PL427144A1 - Method for obtaining hybrid carbon materials containing oligoheterocyclic compounds - Google Patents
Method for obtaining hybrid carbon materials containing oligoheterocyclic compoundsInfo
- Publication number
- PL427144A1 PL427144A1 PL427144A PL42714418A PL427144A1 PL 427144 A1 PL427144 A1 PL 427144A1 PL 427144 A PL427144 A PL 427144A PL 42714418 A PL42714418 A PL 42714418A PL 427144 A1 PL427144 A1 PL 427144A1
- Authority
- PL
- Poland
- Prior art keywords
- oligoheterocyclic
- compounds
- hours
- carbon materials
- hybrid carbon
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 5
- 150000001875 compounds Chemical class 0.000 title abstract 3
- 239000003575 carbonaceous material Substances 0.000 title abstract 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 abstract 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 2
- 229910002804 graphite Inorganic materials 0.000 abstract 2
- 239000010439 graphite Substances 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 238000000197 pyrolysis Methods 0.000 abstract 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 abstract 1
- 229910000019 calcium carbonate Inorganic materials 0.000 abstract 1
- 239000012153 distilled water Substances 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 239000011261 inert gas Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 150000007522 mineralic acids Chemical class 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 229910052757 nitrogen Inorganic materials 0.000 abstract 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L sodium carbonate Substances [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 abstract 1
- 229910000029 sodium carbonate Inorganic materials 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Landscapes
- Carbon And Carbon Compounds (AREA)
Abstract
Przedmiotem zgłoszenia jest sposób wytwarzania hybrydowych materiałów węglowych z dodatkiem związków oligoheterocyklicznych (HMW-OT) poprzez pirolizę grafitu w warunkach beztlenowych. Sposób ten charakteryzuje się tym, że grafit i/lub węgle mikro-mezoporowate pochodzenia naturalnego zawierające azot poddane procesowi pirolizy znanymi sposobami miesza się z węglanem sodu lub wapnia lub wodorotlenek potasu o stężeniu korzystnie 16,9%, i tak powstałą mieszaninę homogenizuje korzystnie mechanicznie w czasie od 0,5 do 3 h i ogrzewa z szybkością z zakresu od 5°C/min do 15°C/min w atmosferze gazu obojętnego, po czym schładza się otrzymany materiał do temperatury około 50°C utrzymując atmosferę beztlenową i poddaje się działaniu mocnego kwasu nieorganicznego, tak wytrawiony kwasem materiał odmywa się wodą destylowaną do uzyskania wartości pH odcieku w zakresie od 6 do 7, po czym suszy przez okres od 12 godzin do 24 godzin w temperaturze z zakresu od 100°C do 110°C, modyfikuje roztworami związków oligoheterocyklicznych i dodaje 1-metylo-2-pirolidon i/lub aceton, korzystnie susząc w warunkach pokojowych.The subject of the application is a method for the production of hybrid carbon materials with the addition of oligoheterocyclic compounds (HMW-OT) by pyrolysis of graphite under anaerobic conditions. This method is characterized in that graphite and / or micro-mesoporous carbon of natural origin containing nitrogen subjected to the pyrolysis process are mixed with sodium or calcium carbonate or potassium hydroxide at a concentration of preferably 16.9% by known methods, and the resulting mixture preferably homogenises mechanically for 0.5 to 3 hours and heated at a rate of 5 ° C / min to 15 ° C / min under an inert gas atmosphere, then the resulting material is cooled to about 50 ° C while maintaining an anaerobic atmosphere and is subjected to strong of inorganic acid, the acid-etched material is washed with distilled water to obtain the pH of the effluent in the range of 6 to 7, and then dried for a period of 12 hours to 24 hours at a temperature in the range of 100 ° C to 110 ° C, modified with solutions of compounds oligoheterocyclic and adds 1-methyl-2-pyrrolidone and / or acetone, preferably drying at room conditions.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL427144A PL427144A1 (en) | 2018-09-20 | 2018-09-20 | Method for obtaining hybrid carbon materials containing oligoheterocyclic compounds |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL427144A PL427144A1 (en) | 2018-09-20 | 2018-09-20 | Method for obtaining hybrid carbon materials containing oligoheterocyclic compounds |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL427144A1 true PL427144A1 (en) | 2019-03-25 |
Family
ID=65799982
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL427144A PL427144A1 (en) | 2018-09-20 | 2018-09-20 | Method for obtaining hybrid carbon materials containing oligoheterocyclic compounds |
Country Status (1)
| Country | Link |
|---|---|
| PL (1) | PL427144A1 (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL417135A1 (en) * | 2016-05-09 | 2017-11-20 | Uniwersytet Mikołaja Kopernika W Toruniu | Method for producing porous carbon matrix with increased oxygen and nitrogen content |
| PL417441A1 (en) * | 2016-06-04 | 2017-12-18 | Uniwersytet Mikołaja Kopernika W Toruniu | Method for obtaining hybrid carbon-nitrogen materials with developed porous structure |
-
2018
- 2018-09-20 PL PL427144A patent/PL427144A1/en unknown
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL417135A1 (en) * | 2016-05-09 | 2017-11-20 | Uniwersytet Mikołaja Kopernika W Toruniu | Method for producing porous carbon matrix with increased oxygen and nitrogen content |
| PL417441A1 (en) * | 2016-06-04 | 2017-12-18 | Uniwersytet Mikołaja Kopernika W Toruniu | Method for obtaining hybrid carbon-nitrogen materials with developed porous structure |
Non-Patent Citations (1)
| Title |
|---|
| PIOTR KAMEDULSKI I IN.: "2018", INFLUENCE OF INTERMOLECULAR INTERACTIONS ON THE PROPERTIES OF CARBON NANOTUBES * |
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