PL8495B1 - The method of obtaining hydrocarbon oils from carbon. - Google Patents

The method of obtaining hydrocarbon oils from carbon. Download PDF

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Publication number
PL8495B1
PL8495B1 PL8495A PL849527A PL8495B1 PL 8495 B1 PL8495 B1 PL 8495B1 PL 8495 A PL8495 A PL 8495A PL 849527 A PL849527 A PL 849527A PL 8495 B1 PL8495 B1 PL 8495B1
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PL
Poland
Prior art keywords
gases
distillation furnace
vapors
fact
carrying
Prior art date
Application number
PL8495A
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Polish (pl)
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Publication date
Application filed filed Critical
Publication of PL8495B1 publication Critical patent/PL8495B1/en

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Description

Bezposrednie uwodornianie weglowodo¬ rów jest mozliwe pod wysokiem cisnieniem i w wysokich temperaturach, co wymaga kosztownych i uciazliwych urzadzen; prócz tego taka przeróbka wegla wymaga uprzed¬ niego jego przygotowania, które jest rów¬ niez kosztowne.Sposób wedlug wynalazku nie wymaga, stosowania drogich urzadzen i polega na tern, ze wegiel doprowadza sie do jednego ze znanych urzadzen do suchej destylacji, zas gazy, uchodzace z pieca destylacyjne¬ go, przetwarza sie bezposrednio na oleje weglowodorowe, zamiast przerabiac je, jak zwykle, na smole. Poniewaz gaz wyde¬ stylowany zawiera równiez i -skladniki, opózniajace, a nawet uniemozliwiajace tworzenie sie olejów weglowodorowych, korzystnie jest w znany sposób usunac pewne skladniki z mieszaniny gazów i par jeszcze przed ich przeróbka na oleje. Do takich skladników szkodliwych naleza np. zwiazki siarkowe, powodujace zatrucie katalizatorów, Z drugiej strony w niektó¬ rych wypadkach korzystnie jest do miesza¬ niny par i gazów dodawac pewnych sub- stancyj. Do takich subsiancyj naleza prze- dewszystkiem gazy, ulatwiajace przemia¬ ne, a wiec: tlenek wegla i wodór, gaz wod¬ ny, albo przegrzana para wodna. Dodawa¬ nie tych substancyj odbywa sie w samym piecu destylacyjnym. Do wytwarzania ga¬ zu wodnego najlepiej jest stonowac koks, pozostaly po destylacji. Generator ga- zu wodnego moze byc w tym wypadku urzadzony bezposrednio pod piecem desty-lacyjnym tak, zeby cieplo wypadajacego koksu mozna bylo uzytkowac do wytwarza¬ nia gazu wodnego. Mozna równiez genera¬ tor gazu wodnego zbudowac lacznie z pie¬ cem destylacyjnym jako osobna jed¬ nostke.Niezbedne w wielu wypadkach kataliza¬ tory, jak cynk, cyna, nikiel i t. d. mozna dodawac w postaci pary lub pylu do mie¬ szaniny par i gazów przed jej wprowadze¬ niem do przestrzeni reakcyjnej albo do¬ piero w tej przestrzeni. Urzadzenie, w kió- rem odbywa sie nastepnie przeróbka mie¬ szaniny par i gazów na olleje weglowodo¬ rowe, dobrze jest budowac jako jedna ca¬ losc z piecem destylacyjnym albo k umieszczac je bezposrednio w jego pobli: PL PLDirect hydrogenation of the hydrocarbons is possible at high pressures and temperatures, requiring expensive and cumbersome equipment; moreover, such processing of coal requires prior preparation, which is also costly. The method according to the invention does not require the use of expensive equipment and consists in the fact that the coal is fed to one of the known dry distillation devices, and to gases escaping from the distillation furnace, they are converted directly into hydrocarbon oils, instead of being converted into tar as usual. Since the distilled gas also contains components which retard or even prevent the formation of hydrocarbon oils, it is advantageous in the known manner to remove certain components from the gas-vapor mixture before they are converted into oils. Such harmful components include, for example, sulfur compounds which poison the catalysts. On the other hand, in some cases it is advantageous to add certain substances to the mixture of vapors and gases. Such subsidies include, first of all, gases that facilitate the transformation, ie: carbon monoxide and hydrogen, water gas, or superheated steam. The addition of these substances takes place in the distillation furnace itself. For the production of water gas, it is best to soften the coke left over from distillation. The water gas generator can in this case be arranged immediately below the distillation furnace so that the heat of the falling out coke can be used to generate water gas. The water gas generator can also be built as a separate unit with the distillation furnace. Catalysts necessary in many cases, such as zinc, tin, nickel, etc., can be added as steam or dust to the vapor-gas mixture before it is introduced into the reaction space, or only there. The device, in a cell, then transforms the mixture of vapors and gases into hydrocarbon oils, it is good to build it as one whole with the distillation furnace or place it directly next to it: PL PL

