NZ626168B2 - Sonotrode and device for reducing and eliminating foaming of liquid products - Google Patents

Abstract

Disclosed is a sonotrode (10) for generating an ultrasonic field in industrial production processes for reducing and eliminating foaming of liquid products (3). The sonotrode (10) includes a main body part (1) with connecting means for connection with a high frequency generator and has a front face from which the ultrasonic field is directed to the desired spot or area of the product (3) to be de-foamed. The main body part (1) has the shape of a rectangular or square block element having a reduced diameter part on the side of the front face which is enlarged compared to the latter. The front face is concave in shape in relation to a product (3) surface for focusing the ultrasonic field to a specific area of the product (3) foam to be treated in a concentrated form compared to a non-focused ultrasound. The front face has a rectangular form with a round concavity in the direction of the longitudinal axis in the shape of a rounded groove or channel. from which the ultrasonic field is directed to the desired spot or area of the product (3) to be de-foamed. The main body part (1) has the shape of a rectangular or square block element having a reduced diameter part on the side of the front face which is enlarged compared to the latter. The front face is concave in shape in relation to a product (3) surface for focusing the ultrasonic field to a specific area of the product (3) foam to be treated in a concentrated form compared to a non-focused ultrasound. The front face has a rectangular form with a round concavity in the direction of the longitudinal axis in the shape of a rounded groove or channel.

Description

DescriptionDescription Sonotrode and Device for Reducing and Eliminating FSonotrode and Device for Reducing and Eliminating Foaming of Liquid Productsoaming of Liquid Products The present invention s to a sonotrode for generating an ultrasonic field in rial production processes such as chemical processes or food-related processes, in which a liquid product is processed, which generates during the processing a g on the upper surface of the product. The invention relates also to a device comprising one or more such sonotrodes for de-foaming.

In different fields of industry, the foam generation of a product to be processed is an inherent problem. In the field of beverage ry, for example, mainly with carbonated products such as cola and beer, but also with non-carbonated products such as fruit juices, etc., there exists during the production process, but also during the filling of the product into bottles or the like the problem that the product generates a large amount of foam.

The generation of foam results often in an red loss of product, and also the contamination of the containers, into which the product is to be filled, is a big m in these industries. During the filling s, the tion of too much foam leads to problems with regard to the sealing of the containers, and furthermore the filling line process is considerably slowed down due to the foam on top of the product. However, also in other industries, the foam generation of liquid products is a matic issue.

Examples of other industries are the chemical, petroleum, pharmaceutical and mining industries. Foam can form in tanks, open vessels or in containers or bottles, into which the product is filled. Due to the foam, there exists also a problem with regard to the vessel capacity/volume, the downstream processing equipment such as pumps, homogenizers, pasteurizers, filling lines and the filtration equipment.

In the prior art, tional technologies used to reduce or to act against the generation of too much foam have for several years involved the use of anti-foam chemicals. However, in the food industry, the use of als is not possible, and in other industries the use of such chemicals for reducing the generation of foam is rather cost-intensive.

Also, the chemicals may change the teristics of the liquid t, which is processed in the production line.

Furthermore, mechanical foam breakers have been ted in the prior art in order to limit the generation of foam during the filling of beer or cola into bottles, for example. A further solution to this type of problem consists in anti-foam devices using ound waves for the destruction of foam on top of the liquid product. In A1, for example, an ultrasonic device is disclosed for eliminating the creation of foam in large containers. This known device uses round, plate-shaped resonators mounted on a rotating device and being ed with means for changing the angle of the treatment surface of the resonator plates of this device in the direction of the product. Through the change of the angle of the plateshaped resonators and the rotation of the two devices, the ultrasonic field is d on a specific spot on the surface of the product container. This system is rather big in its construction and difficult to be implemented in existing filling lines without substantial modifications. Furthermore, this known ultrasonic device needs complicated means for controlling the creation of the ultrasonic field and for permanent modifying the angle of radiation of the focused ultrasonic field.

In A1, a further ultrasonic transducer system is disclosed, having a sonotrode with a main body part and a liquid ent surface on its end. The foam treatment e of this sonotrode is provided with a plurality of horn-shaped cavities. Due to the plurality of cavities, a more intensive ultrasonic field may be emitted. However, also this type of an ultrasonic treatment device has disadvantages in terms of the possibility to eliminate the generation of foam in certain applications, e.g. in filling lines for filling beverages into bottles or containers.

