NZ613736B2 - Synergistic herbicidal composition containing penoxsulam and glyphosate - Google Patents
Synergistic herbicidal composition containing penoxsulam and glyphosate Download PDFInfo
- Publication number
- NZ613736B2 NZ613736B2 NZ613736A NZ61373612A NZ613736B2 NZ 613736 B2 NZ613736 B2 NZ 613736B2 NZ 613736 A NZ613736 A NZ 613736A NZ 61373612 A NZ61373612 A NZ 61373612A NZ 613736 B2 NZ613736 B2 NZ 613736B2
- Authority
- NZ
- New Zealand
- Prior art keywords
- glyphosate
- penoxsulam
- synergistic
- herbicidal
- vegetation
- Prior art date
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- 239000000203 mixture Substances 0.000 title claims abstract description 65
- 230000002195 synergetic Effects 0.000 title claims abstract description 25
- 239000005592 Penoxsulam Substances 0.000 title claims abstract description 22
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- 239000005562 Glyphosate Substances 0.000 title claims abstract description 21
- 229940097068 glyphosate Drugs 0.000 title claims abstract description 21
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- 239000004328 sodium tetraborate Substances 0.000 description 1
- 235000010339 sodium tetraborate Nutrition 0.000 description 1
- KZOJQMWTKJDSQJ-UHFFFAOYSA-M sodium;2,3-dibutylnaphthalene-1-sulfonate Chemical compound [Na+].C1=CC=C2C(S([O-])(=O)=O)=C(CCCC)C(CCCC)=CC2=C1 KZOJQMWTKJDSQJ-UHFFFAOYSA-M 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 235000012424 soybean oil Nutrition 0.000 description 1
- 239000003549 soybean oil Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000007619 statistical method Methods 0.000 description 1
- 239000011550 stock solution Substances 0.000 description 1
- 230000000153 supplemental Effects 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
- RJKCKKDSSSRYCB-UHFFFAOYSA-N tebutam Chemical compound CC(C)(C)C(=O)N(C(C)C)CC1=CC=CC=C1 RJKCKKDSSSRYCB-UHFFFAOYSA-N 0.000 description 1
- BCQMBFHBDZVHKU-UHFFFAOYSA-N terbumeton Chemical compound CCNC1=NC(NC(C)(C)C)=NC(OC)=N1 BCQMBFHBDZVHKU-UHFFFAOYSA-N 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- BQZXUHDXIARLEO-UHFFFAOYSA-N tribenuron Chemical compound COC1=NC(C)=NC(N(C)C(=O)NS(=O)(=O)C=2C(=CC=CC=2)C(O)=O)=N1 BQZXUHDXIARLEO-UHFFFAOYSA-N 0.000 description 1
- 229940087291 tridecyl alcohol Drugs 0.000 description 1
- 125000002889 tridecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000002023 trifluoromethyl group Chemical group FC(F)(F)* 0.000 description 1
- PIHCREFCPDWIPY-UHFFFAOYSA-N tris[2-(2,4-dichlorophenoxy)ethyl] phosphite Chemical compound ClC1=CC(Cl)=CC=C1OCCOP(OCCOC=1C(=CC(Cl)=CC=1)Cl)OCCOC1=CC=C(Cl)C=C1Cl PIHCREFCPDWIPY-UHFFFAOYSA-N 0.000 description 1
- KVEQCVKVIFQSGC-UHFFFAOYSA-N tritosulfuron Chemical compound FC(F)(F)C1=NC(OC)=NC(NC(=O)NS(=O)(=O)C=2C(=CC=CC=2)C(F)(F)F)=N1 KVEQCVKVIFQSGC-UHFFFAOYSA-N 0.000 description 1
- 239000002383 tung oil Substances 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 235000020234 walnut Nutrition 0.000 description 1
- 239000004562 water dispersible granule Substances 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 235000021307 wheat Nutrition 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
- A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
Abstract
The disclosure relates to a synergistic mixture of penoxsulam and glyphosate for controlling weeds in crops, especially vines, range and pasture, industrial vegetation management, rights of way and in any glyphosate tolerant crop, wherein the weight ratio of glyphosate to penoxsulam is from 4:1 to 448:1. 48:1.
