAOYSA-N 0.000 claims 2
- 239000003054 catalyst Substances 0.000 claims 2
- VLTRZXGMWDSKGL-UHFFFAOYSA-N perchloric acid Chemical compound OCl(=O)(=O)=O VLTRZXGMWDSKGL-UHFFFAOYSA-N 0.000 claims 2
- WUOACPNHFRMFPN-VIFPVBQESA-N (R)-(+)-alpha-terpineol Chemical compound CC1=CC[C@H](C(C)(C)O)CC1 WUOACPNHFRMFPN-VIFPVBQESA-N 0.000 claims 1
- WUOACPNHFRMFPN-UHFFFAOYSA-N alpha-terpineol Chemical compound CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 claims 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims 1
- SQIFACVGCPWBQZ-UHFFFAOYSA-N delta-terpineol Natural products CC(C)(O)C1CCC(=C)CC1 SQIFACVGCPWBQZ-UHFFFAOYSA-N 0.000 claims 1
- 230000032050 esterification Effects 0.000 claims 1
- 238000005886 esterification reaction Methods 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 239000000758 substrate Substances 0.000 claims 1
- 229940116411 terpineol Drugs 0.000 claims 1
- 125000001309 chloro group Chemical group Cl* 0.000 description 3
- 125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 description 2
- WTARULDDTDQWMU-UHFFFAOYSA-N Pseudopinene Natural products C1C2C(C)(C)C1CCC2=C WTARULDDTDQWMU-UHFFFAOYSA-N 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 1
- XRGPFNGLRSIPSA-UHFFFAOYSA-N butyn-2-one Chemical group CC(=O)C#C XRGPFNGLRSIPSA-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Claims (3)
1. Sposób wytwarzania octanu terpinylu w rea¬ kcji estryfikacji alfa terpinolu bezwodnikiem kwa- 25 su octowego, znamienny tym, ze proces prowadzi sie w temperaturze 20—32°C w obecnosci katali¬ zatora spreparowanego przez zmieszanie w tempe¬ raturze pokojowej w ciagu 20—24 godzin 1 czesci wagowej kwasu nadchlorowego, 10 czesci wago- 30 wych kwasu fosforowego i 90 czesci wagowych bezwodnika kwasu octowego.
2. Sposób wedlug zastrzezenia 1, znamienny tym, ze katalizator uzywa sie w ilosci 5—10% wago¬ wych korzystnie 5—7% wagowych w stosunku do 35 wagi substratów terpineolu i bezwodnika kwasu octowego zmieszanych w stosunku molowym 1:1,1 do 1:1,
3. Cena 10 zl FIZG Koszalin D-MC9 Naklad: IlLO egz.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL16454273A PL85397B1 (pl) | 1973-08-07 | 1973-08-07 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL16454273A PL85397B1 (pl) | 1973-08-07 | 1973-08-07 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL85397B1 true PL85397B1 (pl) | 1976-04-30 |
Family
ID=19963731
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL16454273A PL85397B1 (pl) | 1973-08-07 | 1973-08-07 |
Country Status (1)
| Country | Link |
|---|---|
| PL (1) | PL85397B1 (pl) |
-
1973
- 1973-08-07 PL PL16454273A patent/PL85397B1/zh unknown
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