NZ615297B2 - A powder mix and a method for producing a building panel - Google Patents
A powder mix and a method for producing a building panel Download PDFInfo
- Publication number
- NZ615297B2 NZ615297B2 NZ615297A NZ61529712A NZ615297B2 NZ 615297 B2 NZ615297 B2 NZ 615297B2 NZ 615297 A NZ615297 A NZ 615297A NZ 61529712 A NZ61529712 A NZ 61529712A NZ 615297 B2 NZ615297 B2 NZ 615297B2
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- New Zealand
- Prior art keywords
- powder mix
- layer
- cure
- mix layer
- powder
- Prior art date
Links
- 239000000843 powder Substances 0.000 title claims abstract description 129
- 239000000203 mixture Substances 0.000 title claims abstract description 103
- 238000004519 manufacturing process Methods 0.000 title abstract description 17
- 238000001035 drying Methods 0.000 claims abstract description 37
- 239000012530 fluid Substances 0.000 claims abstract description 30
- 239000011230 binding agent Substances 0.000 claims abstract description 24
- 230000004580 weight loss Effects 0.000 claims abstract description 18
- 230000003019 stabilising Effects 0.000 claims abstract description 15
- 239000000758 substrate Substances 0.000 claims abstract description 14
- 229920002522 Wood fibre Polymers 0.000 claims abstract description 12
- 239000010410 layer Substances 0.000 claims description 77
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 239000002344 surface layer Substances 0.000 claims description 14
- 230000000694 effects Effects 0.000 claims description 11
- 229920005989 resin Polymers 0.000 claims description 7
- 239000011347 resin Substances 0.000 claims description 7
- 239000002023 wood Substances 0.000 claims description 3
- -1 or a step of drying Substances 0.000 claims description 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N al2o3 Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 18
- 238000011105 stabilization Methods 0.000 description 15
- 238000003825 pressing Methods 0.000 description 10
- 238000010438 heat treatment Methods 0.000 description 9
- 239000000463 material Substances 0.000 description 8
- 239000002245 particle Substances 0.000 description 8
- 239000007787 solid Substances 0.000 description 8
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 8
- 229920000877 Melamine resin Polymers 0.000 description 7
- 230000035699 permeability Effects 0.000 description 7
- 229910001884 aluminium oxide Inorganic materials 0.000 description 6
- 239000000049 pigment Substances 0.000 description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
- 238000010186 staining Methods 0.000 description 6
- 239000003550 marker Substances 0.000 description 5
- 239000011148 porous material Substances 0.000 description 5
- 239000010438 granite Substances 0.000 description 4
- 229920001187 thermosetting polymer Polymers 0.000 description 4
- 238000007906 compression Methods 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- WSFSSNUMVMOOMR-UHFFFAOYSA-N formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- 238000005470 impregnation Methods 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- 239000004640 Melamine resin Substances 0.000 description 2
- 229920003180 amino resin Polymers 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000006482 condensation reaction Methods 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000011888 foil Substances 0.000 description 2
- 229920005610 lignin Polymers 0.000 description 2
- 239000003586 protic polar solvent Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 230000000087 stabilizing Effects 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000004408 titanium dioxide Substances 0.000 description 2
- 240000005337 Agave sisalana Species 0.000 description 1
- 241000609240 Ambelania acida Species 0.000 description 1
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 240000003917 Bambusa tulda Species 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- 240000000218 Cannabis sativa Species 0.000 description 1
- 229920003043 Cellulose fiber Polymers 0.000 description 1
- 241000229754 Iva xanthiifolia Species 0.000 description 1
- 240000006240 Linum usitatissimum Species 0.000 description 1
- 235000004431 Linum usitatissimum Nutrition 0.000 description 1
- JDSHMPZPIAZGSV-UHFFFAOYSA-N Melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N Silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 239000003082 abrasive agent Substances 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000010905 bagasse Substances 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 235000009120 camo Nutrition 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 235000005607 chanvre indien Nutrition 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- IVJISJACKSSFGE-UHFFFAOYSA-N formaldehyde;1,3,5-triazine-2,4,6-triamine Chemical group O=C.NC1=NC(N)=NC(N)=N1 IVJISJACKSSFGE-UHFFFAOYSA-N 0.000 description 1