In view of the mentioned cks of the prior art ons, it is an object of at least red embodiments of the present invention to provide a sonotrode and an ultrasonic device with at least one sonotrode, which are more ent and more flexible with respect to the application in existing production lines and with respect to the foam elimination and foam ion in different tion processes, and/or to at least provide the public with a useful .

This problem is solved by a sonotrode with the features of claim 1 and by a device for generating an ultrasonic field ing to the features of claim 9. Preferred embodiments and characteristics of the invention are disclosed in the respective dependent claims.

A first aspect of the invention as claimed in claim 1 provides a sonotrode for generating an ultrasonic field in industrial production processes for reducing and eliminating foaming of liquid products with a compact onepiece form of the sonotrode body. The sonotrode is provided with a main body part having connecting means for the connection of the sonotrode with a high-frequency generator, and has a front face, from which the ultrasonic field is directed to the desired spot or area of the t to be de-foamed. The main body part has a shape of a rectangular or square block element having a reduced diameter part on the side of the front face which is enlarged compared to the reduced diameter part, and the front face is concave in shape in relation to a product surface for focusing the onic field to a specific area of a product foam to be treated in a concentrated form compared to a non-focused ound. Said front face has a rectangular form with a round concavity in the direction of the longitudinal axis in the shape of a d groove or channel.

In an embodiment, as a result of the concave form of the front face, the ultrasonic field is concentrated compared to a flat or a convex front face.

The cavity of the front face according to the invention is preferably formed such that an increased effect for the de-foaming of a liquid product is achieved. The concave front face of the ode according to the invention may in particular be formed like a rounded groove or channel with an especially optimized ure. In an embodiment, the ultrasonic high-amplitude frequency, which is introduced into the sonotrode by means of a connecting part, is effectively itted by the block-shaped main body part to the concave front face such that the generation of foam during the processing of the liquid product can be effectively eliminated and reduced.

According to an advantageous form of realization of the invention, the sonotrode is provided with a high power output, in particular with an ultrasonic power output into air of between 1 and 10,000 watts, between 2 and 1000 watts, preferably 5 to 1 to 800 watts, more preferably 10 to 700 watts, and even more preferably between 20 to 600 watts.

According to an advantageous form of realization of the invention, the sonotrode is provided with a high-amplitude ratio, in particular with an ultrasonic amplitude of peak-to-peak displacement between 1 and 150 microns, preferably 5 to 140 microns, more preferably 10 to 120 s, and even more preferably 30 to 120 microns. h extensive search, the inventors have found out that with these ranges of a high-amplitude ratio a highly effective foam destruction and reduction is possible.

Surprisingly, these high-frequency ratios have turned out to be most effective for the e of de-foaming liquid products.

According to a further advantageous form of realization of the invention, the main body part is of a rectangular block-like shape having a reduced diameter part on the side of the front face, which is enlarged compared to the latter. This means, the sonotrode has in its upper region a blockshaped part of a t form with the means for connecting the sonotrode to a high-frequency tor. However, in the lower part, i.e. the part closer to the front face, which is provided for directing the ultrasonic field on the foam of the product, there is provided an area of reduced diameter, so that the sonotrode has a cross-sectional tree-like form. This form is most effective for creating a high-frequency ultrasonic field with a compact and – from a first point of view – rather simply formed ode. It has shown that the enlarged n of the front face with a reduced diameter part between the like body part and the front face is excellent for transmitting a large amount of high-frequency ultrasonic beams onto the product to be treated. Therefore, the de-foaming effect is considerably increased by means of this type of sonotrode ing to the invention.

According to a further ageous form of realization of the invention, between the main body part and the front face of the sonotrode for generating the focused ultrasonic field of a high amplitude, a neck-like portion with round lateral ations along a longitudinal axis L of the concave front face is provided, which has a longitudinal axis L, which is approximately perpendicular to a longitudinal axis S of the sonotrode itself.