Claims (10)

1. Zastrzezenia patentowe. 1. Sposób otrzymywania olejów we¬ glowodorowych z wegla, znamienny tern, ze gazy lub pary, wychodzace z pieca do suchej destylacji, wprowadza sie zamiast do chlodnika do urzadzenia uwodorniaja¬ cego.1. Patent claims. 1. A process for the preparation of hydrocarbon oils from coal, characterized by the fact that the gases or vapors coming from the dry distillation furnace are fed to a hydrogenation device instead of a cooler. 2. Sposób wedlug zastrz. 1, znamien¬ ny tern, ze skladniki mieszaniny gazowej, niepozadane w procesie uwodorniajacym, jak np. zwiazki siarki, usuwa sie przed wprowadzeniem mieszaniny do tego urza¬ dzenia.2. The method according to claim According to claim 1, it is characterized by the fact that the components of the gaseous mixture which are not required in the hydrogenation process, such as, for example, sulfur compounds, are removed before the mixture is introduced into the device. 3. Sposób wedlug zastrz. 1, znamien¬ ny tern, ze do gazów i par wydestylowa- nych dodaje sie inne gazy, jak np. wodór, tlenek wegla, gaz wodny, albo przegrzana pare wodna.3. The method according to p. The method of claim 1, characterized by the addition of other gases, such as, for example, hydrogen, carbon monoxide, water gas or superheated water vapor to the distilled gases and vapors. 4. Sposób wedlug zastrz. 1 i 3, zna¬ mienny tern, ze dodatkowe gazy albo pary doprowadza sie wprost do pieca destyla¬ cyjnego.4. The method according to p. 1 and 3, the significant point is that additional gases or vapors are fed directly to the distillation furnace. 5. Sposób wedlug zastrz. 1 — 4, zna¬ mienny tern, ze do wytwarzania gazu wod¬ nego stosuje sie koks, pozostaly po desty¬ lacji.5. The method according to p. 1-4, the example is that the coke remaining after distillation is used to produce the water gas. 6. Sposób wedlug zastrz 1 i 2, znar- mfenny tern, ze do mieszaniny gazów i par przed jej wprowadzeniem do przestrzeni reakcyjnej, albo dopiero w tej przestrzeni dodaje sie katalizatory w postaci pary lub pylu.6. The method according to claims 1 and 2, characterized by the fact that steam or dust catalysts are added to the mixture of gases and vapors before it is introduced into the reaction space, or only in this space. 7. Urzadzenie do wykonania sposobu wedlug zastrz. 5, znamienne tern, ze gene¬ rator gazu wodnego stanowi jedna calosc z piecem destylacyjnym.Device for carrying out the method according to claim 5. The apparatus of claim 5, wherein the water gas generator is integral with the distillation furnace. 8. Urzadzenie do wykonania sposobu wedlug zastrz. 5, znamienne tern, ze gene¬ rator gazu wodnego urzadzony jest bez¬ posrednio pod piecem destylacyjnym.Device for carrying out the method according to claim 5. A method as claimed in claim 5, characterized in that the water gas generator is arranged directly below the distillation furnace. 9. Urzadzenie do wykonania sposobu wedlug zastrz. 1 — 6, znamienne tern, ze urzadzenie, w którem sie odbywa dalsza przeróbka gazu wydestylowanego, stanowi czesc pieca destylacyjnego i jest zbudowa¬ ne, jako jedna calosc z piecem.Device for carrying out the method according to claim According to any of the claims 1-6, characterized by the fact that the plant in which the distilled gas is further processed is part of the distillation furnace and is built in one piece with the furnace. 10. Urzadzenie do wykonania sposobu wedlug zastrz. 1 — 6, znamienne tern, ze urzadzenie, sluzace do dalszej przeróbki gazu wydestylowanego, umieszczone jest bezposrednio wpoblizu pieca destylacyj¬ nego. Joseph Trautmann. Zastepca: M. Brokman. rzecznik patentowy. Druk L. Boguslawskiego, Warszawa*. PL PLDevice for carrying out the method according to claim 1 - 6, characterized in that the device for the further processing of the distilled gas is located directly adjacent to the distillation furnace. Joseph Trautmann. Deputy: M. Brokman. Patent Attorney. Print by L. Boguslawski, Warsaw *. PL PL
PL8495A 1927-05-06 The method of obtaining hydrocarbon oils from carbon. PL8495B1 (en)

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PL8495B1 true PL8495B1 (en) 1928-03-31

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