Description
W0 2012/106566
SYNERGISTIC HERBICIDAL COMPOSITION CONTAINING PENOXSULAM AND
GLYPHOSATE
This invention concerns a synergistic idal composition containing (a)
penoxsulam and (b) sate for controlling the growth of undesirable vegetation,
ally in vines, range and pasture, industrial vegetation management, rights of way and in
any glyphosate tolerant crop. These compositions are disclosed as providing improved post-
emergence herbicidal weed control.
The protection of crops from weeds and other vegetation which inhibit crop growth is
a constantly recurring problem in agriculture. To help combat this problem, researchers in
the field of synthetic chemistry have produced an extensive variety of chemicals and
chemical formulations effective in the control of such unwanted growth. Chemical
ides of many types have been disclosed in the literature and a large number are in
commercial use.
In some cases, herbicidal active ingredients have been shown to be more effective in
combination than when applied individually and this is referred to as “synergism.” As
described in the Herbicide ok of the Weed Science Society of America, Ninth
Edition, 2007, p. 429 “‘synergism’ [is] an ction of two or more factors such that the
effect when combined is greater than the predicted effect based on the response to each factor
applied separately.” The present invention is based on the discovery that penoxsulam and
glyphosate, already known individually for their herbicidal cy, display a synergistic
effect when d in ation.
The present invention concerns a synergistic herbicidal mixture comprising an
herbicidally effective amount of (a) penoxsulam and (b) glyphosate. The compositions may
also contain an agriculturally acceptable adjuvant and/or carrier.
The present invention also concerns herbicidal compositions for and s of
controlling the growth of undesirable vegetation, particularly in range and pasture, industrial
vegetation management, rights of way and in any glyphosate nt crop, and the use of
these synergistic compositions.
W0 06566
The species spectra of penoxsulam and glyphosate, i.e., the weed species which the
respective compounds control, are broad and highly complementary. It has now been found
that a combination of penoxsulam and glyphosate exhibits a istic action in the control
broadleaf signalgrass (Brachiaria platyphylla, BRAPP), yellow nutsedge (Cypems
esculentus, CYPES), barnyardgrass (Echinochloa crus-galli, ECHCG), momingglory
(Ipomoea, hederacea, IPOHE), Chinese sprangletop (Leptochloa chinensis, LEFCH) ryegrass
(Lolium spp, LOLSS), scented mayweed (Matricaria chamomilla, MATCH), and annual
bluegrass (Poa annua, POAAN) at application rates equal to or lower than the rates of the
individual compounds.
Penoxsulam is the common name for 2-(2,2-difluoroethoxy)-N—(5,8-dimethoxy-
[l,2,4]triazolo[1,5-c]pyrimidinyl)(trifluoromethyl)benzenesulfonamide. Its herbicidal
activity is described in The Pesticide , Fifteenth Edition, 2009. Penoxsulam controls
Echinochloa spp., as well as many broadleaf, sedge and aquatic weeds in rice, and Apera spp.
grass in cereals, as well as many broadleaf weeds in aquatics, many cereal crops, range and
pasture, IVM and turf.
sate, N-(phosphonomethyl)glycine is a EPSP synthase tor. Its herbicidal
ty is bed in The Pesticide Manual, Fifteenth Edition, 2009. Glyphosate provides
non-selective post-emergence weed control.
The term herbicide is used herein to mean an active ingredient that kills, controls or
otherwise adversely modifies the growth of . An idally effective or vegetation-
controlling amount is an amount of active ient which causes an adversely modifying
effect and includes deviations from natural development, killing, regulation, desiccation,
retardation, and the like. The terms plants and vegetation include germinant seeds, emerging
seedlings, plants emerging from tive ules, and established vegetation.
Herbicidal activity is exhibited by the nds of the synergistic mixture when
they are applied directly to the plant or to the locus of the plant at any stage of growth. The
effect observed depends upon the plant species to be controlled, the stage of growth of the
plant, the application parameters of dilution and spray drop size, the particle size of solid
components, the environmental conditions at the time of use, the specific compound
employed, the specific adjuvants and carriers employed, the soil type, and the like, as well as
the amount of chemical applied. These and other factors can be adjusted as is known in the
W0 06566
art to promote non-selective or selective herbicidal action. Generally, it is preferred to apply
the ition of the present invention postemergence to relatively immature undesirable
vegetation to achieve the maximum control of weeds.
