PH12016000064A1 - LOW COST ORGANO MINERALS FOR WASTEWATER TREATMENT and ODOUR REMOVAL - Google Patents

LOW COST ORGANO MINERALS FOR WASTEWATER TREATMENT and ODOUR REMOVAL Download PDF

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Publication number
PH12016000064A1
PH12016000064A1 PH12016000064A PH12016000064A PH12016000064A1 PH 12016000064 A1 PH12016000064 A1 PH 12016000064A1 PH 12016000064 A PH12016000064 A PH 12016000064A PH 12016000064 A PH12016000064 A PH 12016000064A PH 12016000064 A1 PH12016000064 A1 PH 12016000064A1
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PH
Philippines
Prior art keywords
wastewater
septic
odor neutralizer
powder mixture
wastewater treatment
Prior art date
Application number
PH12016000064A
Inventor
A Palencia Merlinda
A Dural Clifford
Original Assignee
Palencia Merlinda
A Dural Clifford
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Palencia Merlinda, A Dural Clifford filed Critical Palencia Merlinda
Priority to PH12016000064A priority Critical patent/PH12016000064A1/en
Priority to PCT/PH2016/000006 priority patent/WO2017138822A1/en
Publication of PH12016000064A1 publication Critical patent/PH12016000064A1/en

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/043Carbonates or bicarbonates, e.g. limestone, dolomite, aragonite
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/04Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
    • B01J20/048Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium containing phosphorus, e.g. phosphates, apatites, hydroxyapatites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/12Naturally occurring clays or bleaching earth
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/14Diatomaceous earth
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16Alumino-silicates
    • B01J20/165Natural alumino-silicates, e.g. zeolites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004Sorbent size or size distribution, e.g. particle size
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/3021Milling, crushing or grinding
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/3028Granulating, agglomerating or aggregating
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/28Treatment of water, waste water, or sewage by sorption
    • C02F1/281Treatment of water, waste water, or sewage by sorption using inorganic sorbents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00Aspects relating to sorbent materials
    • B01J2220/40Aspects relating to the composition of sorbent or filter aid materials
    • B01J2220/46Materials comprising a mixture of inorganic and organic materials
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2303/00Specific treatment goals
    • C02F2303/02Odour removal or prevention of malodour

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Hydrology & Water Resources (AREA)
  • Water Supply & Treatment (AREA)
  • Environmental & Geological Engineering (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Water Treatment By Sorption (AREA)
  • Activated Sludge Processes (AREA)

Abstract

The invention describes a composition and method for biochemical and mechanical remediation of wastewater or river in which the biomineral is an oxygen releasing material that increases dissolved oxygen, decreases biochemical oxygen demand and chemical oxygen demand and neutralized strong odor through the use of organo-minerals, The claimed composition comprises of dolostone, organic limestone, rocks, petrified wood, clay minerals and zeolites. The claimed composition is utilized either in powder form and applied through dispersion.