- 239000011487 hemp Substances 0.000 description 1
- 235000012765 hemp Nutrition 0.000 description 1
- 239000008240 homogeneous mixture Substances 0.000 description 1
- 239000000976 ink Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- KFZMGEQAYNKOFK-UHFFFAOYSA-N iso-propanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 1
- 238000004020 luminiscence type Methods 0.000 description 1
- 235000012766 marijuana Nutrition 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000011812 mixed powder Substances 0.000 description 1
- 239000012454 non-polar solvent Substances 0.000 description 1
- 229920001568 phenolic resin Polymers 0.000 description 1
- 239000005011 phenolic resin Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 239000003880 polar aprotic solvent Substances 0.000 description 1
- 238000002310 reflectometry Methods 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27N—MANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
- B27N7/00—After-treatment, e.g. reducing swelling or shrinkage, surfacing; Protecting the edges of boards against access of humidity
- B27N7/005—Coating boards, e.g. with a finishing or decorating layer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C43/00—Compression moulding, i.e. applying external pressure to flow the moulding material; Apparatus therefor
- B29C43/32—Component parts, details or accessories; Auxiliary operations
- B29C43/34—Feeding the material to the mould or the compression means
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2227—Oxides; Hydroxides of metals of aluminium
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/36—Silica
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
- C08K7/02—Fibres or whiskers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L97/00—Compositions of lignin-containing materials
- C08L97/02—Lignocellulosic material, e.g. wood, straw or bagasse
Abstract
Dislcosed herein is a method for producing a building panel comprising the steps of: - applying a powder mix layer (2) on a substrate (1), the powder mix layer comprising wood fibres and a binder; - adjusting a weight loss on cure of the powder mix layer by a step of applying a stabilisation fluid (at 4), or a step of drying (5), or a combination thereof such that the powder mix layer obtains the weight loss on cure in a range of about 2 to about 7 wt-%; and - applying heat and pressure (6) to the powder mix layer when arranged on the substrate and curing the powder mix layer having the weight loss on cure in the range of about 2 to about 7 wt-%, and thereby obtaining a layer of the building panel formed by the powder mix layer. (at 4), or a step of drying (5), or a combination thereof such that the powder mix layer obtains the weight loss on cure in a range of about 2 to about 7 wt-%; and - applying heat and pressure (6) to the powder mix layer when arranged on the substrate and curing the powder mix layer having the weight loss on cure in the range of about 2 to about 7 wt-%, and thereby obtaining a layer of the building panel formed by the powder mix layer.
Description
A POWDER MIX AND A METHOD FOR PRODUCING A BUILDING PANEL
Technical fieId
The disclosure generally relates to the field of fibre-based panels with a wear
resistant decorative surface layer, ularly building panels and more particularly
floor panels. The disclosure relates to a building panel with such wear ance
decorative surface and to production methods for such panels and a mixed/prefab
layer for such methods and panels.
Known Technigues
Recently new “paper free” Wood Fibre Floor (WFF) types have been developed
with solid surfaces comprising a substantially homogenous mix of fibres, binders
and wear resistant particles. Such a new type of panel called Wood Fibre Floor
(WFF) is sed in /065769, which shows both products and methods to
produce such a product.
The wear resistant particles are preferably aluminium oxide particles, the binders
are preferably thermosetting resins such as amino resins and the fibres are
preferably wood based. Other suitable wear resistant materials are for example
silica or silicon carbide. In most applications decorative les such as for
example colour pigments are included in the homogenous mix. In general all these
materials are preferably applied in dry form as a mixed powder on a HDF core and
cured under heat and pressure to a 0.1 - 1.0 mm solid layer.
