PL48933B1 - - Google Patents

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Publication number
PL48933B1
PL48933B1 PL101736A PL10173663A PL48933B1 PL 48933 B1 PL48933 B1 PL 48933B1 PL 101736 A PL101736 A PL 101736A PL 10173663 A PL10173663 A PL 10173663A PL 48933 B1 PL48933 B1 PL 48933B1
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PL
Poland
Prior art keywords
latex
water
edges
air
blow
Prior art date
Application number
PL101736A
Other languages
Polish (pl)
Inventor
inz. Jerzy Wojciechowski mgr
inz. Zbig¬niew Grortel mgr
Kopytko Józef
Original Assignee
Instytut Ciezkiej Syntezy Organicznej
Filing date
Publication date
Application filed by Instytut Ciezkiej Syntezy Organicznej filed Critical Instytut Ciezkiej Syntezy Organicznej
Publication of PL48933B1 publication Critical patent/PL48933B1/pl

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Description

Strumien po- 48933I 48933 3 4 Wietrza powoduje ruch obrotowy zageszczanego lateksu i stale odnawianie jego powierzchni. Stru¬ mien powietrza powoduje zarazem stale odprowa¬ dzanie pary wodnej, przyspieszajac proces zagesz¬ czania. Krawedzie styku lateksu ze scianami apa¬ ratu chronione sa oslonami przed dzialaniem pro¬ mieni. Krawedzie przelewowe 4 dla odplywu la¬ teksu zageszczonego sa dodatkowo chlodzone woda.Powyzsze zabezpieczenia powoduja, ze tempera¬ tura w zadnym punkcie nie jest wyzsza od tem¬ peratury lateksu.Proces zatezania lateksu nastepuje w otwartym zbiorniku 3. Odplywowe ksztalty aparatu zabezpie¬ czaja równomierny i spokojny przeplyw lateksu.Unika sie przez to pienienia i lokalnych róznic w konsystencji (lepkosci) lateksu w calym apara¬ cie. Dzieki temu ograniczono do minimum mozli¬ wosc koagulacji oraz zapewniono równomiernie od¬ parowanie wody w calej masie.Proces zageszczania w urzadzeniu wedlug wy¬ nalazku mozna prowadzic periodycznie, lub metoda ciagla. W metodzie ciaglej do dolnej czesci aparatu doplywa staly strumien lateksu surowego, a góra przez chlodzona i oslonieta od dzialania zródla promieni podczerwonych krawedz przelewowa od¬ plywa lateks zageszczony. W metodzie ciaglej pro¬ ces mozna prowadzic w jednym aparacie lub le¬ piej jest ustawic kaskadowo dwa lub wiecej apa¬ ratów i zageszczanie prowadzic strefami.Przyklad 1. Zageszczanie metoda perio¬ dyczna.Do aparatu jak na rysunku wlano 50 1 lateksu kauczuku syntetycznego o stezeniu 30% suchej ma¬ sy. Podstawowe wymiary aparatu: powierzchnia parowania (swobodna powierzchnia cieczy) 0,6 m2, pojemnosc calkowita aparatu 55 1 lateksu. Zródlo promieni podczerwonych — promienniki gazowe.Temperatura zageszczania od 30°C do 40°C. Na powierzchnie lustra cieczy skierowano strumien powietrza o natezeniu 50 m3/godz. Powietrze wy¬ plywa z dysz pod katem 60° w stosunku do po¬ wierzchni cieczy. Calkowity czas odparowania od 30% suchej masy do 60% suchej masy w lateksie wynosil 10—12 godz. Zuzycie gazu koksowniczego . (wartosc opalowa 4100 kcal/Nm3) 1,0 Nm3/kg od- 5 parowanej wody. Zuzycie powietrza sprezonego 25 Nm3/kg odparowanej wody.Przyklad 2. Zageszczanie metoda ciagla.Do aparatu jak w przykladzie 1 podawano od dolu w sposób ciagly okolo 7,0 1/godz. lateksu z kauczuku syntetycznego o stezeniu okolo 30% suchej masy. Lateks zageszczony o stezeniu okolo 60% suchej masy odprowadzano w sposób ciagly przelewem. Ogrzewanie gazowymi promiennikami podczerwieni i przeplyw powietrza jak w przy¬ kladzie 1.Temperatura zageszczania (mierzona w lateksie) wynosila 40°C. Wydajnosc aparatu wynosi 3,5 1/godz, lateksu zageszczonego (60%). Sprawnosc za¬ geszczania charakteryzuje sie nastepujacymi para¬ metrami : Zuzycie gazu koksowniczego (wartosc opalowa 4100 kcal/Nm3) 1,2 Nm3/kg odparowanej wody, zu¬ zycie powietrza sprezonego 20 Nm3/kg odparowanej wody. PLThe air jet 48933I 48933 3 4 The wind causes the compacted latex to rotate and its surface is constantly renewed. At the same time, the air stream causes a constant discharge of water vapor, accelerating the concentration process. The edges of the contact of latex with the walls of the apparatus are protected against the action of rays. The overflow edges 4 for the concentrated latex outflow are additionally cooled with water. The above-mentioned protections ensure that the temperature at no point is higher than the latex temperature. The latex concentration process takes place in an open reservoir 3. The outflow shape of the apparatus ensures an even smooth latex flow. This avoids foaming and local variations in the consistency (viscosity) of the latex throughout the appliance. As a result, the possibility of coagulation is minimized and the water is evenly evaporated throughout the mass. The concentration process in the device according to the invention can be carried out periodically or continuously. In the method, a constant stream of raw latex flows continuously to the bottom of the apparatus, and the top through the cooled and protected from the infrared light source, the overflow edge flows out of the thickened latex. In the continuous method, the process can be carried out in one apparatus, or it is better to cascade two or more apparatuses and conduct the compaction by zones. Example 1. Compaction method periodical. The apparatus as shown in the figure is filled with 50 liters of synthetic rubber latex by 30% dry weight. Basic dimensions of the apparatus: evaporation area (free liquid surface) 0.6 m2, total capacity of the apparatus 55 1 latex. Source of infrared rays - gas radiators. Thickening temperature from 30 ° C to 40 ° C. An air stream of 50 m3 / h was directed at the surface of the liquid. The air exits the nozzles at an angle of 60 ° with respect to the surface of the liquid. The total evaporation time from 30% dry weight to 60% dry weight in latex was 10-12 hours. Coke oven gas consumption. (opal value 4100 kcal / Nm3) 1.0 Nm3 / kg of evaporated water. Compressed air consumption 25 Nm3 / kg of evaporated water. Example 2. Compaction continuous method. The apparatus as in example 1 was continuously fed from below about 7.0 l / h. synthetic rubber latex with a concentration of approximately 30% dry weight. The thickened latex with a concentration of about 60% dry matter was continuously removed via the overflow. Infrared gas heating and air flow as in Example 1. The thickening temperature (measured in latex) was 40 ° C. The efficiency of the apparatus is 3.5 l / h, thickened latex (60%). The compaction efficiency is characterized by the following parameters: Coke oven gas consumption (heating value 4100 kcal / Nm3) 1.2 Nm3 / kg of evaporated water, compressed air consumption 20 Nm3 / kg of evaporated water. PL