In the composition of this ion, the weight ratio of glyphosate to penoxsulam at
which the herbicidal effect is synergistic lies within the range from 3:2 to 896:1, preferably
from 4:1 to 448:1. The rate at which the synergistic composition is applied will depend
upon the particular type of weed to be controlled, the degree of control required, and the
timing and method of application. In general, the ition of the invention can be
applied at an application rate from 112.5 grams of active ingredient per e (gai/ha) to
2310 gai/ha based on the total amount of active ingredients in the composition. Penoxsulam
is applied at a rate from 2.5 g/ha to 70 g/ha and glyphosate is applied at a rate from 110
g/ha to 2240 g/ha.
The components of the synergistic mixture of the present invention can be applied
either separately or as part of a multipart idal system.
The synergistic mixture of the present invention can be applied in conjunction with
one or more other herbicides to control a wider variety of undesirable vegetation. When used
in conjunction with other herbicides, the composition can be formulated with the other
herbicide or herbicides, tank-mixed with the other herbicide or herbicides or applied
sequentially with the other herbicide or herbicides. Some of the herbicides that can be
employed in conjunction with the synergistic composition of the present invention include: 4-
CPA; 4-CPB; 4-CPP; 2,4-D; 3,4-DA; 2,4-DB; 3,4-DB; 2,4-DEB; 2,4-DEP; 3,4-DP; 2,3,6-
TBA; 2,4,5-T; 2,4,5-TB; acetochlor, acifluorfen, aclonifen, acrolein, alachlor, chlor,
alloxydim, allyl alcohol, alorac, ametridione, ametryn, amibuzin, bazone,
amidosulfuron, aminocyclopyrachlor, aminopyralid, amiprofos-methyl, amitrole, ammonium
sulfamate, anilofos, on, asulam, atraton, atrazine, azafenidin, azimsulfuron, aziprotryne,
barban, BCPC, beflubutamid, benazolin, bencarbazone, benfluralin, benfuresate, bensulfuron,
bensulide, bentazone, benzadox, benzfendizone, benzipram, benzobicyclon, benzofenap,
benzofluor, benzoylprop, benzthiazuron, bicyclopyrone, x, bilanafos, bispyribac,
borax, bromacil, bromobonil, bromobutide, bromofenoxim, bromoxynil, brompyrazon,
butachlor, nacil, fos, butenachlor, buthidazole, buthiuron, butralin, ydim,
n, butylate, cacodylic acid, trole, calcium chlorate, calcium ide,
cambendichlor, carbasulam, carbetamide, carboxazole chlorprocarb, carfentrazone, CDEA,
W0 2012/106566
CEPC, thoxyfen, chloramben, chloranocryl, chlorazifop, chlorazine, chlorbromuron,
chlorbufam, chloreturon, chlorfenac, chlorfenprop, chlorflurazole, chlorflurenol, chloridazon,
chlorimuron, chlomitrofen, chloropon, chlorotoluron, xuron, chloroxynil,
chlorpropham, chlorsulfuron, chlorthal, chlorthiamid, cinidon-ethyl, cinmethylin,
cinosulfuron, cisanilide, dim, cliodinate, clodinafop, clofop, clomazone, clomeprop,
p, cloproxydim, clopyralid, cloransulam, CMA, copper sulfate, CPMF, CPPC,
credazine, cresol, cumyluron, ryn, cyanazine, cycloate, cyclosulfamuron, cycloxydim,
cycluron, cyhalofop, cyperquat, cyprazine, cyprazole, cypromid, daimuron, dalapon,
dazomet, delachlor, desmedipham, desmetryn, di-allate, dicamba, dichlobenil, ralurea,
dichlormate, dichlorprop, dichlorprop—P, diclofop, diclosulam, diethamquat, diethatyl,
difenopenten, difenoxuron, difenzoquat, diflufenican, diflufenzopyr, dimefuron,
dimepiperate, achlor, dimethametryn, dimethenamid, dimethenamid-P, no,
zon, dinitramine, dinofenate, dinoprop, dinosam, dinoseb, rb, diphenamid,
dipropetryn, diquat, disul, dithiopyr, diuron, DMPA, DNOC, DSMA, EBEP, eglinazine,
endothal, epronaz, EPTC, erbon, esprocarb, ethalfluralin, ethametsulfuron, muron,
ethiolate, ethofumesate, ethoxyfen, ethoxysulfuron, etinofen, etnipromid, etobenzanid, EXD,
