PL66661B1 - - Google Patents
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- Publication number
- PL66661B1 PL66661B1 PL135937A PL13593769A PL66661B1 PL 66661 B1 PL66661 B1 PL 66661B1 PL 135937 A PL135937 A PL 135937A PL 13593769 A PL13593769 A PL 13593769A PL 66661 B1 PL66661 B1 PL 66661B1
- Authority
- PL
- Poland
- Prior art keywords
- methyl
- aniline
- iodine
- mercaptophenothiazine
- methylmercaptophenyl
- Prior art date
Links
- 238000006243 chemical reaction Methods 0.000 claims description 8
- IJGRMHOSHXDMSA-UHFFFAOYSA-N nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 8
- NGTRZJDYCCOXBA-UHFFFAOYSA-N 3-methylsulfanyl-N-phenylaniline Chemical compound CSC1=CC=CC(NC=2C=CC=CC=2)=C1 NGTRZJDYCCOXBA-UHFFFAOYSA-N 0.000 claims description 7
- NINIDFKCEFEMDL-UHFFFAOYSA-N sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 6
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 claims description 5
- 229910052740 iodine Inorganic materials 0.000 claims description 5
- 239000011630 iodine Substances 0.000 claims description 5
- YOAFILPTKZIYAB-UHFFFAOYSA-N CC=1C=C(C=2NC3=CC=CC=C3SC2C1)S Chemical compound CC=1C=C(C=2NC3=CC=CC=C3SC2C1)S YOAFILPTKZIYAB-UHFFFAOYSA-N 0.000 claims description 4
- RWSOTUBLDIXVET-UHFFFAOYSA-N dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims description 4
- 229910052757 nitrogen Inorganic materials 0.000 claims description 4
- 239000011261 inert gas Substances 0.000 claims description 3
- -1 m-methyl mercaptophenyl Chemical group 0.000 claims description 3
- 238000002844 melting Methods 0.000 claims description 3
- 239000011874 heated mixture Substances 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims description 2
- 229910052717 sulfur Inorganic materials 0.000 claims description 2
- 239000011593 sulfur Substances 0.000 claims description 2
- JZROAVSLDUAQEI-UHFFFAOYSA-N C1=CC=C2SC3=CC(SC)=CC=C3NC2=C1 Chemical compound C1=CC=C2SC3=CC(SC)=CC=C3NC2=C1 JZROAVSLDUAQEI-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 3
- MVPPADPHJFYWMZ-UHFFFAOYSA-N Chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000000155 melt Substances 0.000 description 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 150000002990 phenothiazines Chemical class 0.000 description 2
- 239000004698 Polyethylene (PE) Substances 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 230000000111 anti-oxidant Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000012267 brine Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000005712 crystallization Effects 0.000 description 1
- 238000005755 formation reaction Methods 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000019796 monopotassium phosphate Nutrition 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL66661B1 true PL66661B1 (de) | 1972-08-31 |
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