Claims (1)

1. Zastrzezenie patentowe Urzadzenie do zageszczania lateksu przez odpa¬ rowanie wody, znamienne tym, ze sklada sie z otwartego zbiornika (3), którego krawedzie chro¬ nione" sa przed nagrzewaniem oslonami, a krawe¬ dzie przelewowe (4) dla odplywu lateksu zagesz¬ czonego sa dodatkowo chlodzone woda, umieszczo¬ nych nad zbiornikiem promienników podczerwieni (I) sluzacych do bezprzeponowego nagrzewania la¬ teksu, oraz rozmieszczonych promieniscie nad po¬ wierzchnia lateksu rur (2) dla nadmuchu powie¬ trza w celu wprawienia lateksu w ruch obrotowy, które posiadaja otwory umozliwiajace nadmuch po¬ wietrza pod katem ostrym do powierzchni la¬ teksu. 15 20 25 30 35 4048933 Lateks roej^iuony FigZ PL1. Patent claim Device for thickening the latex by evaporating water, characterized in that it consists of an open tank (3), the edges of which are protected against heating by shields, and the overflow edges (4) for the latex outflow are concentrated The connection is additionally cooled with water, placed above the tank of infrared radiators (I) for the direct heating of latex, and pipes (2) arranged radially above the surface of the latex to blow air in order to make the latex rotate, which have openings allowing air to blow at an acute angle to the latex surface. 15 20 25 30 35 4048933 Latex foam FigZ PL
PL101736A 1963-05-29 PL48933B1 (en)

Publications (1)

Publication Number Publication Date
PL48933B1 true PL48933B1 (en) 1964-12-15

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