fenasulam, fenoprop, fenoxaprop, prop—P, fenoxasulfone, fenteracol, fenthiaprop,
fentrazamide, fenuron, ferrous sulfate, flamprop, flamprop—M, flazasulfuron, lam,
fluazifop, fluazifop-P, fluazolate, flucarbazone, flucetosulfuron, fluchloralin, cet,
flufenican, flufenpyr, ulam, n, flumiclorac, flumioxazin, flumipropyn,
fluometuron, fluorodifen, fluoroglycofen, fluoromidine, fluoronitrofen, fluothiuron,
flupoxam, flupropacil, flupropanate, flupyrsulfuron, fluridone, flurochloridone, fluroxypyr,
flurtamone, fluthiacet, fomesafen, foramsulfuron, fosamine, furyloxyfen, glufosinate,
glufosinate-P, fen, halosulfuron, haloxydine, haloxyfop, haloxyfop—P,
hexachloroacetone, hexaflurate, hexazinone, imazamethabenz, imazamox, imazapic,
imazapyr, imazaquin, imazethapyr, imazosulfuron, indanofan, indaziflam, iodobonil,
iodomethane, iodosulfuron, ioxynil, ipazine, ipfencarbazone, iprymidam, isocarbamid, isocil,
isomethiozin, isonoruron, isopolinate, palin, isoproturon, isouron, en,
isoxachlortole, isoxaflutole, isoxapyrifop, ilate, ketospiradox, lactofen, lenacil, linuron,
MAA, MAMA, MCPA, MCPA-thioethyl, MCPB, mecoprop, mecoprop-P, terb,
mefenacet, mefluidide, mesoprazine, mesosulfuron, mesotrione, metam, metamifop,
metamitron, metazachlor, metazosulfuron, metflurazon, methabenzthiazuron, methalpropalin,
methazole, methiobencarb, methiozolin, methiuron, methometon, methoprotryne, methyl
bromide, methyl isothiocyanate, methyldymron, metobenzuron, omuron, metolachlor,
W0 2012/106566
metosulam, metoxuron, metribuzin, metsulfuron, molinate, monalide, monisouron,
monochloroacetic acid, monolinuron, monuron, morfamquat, MSMA, naproanilide,
napropamide, am, neburon, nicosulfuron, nipyraclofen, nitralin, nitrofen, nitrofluorfen,
norflurazon, noruron, OCH, orbencarb, ortho-dichlorobenzene, orthosulfamuron, in,
oxadiargyl, oxadiazon, oxapyrazon, oxasulfuron, oxaziclomefone, oxyfluorfen, parafluron,
paraquat, pebulate, pelargonic acid, pendimethalin, pentachlorophenol, ochlor,
pentoxazone, done, pethoxamid, phenisopham, phenmedipham, phenmedipham-ethyl,
phenobenzuron, phenylmercury acetate, picloram, nafen, pinoxaden, piperophos,
potassium arsenite, ium azide, potassium cyanate, pretilachlor, primisulfuron,
procyazine, prodiamine, profluazol, profluralin, profoxydim, proglinazine, prometon,
prometryn, propachlor, propanil, propaquizafop, propazine, propham, propisochlor,
propoxycarbazone, propyrisulfuron, propyzamide, prosulfalin, prosulfocarb, prosulfuron,
proxan, prynachlor, pydanon, pyraclonil, pyraflufen, pyrasulfotole, pyrazolynate,
pyrazosulfuron, pyrazoxyfen, pyribenzoxim, pyributicarb, pyriclor, pyridafol, pyridate,
pyriftalid, pyriminobac, pyrimisulfan, pyrithiobac, pyroxasulfone, pyroxsulam, quinclorac,
rac, quinoclamine, quinonamid, quizalofop, ofop-P, rhodethanil, rimsulfuron,
saflufenacil, S-metolachlor, sebuthylazine, secbumeton, sethoxydim, siduron, simazine,
simeton, yn, SMA, sodium arsenite, sodium azide, sodium chlorate, rione,
sulfallate, trazone, sulfometuron, sulfosulfuron, sulfuric acid, sulglycapin, swep, TCA,
tebutam, tebuthiuron, tefuryltrione, tembotrione, tepraloxydim, terbacil, terbucarb,
terbuchlor, terbumeton, terbuthylazine, ryn, tetrafluron, thenylchlor, thiazafluron,
thiazopyr, thidiazimin, thidiazuron, thiencarbazone-methyl, thifensulfuron, thiobencarb,
tiocarbazil, rim, topramezone, tralkoxydim, triafamone, tri-allate, triasulfuron,
triaziflam, tribenuron, tricamba, triclopyr, hane, trietazine, trifloxysulfuron, trifluralin,
triflusulfuron, trifop, trifopsime, roxytriazine, trimeturon, tripropindan, tritac
tritosulfuron, ate, xylachlor and salts, , optically active isomers and mixtures
thereof.
