PL446802A1 - Method of producing self-regenerating polymer monomers - Google Patents

Method of producing self-regenerating polymer monomers

Info

Publication number
PL446802A1
PL446802A1 PL446802A PL44680223A PL446802A1 PL 446802 A1 PL446802 A1 PL 446802A1 PL 446802 A PL446802 A PL 446802A PL 44680223 A PL44680223 A PL 44680223A PL 446802 A1 PL446802 A1 PL 446802A1
Authority
PL
Poland
Prior art keywords
formula
producing self
polymer monomers
axaca
reacted
Prior art date
Application number
PL446802A
Other languages
Polish (pl)
Inventor
Bożena Tyliszczak
Magdalena Bańkosz
Agnieszka Sobczak-Kupiec
Jolanta JAŚKOWSKA
Agnieszka Tomala
Original Assignee
Politechnika Krakowska im. Tadeusza Kościuszki
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Krakowska im. Tadeusza Kościuszki filed Critical Politechnika Krakowska im. Tadeusza Kościuszki
Priority to PL446802A priority Critical patent/PL446802A1/en
Publication of PL446802A1 publication Critical patent/PL446802A1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00—Carboxylic acid amides
    • C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/45—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups
    • C07C233/46—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom
    • C07C233/49—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by carboxyl groups with the substituted hydrocarbon radical bound to the nitrogen atom of the carboxamide group by an acyclic carbon atom having the carbon atom of the carboxamide group bound to a carbon atom of an acyclic unsaturated carbon skeleton

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Przedmiotem wynalazku jest sposób otrzymywania monomerów z grupy AxACA, w szczególności A2ACA o wzorze VI, A6ACA o wzorze VII, A8ACA o wzorze VIII oraz A12ACA o wzorze IX, w dwuetapowej reakcji. W pierwszym etapie przeprowadza się reakcję kwasu akrylowego o wzorze I z chloromrówczanem etylu o wzorze II w wyniku czego powstaje odpowiedni bezwodnik mieszany o wzorze III, który w kolejnym etapie poddaje się reakcji z kwasem x- aminokarboksylowym o wzorze IV prowadząc do otrzymania kwasu N-akryloilo-x-aminokarboksylowego (AxACA) o wzorze V.The subject of the invention is a method for obtaining monomers from the AxACA group, in particular A2ACA of formula VI, A6ACA of formula VII, A8ACA of formula VIII and A12ACA of formula IX, in a two-stage reaction. In the first stage, acrylic acid of formula I is reacted with ethyl chloroformate of formula II, resulting in the formation of the corresponding mixed anhydride of formula III, which is then reacted with x-aminocarboxylic acid of formula IV to obtain N-acryloyl-x-aminocarboxylic acid (AxACA) of formula V.

PL446802A 2023-11-22 2023-11-22 Method of producing self-regenerating polymer monomers PL446802A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL446802A PL446802A1 (en) 2023-11-22 2023-11-22 Method of producing self-regenerating polymer monomers

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL446802A PL446802A1 (en) 2023-11-22 2023-11-22 Method of producing self-regenerating polymer monomers

Publications (1)

Publication Number Publication Date
PL446802A1 true PL446802A1 (en) 2025-05-26

Family

ID=95821498

Family Applications (1)

Application Number Title Priority Date Filing Date
PL446802A PL446802A1 (en) 2023-11-22 2023-11-22 Method of producing self-regenerating polymer monomers

Country Status (1)

Country Link
PL (1) PL446802A1 (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5369142A (en) * 1993-01-15 1994-11-29 The Ohio State University Water soluble polymers containing amino acid residues for dental restoratives
EP1503717A1 (en) * 2002-01-23 2005-02-09 The UAB Research Foundation Glass-ionomer cements containing amino acids

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5369142A (en) * 1993-01-15 1994-11-29 The Ohio State University Water soluble polymers containing amino acid residues for dental restoratives
EP1503717A1 (en) * 2002-01-23 2005-02-09 The UAB Research Foundation Glass-ionomer cements containing amino acids

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
GOOGLE; Bialik-Wąs K, Tyliszczak B, Walczyk D, Jaśkowska J and Sobczak-Kupiec A (2016). Physicochemical properties of hydrogel matrices based on N - acryloyl aminocapronic acid (A6ACA) stabilized with guar gum. Front. Bioeng. Biotechnol. Conference Abstract: 10th World Biomaterials Congress. doi: 10.3389/conf.FBIOE.2016.01.00637 *

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