According to a further advantageous form of realization of the invention, the sonotrode device improves the impedance ng with air and as a result improves the ultrasonic energy output efficiency and penetration distance through the air with sufficient energy to collapse foam at the following distances away from the emitting surface of the front face of the sonotrode: 0.1mm to 1000mm, preferably 0.2mm to 500mm, more preferably between 1mm and 250mm and most preferably between 10mm and 100mm.

According to a further advantageous form of realization of the invention, the ode device is of such a form and size that it could be orated into a pipe, open trough, closed or open tank, vessel, container (made of steel, plastic, glass, metal) containing a flow-able material of foam, or foam and liquid or foam, liquid and solids and the ultrasonic and in a way that energy emitted from the sonotrode surface or concave front face would break the foam passing through.

According to a further preferred form of realization of the invention, the front face of the sonotrode has a rectangular form with a round ity in the udinal direction L.

According to a further advantageous form of realization of the invention, the sonotrode has a concavity at its front face, which is formed like a segment of a circle with a radius between r = 2 cm to r = .

The sonotrode according to the invention is preferably made of a metal material, such as steel (stainless steel?), aluminum, nickel, titanium or alloys of these types of als. The best de-foaming s have been achieved with a ode made out of a material that has a high degree of tensile strength c force (e.g. titanium alloy).

According to a further advantageous form of ation of the invention, the form and construction of the block-type sonotrode is such that the ultrasonic sound intensity is between 10 to 200 db, preferably 50 to 190 db, more preferably 70 to 180 db, and most ably 100 to 175 db.

These values of ultrasonic sound intensity have shown very good s in the de-foaming of very different types of liquid products such as ges (cola, diet cola, diet carbonated fruit drinks, sugar based carbonated fruit drinks, none carbonated fruit drinks, ginger beer, root beer, dairy products, dairy/fruit drinks, beer, all ated drinks, none carbonated drinks, fermentation , dairy protein based fluids, soy protein based fluids, whey protein based fluids, oil based fluids, etc.) as well as chemical or pharmaceutical products.

According to a further ageous feature of the sonotrode according to the invention, the block-shaped main body part is provided with a circular central connection portion for connecting to an onic generator.

Through this constructive measure, the block element of the sonotrode is on its upper surface formed with a disk-like central connecting part, which has turned out to be very ive for the introduction and distribution of the high-amplitude ultrasonic field from the high-frequency generator to the front face, which emits the high-frequency ultrasound to the product surface to be treated.

A second aspect of the present invention is also directed to a device for de-foaming liquid products in industrial production processes, such as chemical, pharmaceutical or beverage-related processes, according to the features of claim 9, which comprises an ound generator, a converter with a cooling unit and at least one high-frequency cable for connecting sonotrode(s) to the generator. The device is provided with at least one block-shaped high-amplitude ratio sonotrode as described above according to the first aspect.

According to a preferred form of ation the device is provided with two sonotrodes mounted on a common mother sonotrode such that both udinal axis L of the front faces are essentially parallel to one another.

By means of this the de-foaming effect is increased and a larger area of product can be treated at the same time.

According to one further aspect of the de-foaming device according to the invention the sonotrodes are arranged with their front faces in line with a transport direction of a production line of the product to be treated. That means the longitudinal axis of the front faces are in the same direction as the transport of product or bottles in the production line. A rather long ultrasonic field is emitted though this measure.

Alternatively the sonotrodes are ed with their front faces in an angle with respect to a ort direction of a production line of the product to be treated. Preferably the angle n the longitudinal axis L and the direction of product process may be = 90° or more preferably = 45°.

With this kind of a lateral acting of the ultrasonic field to the product surface in some specific applications the treatment ha surprisingly been shown to be more effective.

Further advantages, features and forms of realization are described in the following detailed description of some embodiments of the invention, with reference to the accompanying drawings, in which: Fig. 1 is a ctive view of a first example of ation of the inventive sonotrode; Fig. 2a is a perspective view of an example of realization of a sonotrode device ing to the invention with two sonotrodes in line with the product process; Fig. 2b is a perspective view of an example of realization of a sonotrode device according to the invention with two sonotrodes arranged in an angle compared to the product process; and Fig. 2c is a ctive view of a r example of realization of a ode device ing to the invention with two sonotrodes in an angle of 90° in relation to the product process.