Description

water would be allowed to flow to a fourth chamber until day 14. Cumulatively, said . water has received 1.5 kg/m3 treatment of prepared organominerals. Day 14 would mean the opening of effluent pipes for treated wastewater.
In another aspect of invention, organominerals were applied to wastewater from a concentration of 0.5 kg/m? — 1.5 kg/m3.
In another aspect of the invention, the application of the organomineral mixture is proven effective in the treatment of wastewater as shown in the following results.
A. Odor Removal
Odor was determined by five (5) panelist with a keen sense of smell and were determined to be free from cold and allergies. Samples were diluted with odor-free distilled water using varying proportion until they were of the same odor as the standard odor - free distilled water. The number of dilution gives the TON or threshold odor number (TON) determined through stated formula
TON = (Volume of Sample) + (Volume of added odor — free water)
B. Volume of sample
In another aspect, reduction of odor in the wastewater through TON (Threshold Odor Number) was done. The wastewater before remediation generally had a foul or rotten egg odor with a TON value of 110. The remediation is effective in reducing the odor or wastewater to TON ranging from 1 — 6 only. Higher concentrations of biomineral showed higher % odor reduction. 0.5 — 1.0 kg/m? concentration can reduce odor by 95% while 1.5 kg/m? concentration can reduce odor by as much as 98% after 10 days. The reduction in foul odor can be attributed by the application of biomineral which enhances the growth of bacteria and microorganisms present in wastewater. Bacteria and microorganisms then digested the pollutants present that caused the foul odor. In addition, the organominerals significantly increased the amount of oxygen in wastewater thereby promoting aerobic decomposition reaction while limiting anaerobic reaction.
Odor 0 1 4 10 | 14 [15 cancerration | 105 | S317 60 | #0 16
Page 7 of 13
EEE, ————
water would be allowed to flow to a fourth chamber until day 14. Cumulatively, said . water has received 1.5 kg/m3 treatment of prepared organominerals. Day 14 would mean the opening of effluent pipes for treated wastewater.
In another aspect of invention, organominerals were applied to wastewater from a concentration of 0.5 kg/m? — 1.5 kg/m3.
In another aspect of the invention, the application of the organomineral mixture is proven effective in the treatment of wastewater as shown in the following results.
A. Odor Removal
Odor was determined by five (5) panelist with a keen sense of smell and were determined to be free from cold and allergies. Samples were diluted with odor-free distilled water using varying proportion until they were of the same odor as the standard odor - free distilled water. The number of dilution gives the TON or threshold odor number (TON) determined through stated formula
TON = (Volume of Sample) + (Volume of added odor — free water)
B. Volume of sample
In another aspect, reduction of odor in the wastewater through TON (Threshold Odor Number) was done. The wastewater before remediation generally had a foul or rotten egg odor with a TON value of 110. The remediation is effective in reducing the odor or wastewater to TON ranging from 1 — 6 only. Higher concentrations of biomineral showed higher % odor reduction. 0.5 — 1.0 kg/m? concentration can reduce odor by 95% while 1.5 kg/m? concentration can reduce odor by as much as 98% after 10 days. The reduction in foul odor can be attributed by the application of biomineral which enhances the growth of bacteria and microorganisms present in wastewater. Bacteria and microorganisms then digested the pollutants present that caused the foul odor. In addition, the organominerals significantly increased the amount of oxygen in wastewater thereby promoting aerobic decomposition reaction while limiting anaerobic reaction.
Odor 0 1 4 10 | 14 [15 cancerration | 105 | S317 60 | #0 16
Page 7 of 13
EEE, ————

Claims (1)

