PL424890A1 - Aluminum oxide-based composite and method for producing the aluminum oxide based composite - Google Patents

Aluminum oxide-based composite and method for producing the aluminum oxide based composite

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Publication number
PL424890A1
PL424890A1 PL424890A PL42489018A PL424890A1 PL 424890 A1 PL424890 A1 PL 424890A1 PL 424890 A PL424890 A PL 424890A PL 42489018 A PL42489018 A PL 42489018A PL 424890 A1 PL424890 A1 PL 424890A1
Authority
PL
Poland
Prior art keywords
aluminum oxide
weight
montmorillonite
based composite
producing
Prior art date
Application number
PL424890A
Other languages
Polish (pl)
Other versions
PL240100B1 (en
Inventor
Tomasz Cygan
Andrzej OLSZYNA
Jarosław WOŹNIAK
Mateusz Petrus
Marek Kostecki
Original Assignee
Politechnika Warszawska
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Warszawska filed Critical Politechnika Warszawska
Priority to PL424890A priority Critical patent/PL240100B1/en
Publication of PL424890A1 publication Critical patent/PL424890A1/en
Publication of PL240100B1 publication Critical patent/PL240100B1/en

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  • Compositions Of Oxide Ceramics (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)

Abstract

Przedmiotem zgłoszenia jest kompozyt na osnowie tlenku glinu modyfikowany montmorylonitem w ilości od 0.1% wagowych do 30% wagowych. Zgłoszenie obejmuje też sposób wytwarzania modyfikowanego kompozytu na osnowie tlenku glinu, który polega na tym, że do pojemnika młynka wprowadza się proszek tlenku glinu oraz montmorylonitu gdzie udział masowy montmorylonitu zawiera się od 0.1% wagowych do 30% wagowych, poddanego wcześniej procesowi homogenizacji w ultradźwiękach przez 10 do 60 minut w 30 do 500 ml wody i/lub alkoholu izopropylowego na 1 gram montmorylonitu, całość poddaje się procesowi mieszania w wodzie i/lub alkoholu izopropylowym przez czas od 4 do 12 godzin a następnie mieszaninę suszy się w temperaturze 30°C do 100°C oraz przesiewa przez sito o wielkości oczek 0.1 - 0.5 µm, po czym prowadzi się proces konsolidacji przy użyciu technologii spiekania SPS w próżni w następujących parametrach: temperatura spiekania od 1100°C do 1500°C, prędkość grzania i chłodzenia z zakresu 1 - 300°C/min, czas wygrzewania od 1 do 30 minut, ciśnienie z zakresu 10 – 50 MPa.The subject of the application is an aluminum oxide-based composite modified with montmorillonite in amounts ranging from 0.1% by weight to 30% by weight. The application also includes a method for producing a modified composite based on aluminum oxide, which consists in introducing aluminum oxide and montmorillonite powder into the grinder container, where the mass fraction of montmorillonite ranges from 0.1% by weight to 30% by weight, previously subjected to the ultrasonic homogenization process by 10 to 60 minutes in 30 to 500 ml of water and/or isopropyl alcohol per 1 gram of montmorillonite, the whole thing is stirred in water and/or isopropyl alcohol for 4 to 12 hours and then the mixture is dried at 30°C to 100°C and sieved through a sieve with a mesh size of 0.1 - 0.5 µm, after which the consolidation process is carried out using SPS sintering technology in a vacuum with the following parameters: sintering temperature from 1100°C to 1500°C, heating and cooling speed in the range of 1 - 300°C/min, heating time from 1 to 30 minutes, pressure in the range of 10 - 50 MPa.

PL424890A 2018-03-14 2018-03-14 Aluminum oxide-based composite and method for producing the aluminum oxide based composite PL240100B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL424890A PL240100B1 (en) 2018-03-14 2018-03-14 Aluminum oxide-based composite and method for producing the aluminum oxide based composite

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL424890A PL240100B1 (en) 2018-03-14 2018-03-14 Aluminum oxide-based composite and method for producing the aluminum oxide based composite

Publications (2)

Publication Number Publication Date
PL424890A1 true PL424890A1 (en) 2019-09-23
PL240100B1 PL240100B1 (en) 2022-02-14

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
PL424890A PL240100B1 (en) 2018-03-14 2018-03-14 Aluminum oxide-based composite and method for producing the aluminum oxide based composite

Country Status (1)

Country Link
PL (1) PL240100B1 (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4960738A (en) * 1987-11-02 1990-10-02 Kureha Chemical Industry Co., Ltd. Mullite-alumina composite sintered body and process for producing the same
DE19623425A1 (en) * 1996-06-12 1997-12-18 Dlr Deutsche Forschungsanstalt Reaction bonded mullite-based ceramic article

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4960738A (en) * 1987-11-02 1990-10-02 Kureha Chemical Industry Co., Ltd. Mullite-alumina composite sintered body and process for producing the same
DE19623425A1 (en) * 1996-06-12 1997-12-18 Dlr Deutsche Forschungsanstalt Reaction bonded mullite-based ceramic article

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
ADELE QIWANG, NANDIKAD'SOUZA, TERESA DIANEGOLDEN, CERAMIC MONTMORILLONITE NANOCOMPOSITES BY ELECTROCHEMICAL SYNTHESIS, December 2008 (2008-12-01) *

Also Published As

Publication number Publication date
PL240100B1 (en) 2022-02-14

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