The synergistic composition of the present invention can, further, be used in
conjunction with glufosinate, a, imidazolinones, sulfonylureas, or 2,4-D on
glyphosate-tolerant, glufosinate-tolerant, dicamba-tolerant, imidazolinone-tolerant,
sulfonylurea-tolerant and tolerant crops. It is generally preferred to use the synergistic
composition of the present invention in combination with herbicides that are selective for the
crop being treated and which complement the spectrum of weeds controlled by these
W0 2012/106566
compounds at the ation rate employed. It is r generally preferred to apply the
synergistic composition of the present invention and other mentary herbicides at the
same time, either as a combination formulation or as a tank mix.
The synergistic composition of the present invention can generally be employed in
combination with known herbicide safeners, such as benoxacor, benthiocarb, brassinolide,
cloquintocet ), cyometrinil, daimuron, dichlormid, dicyclonon, dimepiperate,
disulfoton, fenchlorazole-ethyl, fenclorim, flurazole, fluxofenim, furilazole, harpin proteins,
isoxadifen-ethyl, mefenpyr-diethyl, MG 191, MON 4660, naphthalic anhydride (NA),
oxabetrinil, R29148 and N—phenyl-sulfonylbenzoic acid amides, to enhance their selectivity.
In practice, it is preferable to use the synergistic composition of the present invention
in es containing an herbicidally effective amount of the herbicidal components along
with at least one agriculturally acceptable adjuvant or r. Suitable adjuvants or carriers
should not be phytotoxic to valuable crops, particularly at the concentrations employed in
applying the compositions for selective weed control in the presence of crops, and should not
react chemically with herbicidal components or other composition ingredients. Such
mixtures can be designed for application ly to weeds or their locus or can be
concentrates or formulations that are normally diluted with onal carriers and adjuvants
before application. They can be solids, such as, for example, dusts, granules, water-
dispersible granules, or wettable powders, or liquids, such as, for example, emulsifiable
concentrates, solutions, ons or suspensions.
Suitable agricultural adjuvants and carriers that are useful in preparing the herbicidal
mixtures of the invention are well known to those d in the art. Some of these adjuvants
include, but are not limited to, crop oil concentrate (mineral oil (85%) + emulsifiers (15%));
henol late; benzylcocoalkyldimethyl nary ammonium salt; blend of
petroleum arbon, alkyl esters, organic acid, and c surfactant; C9-C1]
alkylpolyglycoside; phosphated alcohol ethoxylate; natural primary alcohol (Cm—C16)
ethoxylate; di-sec-butylphenol EO-PO block copolymer; polysiloxane-methyl cap;
nonylphenol ethoxylate + urea ammonium nitrate; emulsified methylated seed oil; tridecyl
alcohol (synthetic) ethoxylate (8E0); tallow amine ethoxylate (15 E0); PEG(400) dioleate-
99.
Liquid carriers that can be employed include water, toluene, xylene, petroleum
naphtha, crop oil, acetone, methyl ethyl ketone, cyclohexanone, trichloroethylene,
perchloroethylene, ethyl acetate, amyl acetate, butyl acetate, propylene glycol monomethyl
ether and diethylene glycol monomethyl ether, methyl alcohol, ethyl alcohol, isopropyl
alcohol, amyl alcohol, ethylene glycol, propylene glycol, glycerine, N—methyl
pyrrolidinone, N,N—dimethyl alkylamides, dimethyl sulfoxide, liquid fertilizers and the like.