Figure 1 shows in a perspective view a first example of realization of a sonotrode according to the invention. The sonotrode 10 ses in general two different parts: first, on the upper side, there is provided a main body part 1, and second, on the lower part, which is also the part being directed to the liquid product to be treated, there is a front face 2, which according to the invention has a concavity in the direction of the product (bottom part in Fig. 1). Here, the main body part 1 has the rectangular or square form of a compact block-like element 40. At the upper end of the main body part 1, the sonotrode 10 according to this example of realization is provided with a circular central connection portion, which has the form of a disk-shaped part made of the same material and in one piece with the sonotrode 10. In this example of realization, the upper edges of the main body part 2 are slightly rounded, and the lateral edges are chamfered. In the lower half of the sonotrode 10, there is provided a reduced diameter part 41, which in a cross-sectional view has a Y-like form with rounded lateral indentations and which is ed to the bottom end of the sonotrode 10 in order to form a rectangular front face 2 having a concavity 21 in the direction of the product to be treated. The concavity 21 has a longitudinal axis L, which is dicular to the overall longitudinal axis S of the sonotrode 10 and its main body part 1.

The concave front face 2 being ted to the main body part 1 through the reduced diameter part 41 results in an excellent transmission of highamplitude ratio ultrasonic frequencies from the ultrasound generator to the front face 2, from which the onic field is to be emitted in a focused manner onto the foam of a product, which forms, for example, on the upper surface of a liquid product in a production vessel.

The concavity of the front face 2 is formed ably with an radius of r = 2 cm or more. The focusing of the ultrasonic field is hereby optimized in view of the de-foaming purpose of liquid products. With the concave form of the front face 2 a more d and thereby more concentrated ultrasound is d. This increases the effect of eliminating the foam generation. According to advantageous embodiment of the inventive sonotrode is provided with a high amplitude ratio, in ular with an ultrasonic amplitude of peak to peak displacement between 1 and 150 microns, preferably 5 to 140 microns, more ably 10 to 120 microns and more preferably 30 to 120 microns. These values are best for foam eliminating in most liquid products, in particular beverages such as cola or beer.

The form and construction of the sonotrode (10) according to the invention is such that the ultrasonic sound intensity is approximately between 10 to 200 db, preferably 50 to 190 db, more preferably 70 to 180 db and most ably 100 to 175 db. With these ranges of intensity the sonotrode 10 achieves best results and the generation of foam is ted.

In Fig. 2a to 2c three different examples of realization of a sonotrode device ing to the invention with two combined odes are shown. These devises 20 have each two sonotrodes 10 mounted on a common mother sonotrode 4 or common base element. The mother sonotrode 4 is connected to a hiegh frequency cable and ultrasound generator (not shown) and transfers the frequency directly to the both sonotrodes 10. These sonotrodes 10 are essentially of the same shape and have the same characteristics as the form of realization described in connection with Fig. 1.

The mother sonotrode 4 in the examples of realization (Fig. 2a to 2c) is a rectangular block element with a I-type cross-section, i.e. enlarged end portions and a reduced diameter in the middle section. The middle n of the mother sonotrode 4 is here provided with to udinal throughholes in order to reduce the weight and to increase the transfer of ultrasound to the two sonotrodes 10. Both sonotrodes 10 are actuated thereby with the same and increased amount of ound.

Fig. 2a shows an example of realization in which the longitudinal axis L of the sonotrodes 10 are in line or parallel to the transport direction of the production line of the product to be treated (cf. arrows in Fig. 2a).

In Fig. 2b a similar ultrasonic device 20 is shown with the difference that the two parallel sonotrodes 10 are not in line with the transport dorection of the t 3 but are turned in an angle of approximately 45° (angle = 45°). In some application areas this arrangement has resulted in much better results.

The further example of realization ing to Fig. 2c shows both sonotrodes 10 being in an angle of 90° compared to the direction of transport of the t 3 or bottles. By means of this the width of the ultrasonic concentrated field is increased. The number of sonotrodes can be increased and be more than two. Furthermore the form of the sonotrodes 10 and mother-sonotrode 4 may be changed as long as the front faces 2 of the sonotrodes 10 are provided with an concavity increasing the focusing effect as specified in the appended claims.

