MY150197A - Method for producing lithium transition metal polyanion powders for batteries - Google Patents
Method for producing lithium transition metal polyanion powders for batteriesInfo
- Publication number
- MY150197A MY150197A MYPI20095224A MYPI20095224A MY150197A MY 150197 A MY150197 A MY 150197A MY PI20095224 A MYPI20095224 A MY PI20095224A MY PI20095224 A MYPI20095224 A MY PI20095224A MY 150197 A MY150197 A MY 150197A
- Authority
- MY
- Malaysia
- Prior art keywords
- batteries
- product
- suspension
- transition metal
- lithium transition
- Prior art date
Links
- 229910052744 lithium Inorganic materials 0.000 title abstract 2
- -1 lithium transition metal Chemical class 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- 229920000447 polyanionic polymer Polymers 0.000 title 1
- 239000000843 powder Substances 0.000 title 1
- 229910052723 transition metal Inorganic materials 0.000 title 1
- 239000000047 product Substances 0.000 abstract 3
- 239000000725 suspension Substances 0.000 abstract 3
- 238000000034 method Methods 0.000 abstract 2
- 239000002245 particle Substances 0.000 abstract 2
- 239000002243 precursor Substances 0.000 abstract 2
- 239000012265 solid product Substances 0.000 abstract 2
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 abstract 1
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 abstract 1
- 229910019142 PO4 Inorganic materials 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 229910001416 lithium ion Inorganic materials 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 abstract 1
- 239000010452 phosphate Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 229910052720 vanadium Inorganic materials 0.000 abstract 1
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B1/00—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors
- H01B1/06—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances
- H01B1/12—Conductors or conductive bodies characterised by the conductive materials; Selection of materials as conductors mainly consisting of other non-metallic substances organic substances
- H01B1/122—Ionic conductors
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/45—Phosphates containing plural metal, or metal and ammonium
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/362—Composites
- H01M4/366—Composites as layered products
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
- H01M4/624—Electric conductive fillers
- H01M4/625—Carbon or graphite
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M2300/00—Electrolytes
- H01M2300/0017—Non-aqueous electrolytes
- H01M2300/0025—Organic electrolyte
- H01M2300/0028—Organic electrolyte characterised by the solvent
- H01M2300/0037—Mixture of solvents
- H01M2300/004—Three solvents
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/136—Electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Composite Materials (AREA)
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Battery Electrode And Active Subsutance (AREA)
Abstract
THIS INVENTION RELATES TO A PROCESS FOR PRODUCING AN IMPROVED POWDER FOR THE POSITIVE ELECTRODE OF LITHIUM ION BATTERIES WHEREIN THE POWDER COMPRISES LITHIUM, VANADIUM AND PHOSPHATE. THE PROCESS INCLUDES FORMING A SUSPENSION OF THE PRECURSORS WITH A HIGH BOILING TEMPERATURE SOLVENT AND HEATING THE SUSPENSION TO A REACTION TEMPERATURE OF BETWEEN 250°C AND 400°C TO CONVERT THE PRECURSORS TO THE DESIRED SOLID PRODUCT. THE SOLID PRODUCT IS SEPARATED FROM THE SUSPENSION AND IS HEATED TO A HIGHER TEMPERATURE TO CRYSTALLIZE THE PRODUCT. THE RESULTING PRODUCT RETAINS A SMALL PARTICLE SIZE THUS AVOIDING THE NEED FOR MILLING OR OTHER PROCESSING TO REDUCE THE PRODUCT TO A PARTICLE SIZE SUITED FOR BATTERIES.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US93391507P | 2007-06-08 | 2007-06-08 | |
