PL413209A1 - Method for producing androst-1,4-dien-3-on-17-ole propionate - Google Patents

Method for producing androst-1,4-dien-3-on-17-ole propionate

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Publication number
PL413209A1
PL413209A1 PL413209A PL41320915A PL413209A1 PL 413209 A1 PL413209 A1 PL 413209A1 PL 413209 A PL413209 A PL 413209A PL 41320915 A PL41320915 A PL 41320915A PL 413209 A1 PL413209 A1 PL 413209A1
Authority
PL
Poland
Prior art keywords
androst
dien
propionate
ole
producing
Prior art date
Application number
PL413209A
Other languages
Polish (pl)
Other versions
PL228517B1 (en
Inventor
Agnieszka Rugor
Maciej Szaleniec
Tomasz Janeczko
Monika Dymarska
Edyta Kostrzewa-Susłow
Original Assignee
Uniwersytet Przyrodniczy we Wrocławiu
Instytut Katalizy I Fizykochemii Powierzchni Im. Jerzego Habera Polskiej Akademii Nauk
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Uniwersytet Przyrodniczy we Wrocławiu, Instytut Katalizy I Fizykochemii Powierzchni Im. Jerzego Habera Polskiej Akademii Nauk filed Critical Uniwersytet Przyrodniczy we Wrocławiu
Priority to PL413209A priority Critical patent/PL228517B1/en
Publication of PL413209A1 publication Critical patent/PL413209A1/en
Publication of PL228517B1 publication Critical patent/PL228517B1/en

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Abstract

Zgłoszenie dotyczy sposobu wytwarzania propionianu androst-1,4-dien-3-on-17-olu o wzorze 2. W wyniku działania preparatu enzymatycznego o aktywności AcmB uzyskanego ze szczepu bakterii Sterolibacterium denitrificans Chol-1S (DSM: 13999), następuje regioselektywna dehydrogenacja między pierwszym i drugim atomem węgla cząstki substratu o wzorze 1. Uzyskany w ten sposób produkt oczyszcza się metodą SPE z zastosowaniem polimerowych kolumienek chromatograficznych Strata-X, znanym sposobem, stosując jako eluent mieszaninę izopropanol/H2O.The application relates to a method for the production of androst-1,4-dien-3-on-17-ol propionate of formula 2. As a result of the action of the enzyme preparation with AcmB activity obtained from the bacterium strain Sterolibacterium denitrificans Chol-1S (DSM: 13999), regioselective dehydrogenation occurs between the first and second carbon atoms of the substrate particles of formula 1. The product thus obtained is purified by SPE using Strata-X polymer chromatography columns using a known method using an isopropanol / H2O mixture as eluent.

PL413209A 2015-07-21 2015-07-21 Method for producing androst-1,4-dien-3-on-17-ole propionate PL228517B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL413209A PL228517B1 (en) 2015-07-21 2015-07-21 Method for producing androst-1,4-dien-3-on-17-ole propionate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL413209A PL228517B1 (en) 2015-07-21 2015-07-21 Method for producing androst-1,4-dien-3-on-17-ole propionate

Publications (2)

Publication Number Publication Date
PL413209A1 true PL413209A1 (en) 2017-01-30
PL228517B1 PL228517B1 (en) 2018-04-30

Family

ID=57867712

Family Applications (1)

Application Number Title Priority Date Filing Date
PL413209A PL228517B1 (en) 2015-07-21 2015-07-21 Method for producing androst-1,4-dien-3-on-17-ole propionate

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PL (1) PL228517B1 (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
PL248345B1 (en) * 2022-06-29 2025-12-01 Inst Katalizy I Fizykochemii Powierzchni Im Jerzego Habera Polskiej Akademii Nauk Dehydrogenated derivative of dipterocarpol, method of its enzymatic preparation and application

Also Published As

Publication number Publication date
PL228517B1 (en) 2018-04-30

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