Water is generally the carrier of choice for the on of concentrates.
Suitable solid carriers include talc, pyrophyllite clay, silica, attapulgus clay, kaolin
clay, kieselguhr, chalk, diatomaceous earth, lime, calcium carbonate, bentonite clay, Fuller's
earth, cottonseed hulls, wheat flour, soybean flour, pumice, wood flour, walnut shell flour,
lignin, and the like.
It is usually desirable to incorporate one or more surface-active agents into the
compositions of the present invention. Such surface-active agents are advantageously
ed in both solid and liquid compositions, especially those designed to be diluted with
carrier before ation. The surface-active agents can be anionic, cationic or nonionic in
character and can be employed as emulsifying agents, wetting agents, suspending agents, or
for other purposes. Surfactants conventionally used in the art of formulation and which may
also be used in the present formulations are described, inter alia, in “McCutcheon’s
ents and Emulsifiers Annual,” MC Publishing Corp., ood, New Jersey, 1998
and in “Encyclopedia of tants,” Vol. I-III, Chemical Publishing Co., New York, 1980-
81. Typical surface-active agents include salts of alkyl es, such as diethanolammonium
lauryl sulfate; alkylarylsulfonate salts, such as calcium dodecylbenzenesulfonate;
alkylphenol-alkylene oxide addition ts, such as nonylphenol-Clg ethoxylate;
alcohol-alkylene oxide addition products, such as tridecyl alcohol-C16 late; soaps, such
as sodium stearate; alkylnaphthalene-sulfonate salts, such as sodium dibutyl-
naphthalenesulfonate; l esters of sulfosuccinate salts, such as sodium di(2-ethylhexyl)
sulfosuccinate; sorbitol , such as sorbitol oleate; quaternary amines, such as lauryl
trimethylammonium chloride; polyethylene glycol esters of fatty acids, such as polyethylene
glycol stearate; block copolymers of ethylene oxide and propylene oxide; salts of mono- and
dialkyl phosphate ; vegetable or seed oils such as soybean oil, rapeseed/canola oil, olive
oil, castor oil, er seed oil, t oil, corn oil, cottonseed oil, linseed oil, palm oil,
W0 2012/106566
peanut oil, safflower oil, sesame oil, tung oil and the like; and esters of the above vegetable
oils, particularly methyl esters.
Oftentimes, some of these materials, such as vegetable or seed oils and their ,
can be used hangeably as an agricultural nt, as a liquid carrier or as a surface
active agent.
Other ves commonly used in agricultural compositions include compatibilizing
agents, antifoam agents, sequestering agents, lizing agents and buffers, corrosion
inhibitors, dyes, odorants, spreading agents, penetration aids, sticking agents, sing
agents, thickening agents, freezing point depressants, antimicrobial agents, and the like. The
compositions may also contain other ible components, for example, other herbicides,
plant growth regulants, fungicides, insecticides, and the like and can be formulated with
liquid fertilizers or solid, particulate fertilizer carriers such as ammonium nitrate, urea and the
like.
The tration of the active ingredients in the synergistic composition of the
present invention is generally from 0.1 to 98 percent by weight. Concentrations from 10 to
90 percent by weight are often ed. In itions ed to be employed as
concentrates, the active ingredients are generally present in a concentration from 5 to 98
weight percent, preferably 10 to 90 weight percent. Such compositions are typically diluted
with an inert carrier, such as water, before making a postemergence, foliar application to
exposed weed and crop e, or applied as a dry or liquid formulation directly into flooded
rice fields. The diluted compositions usually applied as a postemergence, foliar application
to weeds or the locus of weeds generally contain 0.25 to 20 weight percent active ingredient
and preferably contain 0.4 to 14 weight percent.
The present compositions can be applied to weeds or their locus by the use of
conventional ground or aerial dusters, sprayers, and granule applicators, by addition to
irrigation or paddy water, and by other conventional means known to those skilled in the art.
The following examples illustrate the present invention.