| US12/024,023 US20080303004A1 (en) | 2007-06-08 | 2008-01-31 | Method for producing lithium transition metal polyanion powders for batteries |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MY150197A true MY150197A (en) | 2013-12-13 |
Family
ID=40095007
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MYPI20095224A MY150197A (en) | 2007-06-08 | 2008-06-05 | Method for producing lithium transition metal polyanion powders for batteries |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US20080303004A1 (en) |
| EP (1) | EP2152630A4 (en) |
| JP (1) | JP2010529623A (en) |
| KR (1) | KR20100031728A (en) |
| CN (1) | CN101730659A (en) |
| CA (1) | CA2689098A1 (en) |
| MY (1) | MY150197A (en) |
| TW (1) | TW200906715A (en) |
| WO (1) | WO2008154287A1 (en) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009245740A (en) * | 2008-03-31 | 2009-10-22 | Fuji Heavy Ind Ltd | Layered crystalline material, method of manufacturing electrode material, and energy storage device |
| CN102257660B (en) * | 2008-12-19 | 2015-01-21 | 菲利浦66公司 | Process for making fluorinated lithium vanadium polyanion powders for batteries |
| US20100154206A1 (en) * | 2008-12-19 | 2010-06-24 | Conocophillips Company | Process for making composite lithium powders for batteries |
| US20100266474A1 (en) * | 2009-04-16 | 2010-10-21 | Titus Faulkner | Method of Making Active Materials for Use in Secondary Electrochemical Cells |
| US8372540B2 (en) * | 2009-04-16 | 2013-02-12 | Valence Technology, Inc. | Electrode active material for secondary electrochemical cell |
| JP5612392B2 (en) * | 2010-08-09 | 2014-10-22 | 日本化学工業株式会社 | Method for producing lithium vanadium phosphate carbon composite |
| JP5609485B2 (en) * | 2010-09-22 | 2014-10-22 | Tdk株式会社 | Active material, method for producing active material, electrode, and lithium ion secondary battery |
| US20130029227A1 (en) | 2011-07-26 | 2013-01-31 | Toyota Motor Engineering & Manufacturing North America, Inc. | Polyanion active materials and method of forming the same |
| JP5871543B2 (en) * | 2011-09-29 | 2016-03-01 | 富士重工業株式会社 | Modified vanadium phosphate lithium carbon composite, method for producing the same, lithium secondary battery positive electrode active material, and lithium secondary battery |
| JP5255143B2 (en) * | 2011-09-30 | 2013-08-07 | 富士重工業株式会社 | Positive electrode material, lithium ion secondary battery using the same, and method for manufacturing positive electrode material |
| KR101436828B1 (en) * | 2012-04-25 | 2014-09-18 | 전남대학교산학협력단 | Method for preparing high capacity electrode active material for electrochemical device having improved rate capability in high rate charge and discharge condition |
| JP6345227B2 (en) * | 2016-03-08 | 2018-06-20 | 日本化学工業株式会社 | Method for producing lithium vanadium phosphate |
| CN106099102B (en) * | 2016-07-04 | 2019-05-17 | 大连博融新材料有限公司 | A kind of production method of lithium ion battery electrode active material |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6514640B1 (en) * | 1996-04-23 | 2003-02-04 | Board Of Regents, The University Of Texas System | Cathode materials for secondary (rechargeable) lithium batteries |
| US5910382A (en) * | 1996-04-23 | 1999-06-08 | Board Of Regents, University Of Texas Systems | Cathode materials for secondary (rechargeable) lithium batteries |
| US5871866A (en) * | 1996-09-23 | 1999-02-16 | Valence Technology, Inc. | Lithium-containing phosphates, method of preparation, and use thereof |
| US6203946B1 (en) * | 1998-12-03 | 2001-03-20 | Valence Technology, Inc. | Lithium-containing phosphates, method of preparation, and uses thereof |
