PL411034A1 - Alcohol-free extraction of polyphenols - Google Patents

Alcohol-free extraction of polyphenols

Info

Publication number
PL411034A1
PL411034A1 PL411034A PL41103415A PL411034A1 PL 411034 A1 PL411034 A1 PL 411034A1 PL 411034 A PL411034 A PL 411034A PL 41103415 A PL41103415 A PL 41103415A PL 411034 A1 PL411034 A1 PL 411034A1
Authority
PL
Poland
Prior art keywords
plant material
polyphenols
extract
adsorbed
alcohol
Prior art date
Application number
PL411034A
Other languages
Polish (pl)
Other versions
PL237183B1 (en
Inventor
Krzysztof Lemke
Wojciech Krzyczkowski
Alicja Oldak
Artur Wilandt
Original Assignee
Biovico Spółka Z Ograniczoną Odpowiedzialnością
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Biovico Spółka Z Ograniczoną Odpowiedzialnością filed Critical Biovico Spółka Z Ograniczoną Odpowiedzialnością
Priority to PL411034A priority Critical patent/PL237183B1/en
Priority to PCT/PL2016/000007 priority patent/WO2016118027A1/en
Publication of PL411034A1 publication Critical patent/PL411034A1/en
Publication of PL237183B1 publication Critical patent/PL237183B1/en

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/45—Ericaceae or Vacciniaceae (Heath or Blueberry family), e.g. blueberry, cranberry or bilberry
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/70—Carbohydrates; Sugars; Derivatives thereof
    • A61K31/7042—Compounds having saccharide radicals and heterocyclic rings
    • A61K31/7048—Compounds having saccharide radicals and heterocyclic rings having oxygen as a ring hetero atom, e.g. leucoglucosan, hesperidin, erythromycin, nystatin, digitoxin or digoxin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/60—Moraceae (Mulberry family), e.g. breadfruit or fig
    • A61K36/605—Morus (mulberry)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • A61K36/736—Prunus, e.g. plum, cherry, peach, apricot or almond
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/75—Rutaceae (Rue family)
    • A61K36/754—Evodia
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/87—Vitaceae or Ampelidaceae (Vine or Grape family), e.g. wine grapes, muscadine or peppervine
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D11/00—Solvent extraction
    • B01D11/02—Solvent extraction of solids
    • B01D11/0288—Applications, solvents
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine

Landscapes

  • Health & Medical Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Medicinal Chemistry (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Mycology (AREA)
  • Microbiology (AREA)
  • Medical Informatics (AREA)
  • Botany (AREA)
  • Biotechnology (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Molecular Biology (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Compounds Of Unknown Constitution (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

Ujawniono sposób ekstrakcji polifenoli z materiału roślinnego, który obejmuje następujące etapy: a) materiał roślinny poddaje się ekstrakcji roztworem ekstrakcyjnym składającym się z buforu oraz poliolu przez 1 - 360 minut; b) od surowego ekstraktu oddziela się substancje stałe; c) surowy ekstrakt lub sok uzyskany z materiału roślinnego nanosi się na kolumnę wypełnioną złożem chromatograficznym, na którym następuje zaadsorbowanie polifenoli, a następnie spłukuje się niezaadsorbowane substancje balastowe za pomocą wody; d) zaadsorbowaną na złożu chromatograficznym frakcję polifenoli eluuje się wodnym roztworem rozpuszczalnika organicznego; e) z uzyskanego oczyszczonego ekstraktu usuwa się rozpuszczalnik. Ponadto przedmiotem wynalazku jest ekstrakt z materiału roślinnego otrzymany nowym sposobem oraz jego zastosowanie.A method of extracting polyphenols from plant material is disclosed, which comprises the following steps: a) the plant material is extracted with an extraction solution consisting of a buffer and a polyol for 1-360 minutes; (b) solids are separated from the crude extract; c) the raw extract or juice obtained from the plant material is applied to a column filled with a chromatographic bed on which the polyphenols are adsorbed, followed by the rinsing of non-adsorbed ballast substances with water; d) the polyphenol fraction adsorbed on the chromatographic medium is eluted with an aqueous solution of an organic solvent; e) the solvent is removed from the obtained purified extract. Furthermore, the present invention relates to an extract of plant material obtained by a new method and its use.