Powder technology is very suitable to produce solid decorative surface layer, which
are much thicker than conventional laminate surface layers. Such solid powder
based layers create a much higher tension on the panel when they swell or shrink
and balancing is a problem. It is ore ult to produce a panel with a thick
and a high quality surface, which is also stable and flat in variable moisture
conditions. rmore, pores may be formed in the surface layer resulting in weak
stain resistance.
Summary of the ion
An objective of certain embodiments of the invention is to improve the known Wood
Fibre Floor (WFF) panels. A r object is to provide a product preferably having
a width cupping of —O.15% to +0.20% under test conditions according to ISO
24339:2006(E), and/or a water vapour permeability of less than 3 g/m2*24 hours
according to EN 12572 and/or a e staining of 5(5) according to EN438 based on
test using a ent marker. The foregoing objects should be read disjunctively with
the object of at least ing the public with a useful alternative.
This may be achieved by a powder mix layer for the tive surface layer of a WFF-
panel with a controlled loss on cure and a method of producing a building panel.
By loss on cure is in this application meant the weight loss, calculated as weight
percentage of the original weight, occurring when heating the powder at 160°C for 5
minutes. The weight loss corresponds to re released from the powder. Under
these conditions the released moisture consists of two parts. The first part is the free
moisture formed from water and/or other substances having a boiling point below
160°C being trapped in the powder and the second part origins from the cross linking of
the binder. Melamine formaldehyde resin cures at 160°C and the resin cross-links via a
condensation reaction, i.e. water is released by the condensation reaction.
By moisture content is meant the weight loss, when the powder is dried under milder
conditions at ambient atures and only the free water in the powder is released,
without curing the resin.
If the loss on cure is too low the powder mix layer will not be completely impregnated
by the binder when the binder is in the fluid state during the pressing. An inferior
impregnation of the powder mix layer results in discolouration of the tive surface
of the WFF panel, due to pores close to the surface.
If the loss on cure on the other hand is too high, a high amount of pores in the WFF
layer are created during the pressing. The pores give a poor resistance of surface
staining and increased water/vapour permeability. Increased water/vapour permeability
can result in increased cupping of the panels under test conditions according to lSO
24339:2006(E).
The loss on cure depends on the amount of binder in the powder mix layer, the
moisture content in the powder mix layer when entering the WFF production line and
the amount of powder stabilization fluid d in the WFF production line. The loss on
cure before pressing may be controlled by an in-Iine or off—line drying process in which
the powder layer is dried. The drying may be carried out by heating, e.g., lR heating,
preferably in-line, drying in a chamber, preferably in-line, or drying in a controlled
climate, preferably off-line.
The drying process stabilizes the powder in the powder mix layer and applying a powder
ization fluid may not be necessary.
If the drying process es heating, the binder in the powder mix layer may be melted
and the powder is stabilized by the melted binder. Thereby, the drying process may make
the stabilization fluid redundant.
According to a first aspect of the invention a powder mix layer for producing a building
panel with a loss on cure in the range of about 2.5 to about 7 wt-%, preferably about 3 to
about 6 wt-% is provided.
A powder mix layer having a loss on cure in the above described range overcomes the
above described disadvantages and exhibits improved stain resistance, water/vapour
ance and binder impregnation as described above.
The powder mix layer may have a loss on cure in the range of about 2 to about 7 wt—%,
preferably in the range of about 4 to about 6 wt-%, preferably about 5 wt-%.
The powder mix is a substantially homogenous mix, which comprises in one embodiment
wood fibres, preferably of HDF, a binder, preferably a melamine resin, and wear resistant
particles, ably a powder of silica, more preferably essentially of aluminium oxide. A
more preferred loss on cure is about 3.5 wt-%, to 5.5 wt-%.
