PL2222628T3 - Formation of nitrate esters in microreactors and millireactors using a continuous product extraction in a turbulent flow regime - Google Patents

Formation of nitrate esters in microreactors and millireactors using a continuous product extraction in a turbulent flow regime

Info

Publication number
PL2222628T3
PL2222628T3 PL08864709T PL08864709T PL2222628T3 PL 2222628 T3 PL2222628 T3 PL 2222628T3 PL 08864709 T PL08864709 T PL 08864709T PL 08864709 T PL08864709 T PL 08864709T PL 2222628 T3 PL2222628 T3 PL 2222628T3
Authority
PL
Poland
Prior art keywords
millireactors
microreactors
formation
turbulent flow
flow regime
Prior art date
Application number
PL08864709T
Other languages
Polish (pl)
Inventor
Sascha Braune
Stefan Steinhofer
Peter Poechlauer
Rafael Wilhelmus Elisabeth Ghislain Reintjens
Nicole Theodora Wilhelmina Linssen
Mehul Thathagar
Original Assignee
Dsm Fine Chemicals Austria Nfg Gmbh & Co Kg
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dsm Fine Chemicals Austria Nfg Gmbh & Co Kg filed Critical Dsm Fine Chemicals Austria Nfg Gmbh & Co Kg
Publication of PL2222628T3 publication Critical patent/PL2222628T3/en

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/02—Preparation of esters of nitric acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00851—Additional features
    • B01J2219/00858—Aspects relating to the size of the reactor
    • B01J2219/0086—Dimensions of the flow channels
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00873—Heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00889—Mixing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/0095—Control aspects
    • B01J2219/00952—Sensing operations
    • B01J2219/00954—Measured properties
    • B01J2219/00966—Measured properties pH
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/0095—Control aspects
    • B01J2219/00984—Residence time

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
PL08864709T 2007-12-20 2008-12-19 Formation of nitrate esters in microreactors and millireactors using a continuous product extraction in a turbulent flow regime PL2222628T3 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP07024754 2007-12-20
PCT/EP2008/068034 WO2009080755A1 (en) 2007-12-20 2008-12-19 Formation of nitrate esters in microreactors and millireactors using a continuous product extraction in a turbulent flow regime
EP08864709A EP2222628B1 (en) 2007-12-20 2008-12-19 Formation of nitrate esters in microreactors and millireactors using a continuous product extraction in a turbulent flow regime

Publications (1)

Publication Number Publication Date
PL2222628T3 true PL2222628T3 (en) 2012-12-31

Family

ID=39313631

Family Applications (1)

Application Number Title Priority Date Filing Date
PL08864709T PL2222628T3 (en) 2007-12-20 2008-12-19 Formation of nitrate esters in microreactors and millireactors using a continuous product extraction in a turbulent flow regime

Country Status (8)

Country Link
US (1) US8536366B2 (en)
EP (1) EP2222628B1 (en)
KR (1) KR101579989B1 (en)
CN (1) CN101903328B (en)
ES (1) ES2391601T3 (en)
HK (1) HK1151281A1 (en)
PL (1) PL2222628T3 (en)
WO (1) WO2009080755A1 (en)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW201139337A (en) 2010-03-31 2011-11-16 Lonza Ag Process for the production of esters of nitric acid
KR101433422B1 (en) * 2010-11-23 2014-08-27 주식회사 엘지화학 Device for nitration reaction and nitration method
EP2535105A1 (en) 2011-06-14 2012-12-19 Corning Incorporated Systems and methods for scale-up of microreactors
CN105330549A (en) * 2015-11-20 2016-02-17 南京理工大学 Method for preparing isooctyl nitrate in micro-channel reactor
CN105566117A (en) * 2015-12-25 2016-05-11 江西西林科股份有限公司 Isooctyl nitrate crude product deacidification method
EP3592454B1 (en) 2017-03-05 2022-10-19 Corning Incorporated Flow reactor for photochemical reactions
CN108359811A (en) * 2018-03-07 2018-08-03 昆明理工大学 A method of being stripped cobalt using micro-fluidic technologies
EP3539943A1 (en) * 2018-03-15 2019-09-18 Nitrochemie Aschau GmbH Process for the preparation of n-alkyl-nitratoethylnitramine
US10703707B2 (en) 2018-11-07 2020-07-07 Industrial Technology Research Institute Method for preparing nitrate ester
US10562873B1 (en) * 2018-12-07 2020-02-18 Northrop Grumman Innovation Systems, Inc. Methods of producing glycidyl nitrate
CN110433682B (en) * 2019-08-30 2024-04-12 欧志安 Pressure-bearing fluid mixing device

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5089652A (en) * 1990-01-17 1992-02-18 Atlas Powder Company Nitrate ester preparation
AU1090301A (en) * 1999-10-19 2001-04-30 Alliant Techsystems Inc. Polymerization of poly(glycidyl nitrate) from high purity glycidyl nitrate synthesized from glycerol
DE10014296A1 (en) * 2000-03-23 2001-09-27 Merck Patent Gmbh Dehydration of organic compounds to form unsaturated compounds comprises mixing the organic compound in liquid or dissolved form with a dehydrating agent in liquid or dissolved form in a microreactor
AU2001283076A1 (en) * 2000-08-14 2002-02-25 Chevron U.S.A. Inc. Use of microchannel reactors in combinatorial chemistry
US20050234123A1 (en) * 2001-11-27 2005-10-20 Aldo Belli Process
JP4260746B2 (en) 2002-06-26 2009-04-30 パナソニック株式会社 Characteristic correction apparatus, imaging reproduction system, characteristic correction method, and program recording medium
ITMI20022410A1 (en) 2002-11-14 2004-05-15 Dinamite Dipharma S P A PROCEDURE FOR THE NITRATION OF ALCANDIOLI.
ITMI20022409A1 (en) * 2002-11-14 2004-05-15 Dinamite Dipharma S P A PURIFICATION PROCEDURE FOR 1, 4-BUTANDIOL MONONITRATE.
US6995549B2 (en) 2003-10-14 2006-02-07 Intersil Americas Inc. DC-to-DC power regulator having non-linear load line and automatic leakage current offset adjustment
DE102004007706A1 (en) * 2004-02-16 2005-08-25 Dynamit Nobel Gmbh Explosivstoff- Und Systemtechnik Liquid nitrate esters production by esterifying alcohols with nitrating acid is effected in a microreactor to give improved safety
US7874432B2 (en) * 2004-03-23 2011-01-25 Velocys Protected alloy surfaces in microchannel apparatus and catalysts, alumina supported catalysts, catalyst intermediates, and methods of forming catalysts and microchannel apparatus
EP1944079B1 (en) 2004-06-11 2012-05-30 Corning Incorporated Microstructure designs for optimizing mixing and pressure drop
EP1838431A4 (en) * 2004-12-03 2012-08-22 California Inst Of Techn Microfluidic devices with chemical reaction circuits

Also Published As

Publication number Publication date
EP2222628A1 (en) 2010-09-01
HK1151281A1 (en) 2012-01-27
US20110034720A1 (en) 2011-02-10
WO2009080755A1 (en) 2009-07-02
CN101903328A (en) 2010-12-01
EP2222628B1 (en) 2012-07-18
KR101579989B1 (en) 2015-12-23
ES2391601T3 (en) 2012-11-28
KR20100117569A (en) 2010-11-03
CN101903328B (en) 2013-05-15
US8536366B2 (en) 2013-09-17

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