  1. ~ » Claims « I 1. An organomineral powder mixture suitable for wastewater and/ or septic wastewater treatment and odor neutralizer comprising of % weight Dolostone - 15-35 Lo ~Organic Limestone 15-35 = 2% Biogenic Siliceous rocks 5-15 o, 2 2, i Biogenic Phosphate rocks 1-15 : \, \ : Petrified Wood 1-10 %
    _.Clay Minerals 1-10 = A Natural Zeolites 1-15 — Organic Solution 1-10 Wherein the powder mixture is capable of odor neutralizer of wastewater and/ or septic tanks.
    0 2. An organomineral powder mixture suitable for wastewater and/ or septic wastewater treatment and odor neutralizer as claimed in 1 wherein the organic solution is selected from exotic fruit juices or extracts. . ~My 3. An organomineral powder mixture suitable for wastewater and / (Or, septic irre wastewater treatment and odor neutralizer as claimed in1 ol 2 wherein exotic fruit juices or extracts are preferably chosen from any of the following such as watermelon, pineapple or coconut. Aa p odd U0 peat 1 4, A process for preparation of powder mixtuge suitable for wastewater and/ or v res septic wastewater treatment and odor neutralizer comprising the steps of -;7 + Preparation of raw materials - Primary and secondary crushing or size reduction of raw materials - Primary and secondary vibrating screening - Weighing and mixing of crushed raw materials - Thermal treatment of prepared materials - Pulverizing or grinding of prepared materials - Packaging of prepared materials
    U 5. A frocess for preparation of powder mixture suitable for wastewater and/ or ] septic wastewater treatment and odor neutralizer as claimed in (claim 1 Fi dud wherein the size of the powder is limited. — Page 11 of 13
    ~ » Claims « I 1. An organomineral powder mixture suitable for wastewater and/ or septic wastewater treatment and odor neutralizer comprising of % weight Dolostone - 15-35 Lo ~Organic Limestone 15-35 = 2% Biogenic Siliceous rocks 5-15 o, 2 2, i Biogenic Phosphate rocks 1-15 : \, \ : Petrified Wood 1-10 %
    _.Clay Minerals 1-10 = A Natural Zeolites 1-15 — Organic Solution 1-10 Wherein the powder mixture is capable of odor neutralizer of wastewater and/ or septic tanks.
    0 2. An organomineral powder mixture suitable for wastewater and/ or septic wastewater treatment and odor neutralizer as claimed in 1 wherein the organic solution is selected from exotic fruit juices or extracts. . ~My 3. An organomineral powder mixture suitable for wastewater and / (Or, septic irre wastewater treatment and odor neutralizer as claimed in1 ol 2 wherein exotic fruit juices or extracts are preferably chosen from any of the following such as watermelon, pineapple or coconut. Aa p odd U0 peat 1 4, A process for preparation of powder mixtuge suitable for wastewater and/ or v res septic wastewater treatment and odor neutralizer comprising the steps of -;7 + Preparation of raw materials - Primary and secondary crushing or size reduction of raw materials - Primary and secondary vibrating screening - Weighing and mixing of crushed raw materials - Thermal treatment of prepared materials - Pulverizing or grinding of prepared materials - Packaging of prepared materials
    U 5. A frocess for preparation of powder mixture suitable for wastewater and/ or ] septic wastewater treatment and odor neutralizer as claimed in (claim 1 Fi dud wherein the size of the powder is limited. — Page 11 of 13
PH12016000064A 2016-02-12 2016-02-12 LOW COST ORGANO MINERALS FOR WASTEWATER TREATMENT and ODOUR REMOVAL PH12016000064A1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
PH12016000064A PH12016000064A1 (en) 2016-02-12 2016-02-12 LOW COST ORGANO MINERALS FOR WASTEWATER TREATMENT and ODOUR REMOVAL
PCT/PH2016/000006 WO2017138822A1 (en) 2016-02-12 2016-09-07 Low cost organominerals for wastewater treatment and odor neutralizer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PH12016000064A PH12016000064A1 (en) 2016-02-12 2016-02-12 LOW COST ORGANO MINERALS FOR WASTEWATER TREATMENT and ODOUR REMOVAL

Publications (1)

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PH12016000064A1 true PH12016000064A1 (en) 2017-08-23

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PH12016000064A PH12016000064A1 (en) 2016-02-12 2016-02-12 LOW COST ORGANO MINERALS FOR WASTEWATER TREATMENT and ODOUR REMOVAL

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WO (1) WO2017138822A1 (en)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2020097680A1 (en) * 2018-11-13 2020-05-22 Southern Spongolite Industries Pty Ltd Method for decontaminating a liquid

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ITMI981667A1 (en) * 1998-07-20 2000-01-20 Manitoba Italia Spa COMPOSITION FOR THE TREATMENT OF WASTEWATER IN PARTICULAR FOR THE TREATMENT OF THE WATER FROM BIOLOGICAL TANKS
US6808631B2 (en) 2002-10-22 2004-10-26 Rolf Paloheimo Aerobic wastewater treatment apparatus
WO2004067453A1 (en) * 2003-01-31 2004-08-12 Idemitsu Kosan Co., Ltd. Method of treating wastewater containing hardly decomposable harmful substances
GB0821881D0 (en) 2008-12-01 2009-01-07 Jowett E C Biological filtration system with socks of absorbent material
CN105110395A (en) * 2015-09-30 2015-12-02 宁波保税区韬鸿化工科技有限公司 Water treatment agent and preparing method

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