According to a second aspect of the invention, a method of producing a building panel is
provided. The method comprises the steps of:
- applying a powder mix layer on a ate, the powder mix layer sing wood fibres
and a ;
- adjusting a weight loss on cure of the powder mix layer by a step of applying a
stabilisation fluid, or a step of drying, or a combination thereof such that the powder mix
layer obtains the weight loss on cure in a range of about 2 to about 7 wt—%; and
- applying heat and pressure to the powder mix layer when arranged on the ate and
curing the powder mix layer having the weight loss on cure in the range of about 2 to about
7 wt-%, and thereby obtaining a layer of the building panel formed by the powder mix layer.
Preferred weight loss on cure ranges are about 4 to about 6 wt—%, about 5 wt—% and about
2.5 wt—% to about 7 wt-%.
A powder mix layer produced according to the ive method wherein the powder mix
layer has a loss on cure in the above described range overcomes the above described
disadvantages and exhibits improved stain resistance, water/vapour resistance and binder
impregnation as described above.
In one embodiment, a powder mix is chosen such that the powder mix already has a loss
on cure in the above defined ranged. As an alternative, the loss on cure of
WC 2012/141646
the powder mix layer may be adjusted by for e applying a stabilisation fluid
or by drying in order to change the moisture content of the powder mix. The
relevant time for determining the loss on cure of the powder mix layer is the
moment before applying heat and pressure.
By adjusting the binder content and the re content in the powder mix, and the
amount of any added ization fluid, a desired loss on cure of the powder mix
layer may be obtained. Furthermore, the loss on cure may be controlled by drying
the mix, thereby adjusting the moisture content.
The curing performed by applying heat and pressure may be performed at high line
speed and the powder layer withstands high acceleration and retardation forces
created, at short press cycles of about 20 seconds.
The powder mix in the second aspect may be the same as the embodiments of the
first aspect. ingly, the powder mix layer may comprise a substantially
homogenous mix of wood fibres and a binder, preferably a thermosetting resin,
more preferably melamine. The powder mix layer may further comprise wear
ant particles, preferably of aluminium oxide or of a silica powder.
The loss on cure is measured using a gravimetric method comprising heating the
powder mix layer at 160°C for five s.
The powder mix layer may be heated before pressing, preferably by lR heating, and
preferably with an effect of about 15-25 kW/m. A preferred g speed in the
range of about 1-4 m/min, most preferably about 3m/min at an effect of about 20kw.
Preferably, the substantially homogenous mix is ioned before being applied in
order to obtain the desired loss on cure of the powder mix layer.
In the curing step, the pressure applied may be in the range of about 20 kg/cm2 to
about 60 kg/cmz, preferably about 40 kg/cmz, and the temperature of the press
plate may be in the range of about 160 to about 200°C, preferably about 180°C,
The heat and pressure may be applied in the range of about 10 to about 200
seconds, preferably in the range of about 10—60 seconds, and as an example in
about 40 seconds.
The powder mix layer may comprise wood fibres and a binder, preferably a
thermosetting resin.
2012/050384
The method may comprise the further step of applying a stabilisation fluid,
preferably water, on the powder mix.
The method may comprise the further step of drying the powder mix layer,
preferably by applying heat with an effect of about 15-25 kW/m and a g speed
in the range of about 1—4 m/min, preferably about 3 m/min.
The method may comprise the further steps of fixing the powder mix layer to the
ate, preferably by applying stabilisation fluid and drying with an effect of about
—25 kW/m and a feeding speed in the range of about 1-4 m/min, preferably about
3 m/min.
The method may comprise the further step of adjusting the loss on cure of the
powder mix layer by the step of applying the stabilisation fluid, or the step of drying,
or a combination thereof such that the powder mix layer obtains the loss on cure in
said range. Thereby, the loss on cure of the powder mix layer can be adjusted such
that a loss on cure in the desired range can be obtained, even if the powder mix
originally has a loss on cure outside the desired range.