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Examples
Evaluation of Postemergence Herbicidal Activity of Mixtures in the Greenhouse
Seeds of the desired test plant species were planted in 80% mineral soil/20% grit
planting mixture, which typically has a pH of 7.2 and an organic matter content of 2.9
percent, in c pots with a surface area of 128 square centimeters (cmZ). The growing
medium was steam sterilized. The plants were grown for 7-19 days in a greenhouse with an
approximate 14-hour (h) photoperiod which was maintained at 29 0C during the day and 26
0C during the night. Nutrients and water were added on a regular basis and supplemental
lighting was provided with overhead metal halide 1000-Watt lamps as necessary. The plants
were treated with postemergence foliar applications when they reached the second to fourth
true leaf stage. All treatments were applied using a randomized complete block trial ,
with 4 ations per treatment.
Formulated amounts of penoxsulam and glyphosate IPA salt were placed in 60
milliliter (mL) glass vials and dissolved in a volume of 60 mL of a water solution containing
Agri-dex crop oil concentrate in a 1% volume per volume (v/v) ratio. Compound
requirements are based upon a 12 mL application volume at a rate of 187 liters per hectare
(L/ha). Spray solutions of the mixtures were prepared by adding the stock solutions to the
appropriate amount of dilution solution to form 12 mL spray solution with active ingredients
in single and two way combinations. Formulated compounds were applied to the plant
material with an overhead Mandel track r ed with 8002E nozzles calibrated to
r 187 L/ha at a spray height of 18 inches (43 centimeters (cm)) above average plant
canopy. The weed spectrum included broadleaf signalgrass iaria platyphylla,
BRAPP), yellow nutsedge (Cyperus esculentus, CYPES), barnyardgrass (Echinochloa crus-
galli, ECHCG), morningglory ea, hederacea, IPOHE), and Chinese sprangletop
chloa chinensis, LEFCH).
The treated plants and control plants were placed in a greenhouse as described above
and d by sub-irrigation to prevent wash-off of the test compounds. Treatments were
rated at 16 days after application (DAA) as compared to the untreated control . Visual
weed control was scored on a scale of 0 to 100 percent where 0 corresponds to no injury and
100 corresponds to complete kill. Results are reported in Tables 1-3.
W0 2012/106566
tion of ergence Herbicidal Activity of Mixtures under Field Conditions
Methodology
Trial site was located in commercially grown vines of European grape (Vitis
vinifera). The trial was conducted using normal research ology. Trial plots were
n 2 m wide by 6 10 m long. All treatments were applied using a randomized complete
block trial design with 3 ations per treatment. The trial sites had naturally occurring
populations of weeds. The weed spectrum included, but was not limited to, ryegrass (Lolium
spp, LOLSS), scented mayweed (Matricaria chamomilla, MATCH), and annual bluegrass
(Poa annua, POAAN).
Treatments consisted of tank mixes of an oil dispersion of penoxsulam and
commercially available formulation of sate applied in water. The application volume
was 250 liters per hectare (L/ha). Application was made using a precision gas hand sprayer at
250 kPA pressure using a 2 m boom with flat fan (80015VS) nozzles to broadcast the
treatments to the weeds and to the soil.
The treated and control pots were rated blind at s intervals after ation,
with the last evaluation taken 16 days after application. Ratings were based on Percent (%)
Visual weed control, where 0 corresponds to no control and 100 corresponds to te
control. Results are reported in Table 4.
Evaluation
Data was collected and analyzed using various statistical methods.
Colby’s equation was used to determine the herbicidal effects expected from the
mixtures (Colby, S. R. Calculation of the synergistic and antagonistic se of ide
combinations. Weeds 1967 15, 20-22).
The following equation was used to calculate the expected activity of mixtures
containing two active ingredients, A and B:
Expected = A + B - (A x B/lOO)
A = observed efficacy of active ingredient A at the same concentration as used in the
mixture ;
W0 2012/106566
B = observed efficacy of active ingredient B at the same concentration as used in the
mixture.
The results are summarized in Tables 1-4.
