PH12023552964A1 - Process for preparing a spray dried detergent particle - Google Patents

Process for preparing a spray dried detergent particle

Info

Publication number
PH12023552964A1
PH12023552964A1 PH1/2023/552964A PH12023552964A PH12023552964A1 PH 12023552964 A1 PH12023552964 A1 PH 12023552964A1 PH 12023552964 A PH12023552964 A PH 12023552964A PH 12023552964 A1 PH12023552964 A1 PH 12023552964A1
Authority
PH
Philippines
Prior art keywords
preparing
spray
detergent particle
dried
slurry
Prior art date
Application number
PH1/2023/552964A
Inventor
Abraham Chacko
Girish Kumar
Sharavan Kumar
Kunal Shankar Pawar
Nadeem Shaikh
Original Assignee
Unilever Ip Holdings B V
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Unilever Ip Holdings B V filed Critical Unilever Ip Holdings B V
Publication of PH12023552964A1 publication Critical patent/PH12023552964A1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/10Carbonates ; Bicarbonates
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02Anionic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00Special methods for preparing compositions containing mixtures of detergents
    • C11D11/02Preparation in the form of powder by spray drying
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/046Salts
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/04Water-soluble compounds
    • C11D3/08Silicates
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/12Water-insoluble compounds
    • C11D3/122Sulfur-containing, e.g. sulfates, sulfites or gypsum
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/12Water-insoluble compounds
    • C11D3/1233Carbonates, e.g. calcite or dolomite

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

The present invention relates to a process for preparing of a particulate, free flowing detergent particle by a slurry making and spray drying technique. In particular it relates to the process for preparing a slurry with lower alkalinity for the production of spray dried laundry detergent particle. It is thus an object of the present invention to provide a process for preparing a detergent solution for a spray-dried detergent particle which provides for incorporating higher levels of the detersive surfactant whilst providing good powder properties. The present inventors have found that a spray dried detergent particle prepared from a slurry with high detersive surfactant content in presence of an in-situ formed silicate and/or a disilicate salt of alkaline earth metal, formed by reacting an alkali metal silicate with an alkaline earth metal salt, and an alkali metal silicate salt provides for excellent powder properties and extended shelf life without getting caked. It is also surprisingly found that the spray-dried particle provides desired pH in wash solution required for good stain removal performance without being harsh on the hands or the fabrics.
PH1/2023/552964A 2021-05-19 2022-05-17 Process for preparing a spray dried detergent particle PH12023552964A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP21174577 2021-05-19
PCT/EP2022/063233 WO2022243265A1 (en) 2021-05-19 2022-05-17 Process for preparing a spray dried detergent particle

Publications (1)

Publication Number Publication Date
PH12023552964A1 true PH12023552964A1 (en) 2024-03-11

Family

ID=76011745

Family Applications (1)

Application Number Title Priority Date Filing Date
PH1/2023/552964A PH12023552964A1 (en) 2021-05-19 2022-05-17 Process for preparing a spray dried detergent particle

Country Status (6)

Country Link
EP (1) EP4341367B1 (en)
CN (1) CN117242164A (en)
BR (1) BR112023024010A2 (en)
PH (1) PH12023552964A1 (en)
WO (1) WO2022243265A1 (en)
ZA (1) ZA202309729B (en)

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5335081B1 (en) 1971-06-30 1978-09-25
AT330930B (en) 1973-04-13 1976-07-26 Henkel & Cie Gmbh PROCESS FOR THE PRODUCTION OF SOLID, SPILLABLE DETERGENTS OR CLEANING AGENTS WITH A CONTENT OF CALCIUM BINDING SUBSTANCES
DE2433485A1 (en) 1973-07-16 1975-02-06 Procter & Gamble ALUMINOSILICATE ION EXCHANGERS SUITABLE FOR USE IN DETERGENTS
DE2413561A1 (en) 1974-03-21 1975-10-02 Henkel & Cie Gmbh STORAGE-RESISTANT, EASILY-RELEASE DETERGENT ADDITIVE AND METHOD FOR MANUFACTURING IT
GB1504878A (en) 1974-05-30 1978-03-22 Unilever Ltd Production of detergent compositions
US4139486A (en) 1977-03-22 1979-02-13 The Procter & Gamble Company Built detergent composition
DE3413571A1 (en) 1984-04-11 1985-10-24 Hoechst Ag, 6230 Frankfurt USE OF CRYSTALLINE LAYERED SODIUM SILICATES FOR WATER SOFTENING AND METHOD FOR WATER SOFTENING
CA2001927C (en) 1988-11-03 1999-12-21 Graham Thomas Brown Aluminosilicates and detergent compositions
US5773399A (en) 1993-12-10 1998-06-30 The Procter & Gamble Comapny Stabilization of oxidation-sensitive ingredients in percarbonate detergent compositions
WO2005037712A1 (en) 2003-10-20 2005-04-28 Theo Jan Osinga Method for the preparation of a suspension
GB0420356D0 (en) 2004-09-13 2004-10-13 Unilever Plc Detergent compositions and their manufacture
EP2138565A1 (en) * 2008-06-25 2009-12-30 The Procter and Gamble Company A spray-drying process
HUE046263T2 (en) 2016-10-03 2020-02-28 Procter & Gamble Process for the manufacture of a spray dried detergent particle

Also Published As

Publication number Publication date
EP4341367B1 (en) 2024-11-20
BR112023024010A2 (en) 2024-01-30
EP4341367C0 (en) 2024-11-20
ZA202309729B (en) 2025-03-26
EP4341367A1 (en) 2024-03-27
WO2022243265A1 (en) 2022-11-24
CN117242164A (en) 2023-12-15

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