The powder mix layer may be applied by scattering. The powder mix may be
applied by an applying unit, preferably a scattering unit, which forms the powder
mix layer.
The powder mix layer may be applied as a continuous powder mix sheet.
Consequently, it is possible to produce a separate layer such as a uous
powder mix sheet. In this embodiment, the substrate may be a press belt, a release
foil etc. The components of the powder mix is connected er but essentially
uncured, in a te process and in a separate production line. The separate
layer may be based on carrier, e.g. a paper or a metal or plastic foil, but the powder
mix may also only be bonded together by it self achieved by e.g. g with a
fluid, preferably water and drying. The powder mix sheet may be stored and later
applied on the core as a powder mix layer.
The substrate may be a core, preferably a wood-based core, more preferably a
HDF or MDF board.
The layer may form a decorative surface layer arranged on the core.
A third aspect of the invention is a production line comprising an ng unit for
applying a powder mix layer on a substrate, a pressing unit for applying heat and
W0 2012/141646
pressure on the powder mix layer and a conveyor that comprises conveyor units
preferably with separately controllable feeding speed of the substrate. The
tion line may also se stabilisation units and/or drying units. The
conveyor preferably ses separate or units at each of the production
units. The separate conveyor units provide an enhanced control of the loss on cure,
since the feeding speed at each production unit (the applying unit, stabilisation unit
and/or drying unit) can be controlled and thereby it will be easier to control the
amount of applied powder or stabilisation unit or degree of drying. Furthermore the
separate or units prevent moisture/water from being transported between
the production units by the conveyor .
In all s the wood fibres may be both virgin, refined and/or processed,
sing lignin and without lignin, e.g. or-cellulose fibres or holocellulose. A
mixture of refined and unrefined fibres may also be used. It is also contemplated
that vegetable fibres asjute, linen, flax, , hemp, bamboo, bagasse and sisal
may be used. Also mineral fibres and carbon fibres may be used.
The applying unit is preferably a scattering device. The substrate is preferably an
HDF or MDF board, which is preferably provided with a balancing layer .
Brief Description of the Drawings
The invention will in the following be described in connection to preferred
embodiments and in greater detail with reference to the appended ary
drawings, wherein
Fig 1 illustrates a production line ing to an embodiment of the
invention;
Fig 2 illustrates a panel with a decorative layer according to an
embodiment of the invention;
Fig 3 illustrate the relationship between moisture content and loss on
cure for the formulation in e 1-4
Detailed Description of Embodiments
A panel 7, which is described with reference to fig 1 and 2, comprises according to
one embodiment of the invention a wood fibre based core 1, an essentially
homogenous decorative surface layer (transparent or non-transparent) 2 and
preferably a balancing layer 8. The panel 7 is in one embodiment integrally formed
in a production line (see fig 1) where the surface layer 2, the core 7 and the
balancing layer 8 are formed in the same pressing operation 6.
Figure 2 shows the decorative surface layer and the core in more detail. The
surface layer ses a substantially homogenous mixture of fibres 14, small
hard wear resistant particles 12, 12’ and a binder 19. The fibres 14 are ably
wood fibres. The binder 19 is preferably a binder that cross-links by a condensation
on. The binder is preferably a thermosetting resin such as amino-resins or
phenolic resin. In one embodiment, the binder is melamine formaldehyde. The wear
resistant particles 12,12’ are preferably aluminium oxide particles. The surface layer
preferably may also comprise pigment 15.
The e layer may comprise colour pigments 15 , optionally, other
decorative materials or chemicals. tive materials include, for example,
materials that may affect design aspect(s) the surface layer. Exemplary design
materials include materials effecting texture, reflectivity, shine, luminescence,
transparency, etc.