Table 1. Control of CYPES and LEFCH in the greenhouse with Penoxsulam plus
53 grams ai/ha of Glyphosate
Days
Penoxsulam Glyphosate CYPES LEFCH
After
(rate in grams ai/ha) Application Obs Exp* Obs Exp*
CYPES = yellow nutsedge, grams ai/ha = grams of active ingredient
Cyperus esculentus per hectare
LEFCH = Chinese sprangletop, Obs = Observed control (%)
hloa sis EXp* = Expected control (%)
2012/023707
Table 2. Control of CYPES and BRAPP in the greenhouse with Penoxsulam plus
110 grams ai/ha of Glyphosate
Days
Penoxsulam Glyphosate CYPES BRAPP
After
(rate in grams ai/ha) Application Obs Exp* Obs Exp*
CYPES = yellow nutsedge, grams ai/ha = grams of active ingredient
s esculentus per hectare
BRAPP = broadleaf signalgrass, 10 Obs = Observed control (%)
Brachiaria plalyphylla EXp* = Expected control (%)
Table 3. Control of CYPES, ECHCG, IPOHE and LEFCH in the greenhouse with
Penoxsulam plus 210 grams ai/ha of Glyphosate
Penox- Glypho-
sulam sate
(rate in grams ai/ha) cation Obs Exp* Obs Exp* Obs Exp* Obs Exp*
CYPES = yellow nutsedge, IPOHE = morningglory, Ipomoea
s esculentus hederacea
LEFCH = Chinese sprangletop, grams ai/ha = grams of active ingredient
Leptochloa chinensis per hectare
ECHCG = barnyardgrass, Obs = Observed control (%)
Echinochloa crus-galli EXp* = Expected l (%)
Table 4. S ner istic control of MATCH POAAN and LOLSS in the field with 20
+ 720 rams ai/ha of Penoxsulam + G] hosate res ectivel
Penox' Glyph“
MATCH POAAN LOLSS
sulam sate
(rate in grams ai/ha) ' Obs Exp* Obs Exp* Obs Exp*
LOLSS = ryegrass, Lolium spp.i—ngredientgrams ai/ha = grams of active
MATCH = scented mayweed, per hectare
Matricaria Chamomilla Obs = Observed l (%)
POAAN = annual bluegrass, Poa EXp* = Expected control (%)
annua
1001140880
Reference to any prior art in the specification is not, and should not be taken as, an
acknowledgment, or any form of suggestion, that this prior art forms part of the common
general knowledge in New d or any other jurisdiction or that this prior art could
reasonably be expected to be ascertained, understood and regarded as relevant by a person
skilled in the art.
As used herein, except where the context requires otherwise, the term "comprise" and
variations of the term, such as ”comprisingH H
, ses" and ised", are not intended
to exclude other additives, components, integers or steps.
1001140880
Claims (8)
1. A synergistic herbicidal mixture comprising an herbicidally effective amount of (a) penoxsulam and (b) glyphosate, wherein the weight ratio of sate to ulam is from 4:1 to 448:1. U}
2. The synergistic herbicidal mixture of Claim 1 in which sate is an agriculturally acceptable salt.
3. An herbicidal composition comprising an herbicidally effective amount of the synergistic idal mixture of Claim 1 or 2 and an agriculturally acceptable adjuvant and/or carrier. 10
4. A method of lling undesirable vegetation which comprises contacting the vegetation or the locus thereof with an herbicidally effective amount of the synergistic herbicidal mixture of Claim 1 or 2.
5. A method of controlling undesirable vegetation which comprises contacting the vegetation or the locus thereof with an herbicidally effective amount of the herbicidal 15 composition of Claim 3.
6. The method ofClaim 4 or 5, wherein the undesirable vegetation is in vines, pasture. rangeland, industrial vegetation management, cs or turf.
7. The method of Claim 4 or 5, wherein the undesirable vegetation is in a glyphosate tolerant crop. 20
8. The synergistic herbicidal e of Claim 1, substantially as herein described.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161439478P | 2011-02-04 | 2011-02-04 | |
US61/439,478 | 2011-02-04 | ||
PCT/US2012/023707 WO2012106566A1 (en) | 2011-02-04 | 2012-02-03 | Synergistic herbicidal composition containing penoxsulam and glyphosate |
Publications (2)
Publication Number | Publication Date |
---|---|
NZ613736A NZ613736A (en) | 2015-07-31 |
NZ613736B2 true NZ613736B2 (en) | 2015-11-03 |
Family
ID=
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