The product 3 or liquid to be med by the sonotrode 10 or device 20 according to the invention may be in a vessel, container etc. (in Fig. 2a to 2c only schematically indicated). Or the product is filled in a filling line into separate bottles or the like. The ive sonotrode and device is especially adapted for both applications due to its new sonotrode design and highly focused ultrasound field. The flexibility and variation of application areas is therefore y increased for very different industrial production processes regarding foam creating liquids.

The term ‘comprising’ as used in this specification and claims means ‘consisting at least in part of’. When interpreting statements in this specification and claims which include the term ‘comprising’, other features besides the features prefaced by this term in each ent can also be present. d terms such as ise’ and ‘comprised’ are to be interpreted in similar manner.

Claims (18)

Claims

1. Sonotrode for generating an ultrasonic field in industrial production processes for reducing and eliminating foaming of liquid products with a compact onepiece form of the sonotrode body, wherein the sonotrode is provided with a main body part having ting means for connection with a high frequency generator and having a front face from which the ultrasonic field is directed to the desired spot or area of the product to be de-foamed, wherein the main body part has the shape of a rectangular or square block element having a d diameter part on the side of the front face which is enlarged compared to the reduced diameter part and wherein the front face is concave in shape in relation to a product surface for focusing the ultrasonic field to a specific area of a product foam to be treated in a concentrated form compared to a nonfocused ultrasound and wherein said front face has a rectangular form with a round concavity in the direction of the longitudinal axis in the shape of a rounded groove or channel.

2. Sonotrode according to claim 1, n between the main body part and the front face for generating the focused ultrasonic field, a neck-like tapered portion with round lateral indentations along a longitudinal axis of the front face is provided which axis is imately perpendicular to a longitudinal axis of the sonotrode.

3. Sonotrode according to any one of the ing claims, wherein said concavity of the front face is formed in its cross section perpendicular to a longitudinal axis of the ode like a segment of a circle with a radius between r = 2 cm to r = .

4. ode according to any one of the preceding claims, wherein the sonotrode is made of steel, aluminium, nickel, titanium or alloys of these materials.

5. Sonotrode according to any one of the preceding , wherein said the main body part and said front face are formed in a one-piece body realized of the same al.

6. ode according to claim 5, wherein said same material is titanium or an alloy including titanium.

7. Sonotrode according to any one of the ing claims, wherein the blockshaped main body part is provided with a ar central connection portion for connecting to an onic generator.

8. Sonotrode according to any one of the preceding claims, wherein said industrial production processes is selected from the group consisting of chemical, food, petroleum, ceutical, beverage or mining-related processes.

9. Device for de-foaming liquid products in industrial production processes comprising an ultrasound generator, a converter with a g unit, at least one high frequency cable for connecting ode(s) to the generator, wherein said device is provided with at least one shaped high amplitude ratio sonotrode according to any of the preceding claims 1 to 8.

10. Device according to claim 9, comprising means for producing a high amplitude ratio ultrasound

11. Device according to claim 10, wherein said means for producing a high amplitude ratio ultrasound are means for producing a high amplitude ratio ultrasound in the range of an ultrasonic ude of peak to peak cement between 1 and 150 microns.

12. Device according to any one of claims 9 to 11, wherein the ultrasonic sound intensity is between 10 and 200 db.

13. Device according to any one of claims 9 to 12, wherein at least two sonotrodes are provided which are mounted on a common mother sonotrode such that both longitudinal axis of the front faces are parallel to one another and that both ultrasonic fields are combined in the area of the product to be treated in order to increase the de-foaming effect.

14. Device according to any one of claims 9 to 13, wherein the sonotrodes are arranged away from the product to be treated such that the ultrasound ng surface of the front faces of the sonotrode(s) is/are in a distance of 0.1 mm to 1000 mm.

15. Device according to any one of claims 9 to 14, wherein said inductrial production processes is ed from the group consisting of chemical, pharmaceutical or beverage related processes.

16. Sonotrode according to claim 1, substantially as herein described with reference to any embodiment disclosed.

17. A sonotrode for ting an ultrasonic field in industrial production processes, substantially as herein described with nce to any embodiment shown in the accompanying drawings.

18. A device according to claim 9, substantially as herein described with reference to any embodiment disclosed. WO 72296 /*'\