In methods according to embodiments of the invention preferably the same
scattering 3 and pressing units 6 as disclosed in or WO
2009/124704 are used, ably together with a structured press plate in the
method. Each of and are hereby incorporated
2O by reference in its entirety.
Fig 1 discloses a production line according to an embodiment of the invention. The
production line comprises an applying unit 3, preferably a scattering unit for
applying/scattering a powder mix 2 on the core 1, e.g. an HDF/MDF board, which is
ably already provided with a balancing layer 8. A stabilisation unit 4 for
applying a stabilization fluid and a drying unit 5 for drying the powder mix layer are
provided. A pressing unit 6 finally s heat and re on the powder mix
layer, the core and the balancing layer in order to cure the binder and thereby
obtaining the finished building panel 7 with a decorative surface layer. The
production line further comprises a conveyor (not shown) preferably sing
separate conveyor units such that the speed of the core 1 through the production
line can be varied at the ent units e.g. at the applying unit 3, the stabilisation
unit 4 or at the drying unit 5. A suitable conveyor is a belt or roller conveyor.
A powder formulation can for example se an essentially homogenous
W0 41646 2012/050384
powder mixture comprising 187.5 g/m2 recycled HDF fibre with a moisture content
of 5.2 %, 62.5 g/m2 Aluminium Oxide (ZWSK-180 ST, Treibacher Schleifmittel AG),
265,625 g/m2 Melamine Formaldehyde resin (Prefere 4865, Dynea), 62.5 g/m2
Titanium dioxide (Kronos 2190, Kronos) and 46,875 g/m2 pigment (Heucosin
G10512, Heubach).
The core of an HDF board preferably has a moisture content of 0-6 %.
The ring unit has the capacity of scattering of 100-1000 g/m2 with a tolerance
of +/- 5% as measured using a calibration cup with an area of 100x100 mm cross-
and length wise the board. The amount of stabilization fluid may vary between 0 up
to 200 g/m2.
The scattering unit comprises a needle belt and a scattering roller. The scattering
roller is provided with needles in the range of about , preferably about 50-
100, and most preferably about 70—90 needles per cmz. The needle length is about
0.5-2.5 mm, preferably about 1—2 mm and most ably about 1.5 mm. Several
ring units machines to even out differences in the applied powder mixture.
Furthermore, the scattering device may be provided with a needle belt with s
with a preferred length of about 15—20 mm, a preferred frequency in the range of
about 500—1000 rpm preferably about 1000 rpm, and a stroke length of about +/- 3
The stabilization unit may stabilize using steam, nozzle spray coating, ultra sonic
spray coating, a stabilization sheet comprising a sheet based material with inherent
stabilizing properties or a surface coverage providing the stabilizing properties.
Stabilization fluid may comprise solvents such as non-polar solvents, polar aprotic
solvents and polar protic solvents or es thereof. red solvents are polar
protic solvents such as isopropanol, ethanol and water. Most preferred is water.
The stabilization fluid can further comprise additives such as wetting agents,
ers, release agents, anti-slip agents, anti-abrasives and catalysts.
tive effects can also be added in the form of inks, dyes and effect pigments.
ln examples 1-4 below the powder formulation was used comprising 34 weight-%
recycled HDF fibre (valinge innovation ), 10 weight—% Aluminium oxide
(ZWSK 180-ST, cher Schleifmittel AG), 50 weight—% Melamine
Formaldehyde resin (Prefere 4865, Dynea), 2 weight-% Titanium dioxide (Kronos
WO 41646
2190, Kronos) and 4 weight—% pigment (G 6555 N, Heubach GmbH).
The relation between Weight Loss on Cure and the free moisture content, that is
excluding the water released in the curing of the melamine resin, in the powders
used in the examples, is shown in fig 3.