PL411034A 2015-01-23 2015-01-23 Alcohol-free extraction of polyphenols PL237183B1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
PL411034A PL237183B1 (en) 2015-01-23 2015-01-23 Alcohol-free extraction of polyphenols
PCT/PL2016/000007 WO2016118027A1 (en) 2015-01-23 2016-01-22 Ethanol-free extraction of polyphenols

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL411034A PL237183B1 (en) 2015-01-23 2015-01-23 Alcohol-free extraction of polyphenols

Publications (2)

Publication Number Publication Date
PL411034A1 true PL411034A1 (en) 2016-08-01
PL237183B1 PL237183B1 (en) 2021-03-22

Family

ID=55405414

Family Applications (1)

Application Number Title Priority Date Filing Date
PL411034A PL237183B1 (en) 2015-01-23 2015-01-23 Alcohol-free extraction of polyphenols

Country Status (2)

Country Link
PL (1) PL237183B1 (en)
WO (1) WO2016118027A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112334205A (en) * 2018-06-21 2021-02-05 Gs 加德士 Solvent composition for extracting natural substance

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106420699A (en) * 2016-09-09 2017-02-22 河南城建学院 Novel tyrosinase inhibitor
CN106526025A (en) * 2016-11-01 2017-03-22 铜仁学院 Separation method for phenolic compounds in rubus corchorifolius
CN107552536B (en) * 2017-09-05 2020-02-07 贵州慧静生物科技有限公司 Comprehensive extraction process of wine waste residues
CN107821924A (en) * 2017-11-14 2018-03-23 蚌埠市涂山村富民石榴专业合作社 A kind of extraction process of garnet pigment
US20210361730A1 (en) * 2018-04-23 2021-11-25 Evonik Operations Gmbh Preparations containing anthocyanins for use in the influence of cardiovascular conditions
CN109825106A (en) * 2019-03-29 2019-05-31 江苏省农业科学院宿迁农科所 The one seed pod mulberry " Extraction of Pigment of no big ten " of seed
CN110433190B (en) * 2019-08-28 2020-12-08 汤臣倍健股份有限公司 Method for separating and extracting effective components from cowberry
CN113125581B (en) * 2020-01-10 2024-04-09 中国科学院西北高原生物研究所 HPLC method for determining anthocyanin monomer content
CN113030337B (en) * 2021-03-31 2022-10-04 福建省农业科学院农业工程技术研究所 Method for rapidly detecting citrus triterpenes, alkaloids and phenolic substances
CL2021001886A1 (en) * 2021-07-15 2021-12-17 American Bioprocess Ltda Process for purification of anthocyanins and anthocyanidins from natural extracts using adsorption resins and acidified water as desorbent
EP4241780A1 (en) * 2022-03-09 2023-09-13 Diana Enriched polyphenolic fractions of aronia extracts and uses thereof
CN115925547A (en) * 2022-12-27 2023-04-07 北京石油化工学院 Method for extracting chlorogenic acid from honeysuckle

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7306815B2 (en) * 2000-08-31 2007-12-11 Phenolics, Llc Compositions enriched in phenolic compounds and methods for producing the same
CN100560579C (en) * 2007-07-04 2009-11-18 北京绿色金可生物技术股份有限公司 Vaccinnium vitis-idaea extract and its production and application
WO2009059218A1 (en) * 2007-10-31 2009-05-07 Phytomedics, Inc. Berry preparations for treatment of diabetes and metabolic syndrome
GB0908397D0 (en) * 2009-05-15 2009-06-24 Univ Leeds Natural hair dyes

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112334205A (en) * 2018-06-21 2021-02-05 Gs 加德士 Solvent composition for extracting natural substance
CN112334205B (en) * 2018-06-21 2022-09-06 Gs 加德士 Solvent composition for extracting natural substance

Also Published As

Publication number Publication date
PL237183B1 (en) 2021-03-22
WO2016118027A1 (en) 2016-07-28

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