NL7102065A - Gas chromatography column - having a capillary tube filled with impregnated particles - Google Patents

Gas chromatography column - having a capillary tube filled with impregnated particles

Info

Publication number
NL7102065A
NL7102065A NL7102065A NL7102065A NL7102065A NL 7102065 A NL7102065 A NL 7102065A NL 7102065 A NL7102065 A NL 7102065A NL 7102065 A NL7102065 A NL 7102065A NL 7102065 A NL7102065 A NL 7102065A
Authority
NL
Netherlands
Prior art keywords
column
capillary tube
gas chromatography
chromatography column
tube filled
Prior art date
Application number
NL7102065A
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Priority to NL7102065A priority Critical patent/NL7102065A/en
Publication of NL7102065A publication Critical patent/NL7102065A/en

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/50Conditioning of the sorbent material or stationary liquid
    • G01N30/56Packing methods or coating methods

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)

Abstract

A capillary tube, 1 mm in dia., and esp. wound in a spiral is filled, batchwise, with carrier particles whose dia. is between 80-300 mu but with a max. spread of 25 mu, and these are then coated or impregnated in batches, progressively, under pressure with a stationary phase liquid. Whilst the pressure is applied (e.g. 1-2 kg/cm2 per metre length) the other end of the column is closed by a porous plug and the column is exposed to ultrasonic vibrations. As an alternative to compressed gas, a vacuum of 10-20 Torr may be applied to the other end of the column using a water jet vacuum pump. Higher band width without loss of efficiency is obtd.
NL7102065A 1971-02-16 1971-02-16 Gas chromatography column - having a capillary tube filled with impregnated particles NL7102065A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
NL7102065A NL7102065A (en) 1971-02-16 1971-02-16 Gas chromatography column - having a capillary tube filled with impregnated particles

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NL7102065A NL7102065A (en) 1971-02-16 1971-02-16 Gas chromatography column - having a capillary tube filled with impregnated particles

Publications (1)

Publication Number Publication Date
NL7102065A true NL7102065A (en) 1972-08-18

Family

ID=19812490

Family Applications (1)

Application Number Title Priority Date Filing Date
NL7102065A NL7102065A (en) 1971-02-16 1971-02-16 Gas chromatography column - having a capillary tube filled with impregnated particles

Country Status (1)

Country Link
NL (1) NL7102065A (en)

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