Depending on the loss cure of the powder mix applied to the substrate, a
stabilization fluid may be applied and/or drying may be performed. if the loss on
cure of the powder mix applied to the substrate is within the above described range,
no stabilization fluid is to be added and no drying is to be performed. If the loss on
cure of the powder mix applied to the ate is outside the above described
range, a ization fluid is to be added, or drying is to be performed, depending if
the loss on cure is too low or too high, in order to obtain a powder mix having the
desired loss on cure before applying heat and pressure.
Even if the loss on cure of the powder mix d is within the above described
range, it may be desired to apply a stabilization fluid in order to stabilize the powder
layer. In order to adjust the loss on cure of the powder mix layer, subsequent drying
may be required.
Alternatively, the binder content of the powder may also be adjusted in order to
obtain the desired loss on cure of the powder mix layer.
Example 1: Powder based product obtained through heat compression of an
incorrectly treated powder, ative example; no drying and a stabilization fluid
of water (ZOg/mz)
A powder based product comprising an HDF core with a thickness of 9.7 mm, a
balancing paper 550 g/m2 of a scattered powder layer and 20 g/m2 isation
fluid, giving an a loss on cure of 8 wt-%, was pressed in a short cycle press using a
force of 40 kg/cm2 for 37 seconds at a surface temperature on the upper press
plate of 184 °C and a surface temperature on the lower press plate of 180 °C. The
press plate was a granite structure plate.
The resulting product was:
o a building panel with a solid surface having a width cupping outside -O.15 %
to +02% led board according to lSO 24339:2006(E). Typical values
obtained are -O.26 % to +0.29%.
. staining of 3(5) according to EN438 based on test using a permanent marker
. water vapour permeability in excess of 5.3 g/m2*24 hours according to EN
12572
Example 2: Powder based product obtained through heat ssion of a treated
, preferred example, drying and a stabilization fluid of water (20g/m2)
A powder based product comprising a HDF core with a thickness of 9.7 mm, a
balancing paper and 550 g/m2 of a scattered powder layer and 20 g/m2 of
isation fluid was pressed in a short cycle press using a force of 40 kg/cm2 for
37 seconds at a surface ature on the upper press plate of 184 °C and a
surface temperature on the lower press plate of 180 °C. The press plate had a
granite structure. Prior to pressing the powder was treated by an IR drying with an
effect of 19 kW/m and a g speed of 27 m/min in order to obtain a loss on
cure of 4.6 wt-% as measured using a gravimetric method comprising heating the
treated powder at 160 °C for five minutes.
The ing product was:
0 a solid surface having a width cupping within -0.15 % to +02 % installed
board according to ISO 24339:2006(E), typical values obtained are -0.07 %
to +0.17 %.
. staining of 5(5) according to EN438 based on test using a permanent marker
. water vapour permeability lower than 1.1 g/m2*24 hours according to EN
12572.
Example 3: Powder based product obtained h heat compression of an
incorrectly treated powder, comparative example, stabilization fluid and over drying.
A powder based product comprising a HDF core with a thickness of 9.7 mm, a
balancing paper and 550 g/m2 of a scattered powder layer with 20 g/m2 of
stabilisation fluid, was pressed in a short cycle press using a force of 40 kg/cm2 for
37 seconds at a surface temperature on the upper press plate of 184°C and a
surface temperature on the lower press plate of 180°C. The press plate had a
granite structure. Prior to ng the powder was treated by an lR drying process
with an effect of 19 kW/m and a feeding speed of 1.5 m/min in order to obtain a loss
on cure of 2.5 wt-% as measured using a gravimetric method comprising heating
the treated powder at 160°C for five s.
The resulting product was:
W0 2012/141646
. a building panel with a solid surface having a width cupping inside -O.15 %
to +0.2 % on installed board according to ISO 2433912006(E)
o staining of 3(5) according to EN438 based on test using a permanent marker
0 water vapour permeability of 2.5 g/m2*24 hours according to EN 12572
. Discoloured decorative surface, due pores close to surface.
Example 4: Powder based product obtained through heat compression of a treated
powder, red example, drying and without stabilization fluid of water.
A powder based product sing a HDF core with a thickness of 9.7 mm, a
balancing paper and 550 g/m2 of a red powder layer, with a loss on cure of
5.3 % before drying, was pressed in a short cycle press using a force of 40 kg/cm2
for 37 seconds at a e temperature on the upper press plate of 184 °C and a
surface temperature on the lower press plate of 180 °C. The press plate had a
granite structure. Prior to pressing the powder was treated by an IR drying with an
effect of 19 kW/m and a feeding speed of 2.7 m/min in order to obtain a loss on
cure of 3.7 wt-% as measured using a etric method comprising heating the
treated at 160 °C for five minutes.
The resulting product was:
. A solid surface having a width cupping within —O.15 % to +0.2 % on the
installed board ing to ISO 24339:2OOG(E), typical values obtained are
-0.05 % to +020 %.
o staining of 5(5) according to EN438 based on test using a permanent marker
. water vapour permeability lower than 1.9 g/m2*24 hours according to EN
12572.
Claims (17)
1. A method of producing a building panel comprising the steps of: - applying a powder mix layer on a substrate, the powder mix layer comprising wood fibres and a binder; - adjusting a weight loss on cure of the powder mix layer by a step of applying a stabilisation fluid, or a step of drying, or a combination thereof such that the powder mix layer obtains the weight loss on cure in a range of about 2 to about 7 wt-%; and 10 - applying heat and pressure to the powder mix layer when arranged on the substrate and curing the powder mix layer having the weight loss on cure in the range of about 2 to about 7 wt—%, and thereby obtaining a layer of the building panel formed by the powder mix layer. 15
2. The method according to claim 1, wherein the weight loss on cure is in the range of about 4 to about 6 wt—%.
3. The method according to claim 1 or 2, n the weight loss on cure is about 5 wt-%.
4. The method ing to any one of claims 1—3, wherein the binder is a setting resin. 25
5. The method according to any one of claims 1-4, wherein the stabilisation fluid is water.
6. The method according to any one of claims 1-5, wherein the step of 30 drying comprises applying heat with an effect of about 15-25 kW/m and a feeding speed in the range of about 1—4 m/min.
7. The method ing to any one of claims 1-6, comprising the further steps of fixing the powder mix layer to the substrate.
8. The method according to claim 7, wherein the step of fixing comprises applying stabilisation fluid and drying with an effect of about 15—25 kW/m and a feeding speed in the range of about 1-4 m/min.
9. The method according to claim 6 or 8, wherein the feeding speed is about 3 m/min.
10. The method according to any one of claims 1-9, wherein the powder mix layer is applied by scattering.
11. The method according to any one of claims 1-10, wherein the powder mix layer is applied as a continuous powder mix sheet.
12. The method according to any one of claims 1-11, wherein the substrate is a core.
13. The method according to claim 12, n the core is a wood-based 15 core.
14. The method according to claim 12 or 13, wherein the core is a HDF or MDF board. 20
15. The method according to any one of claims 12-14, wherein the layer forms a decorative surface layer arranged on the core.
16. A building panel ed by the method according to any one of claims 1-15.
17. The method according to claim 1, substantially as herein bed with reference to any one of the Examples and/or
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161474485P | 2011-04-12 | 2011-04-12 | |
US61/474,485 | 2011-04-12 | ||
SE1150321 | 2011-04-12 | ||
SE1150321-6 | 2011-04-12 | ||
PCT/SE2012/050384 WO2012141646A1 (en) | 2011-04-12 | 2012-04-11 | A powder mix and a method for producing a building panel |
Publications (2)
Publication Number | Publication Date |
---|---|
NZ615297A NZ615297A (en) | 2015-09-25 |
NZ615297B2 true NZ615297B2 (en) | 2016-01-06 |
Family
ID=
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