| US6506520B1 (en) * | 1998-12-02 | 2003-01-14 | Matsushita Electric Industrial Co., Ltd. | Non-aqueous electrolyte secondary battery |
| CA2270771A1 (en) * | 1999-04-30 | 2000-10-30 | Hydro-Quebec | New electrode materials with high surface conductivity |
| US7001690B2 (en) * | 2000-01-18 | 2006-02-21 | Valence Technology, Inc. | Lithium-based active materials and preparation thereof |
| US6528033B1 (en) * | 2000-01-18 | 2003-03-04 | Valence Technology, Inc. | Method of making lithium-containing materials |
| US6645452B1 (en) * | 2000-11-28 | 2003-11-11 | Valence Technology, Inc. | Methods of making lithium metal cathode active materials |
| DE10117904B4 (en) * | 2001-04-10 | 2012-11-15 | Zentrum für Sonnenenergie- und Wasserstoff-Forschung Baden-Württemberg Gemeinnützige Stiftung | Binary, ternary and quaternary lithium iron phosphates, process for their preparation and their use |
| KR101209358B1 (en) * | 2001-12-21 | 2012-12-07 | 메사추세츠 인스티튜트 오브 테크놀로지 | Conductive lithium storage electrode |
| US20030160215A1 (en) * | 2002-01-31 | 2003-08-28 | Zhenhua Mao | Coated carbonaceous particles particularly useful as electrode materials in electrical storage cells, and methods of making the same |
| CN100379062C (en) * | 2002-06-21 | 2008-04-02 | 优米科尔公司 | Carbon-coated lithium-containing powder and manufacturing method thereof |
| US6913855B2 (en) * | 2002-07-22 | 2005-07-05 | Valence Technology, Inc. | Method of synthesizing electrochemically active materials from a slurry of precursors |
| JP4011442B2 (en) * | 2002-08-30 | 2007-11-21 | 住友大阪セメント株式会社 | Method for producing positive electrode material for lithium ion battery and lithium ion battery |
| DE10353266B4 (en) * | 2003-11-14 | 2013-02-21 | Süd-Chemie Ip Gmbh & Co. Kg | Lithium iron phosphate, process for its preparation and its use as electrode material |
| JP2005247649A (en) * | 2004-03-05 | 2005-09-15 | Yuasa Corp | Metal chalcogen compound and method for producing the same, and electrode and electrochemical device using the same |
| US7338647B2 (en) * | 2004-05-20 | 2008-03-04 | Valence Technology, Inc. | Synthesis of cathode active materials |
| CA2613926C (en) * | 2005-06-29 | 2013-10-29 | Umicore | Crystalline nanometric lifepo4 |
| US7524529B2 (en) * | 2005-09-09 | 2009-04-28 | Aquire Energy Co., Ltd. | Method for making a lithium mixed metal compound having an olivine structure |
| JP2007103298A (en) * | 2005-10-07 | 2007-04-19 | Toyota Central Res & Dev Lab Inc | Positive electrode active material, method for producing the same, and aqueous lithium secondary battery |
| JP5084131B2 (en) * | 2005-10-28 | 2012-11-28 | トヨタ自動車株式会社 | Method for producing LiMnPO4 |
| US20070160752A1 (en) * | 2006-01-09 | 2007-07-12 | Conocophillips Company | Process of making carbon-coated lithium metal phosphate powders |
| CN100427387C (en) * | 2006-11-21 | 2008-10-22 | 华南理工大学 | A kind of sol-gel preparation method of lithium vanadium phosphate lithium ion battery cathode material |
| US20080305256A1 (en) * | 2007-06-08 | 2008-12-11 | Conocophillips Company | Method for producing lithium vanadium polyanion powders for batteries |
-
2008
- 2008-01-31 US US12/024,023 patent/US20080303004A1/en not_active Abandoned
- 2008-05-09 TW TW097117120A patent/TW200906715A/en unknown
- 2008-06-05 KR KR1020107000317A patent/KR20100031728A/en not_active Ceased
- 2008-06-05 WO PCT/US2008/065909 patent/WO2008154287A1/en not_active Ceased
- 2008-06-05 CN CN200880019362A patent/CN101730659A/en active Pending
- 2008-06-05 MY MYPI20095224A patent/MY150197A/en unknown
- 2008-06-05 CA CA002689098A patent/CA2689098A1/en not_active Abandoned
- 2008-06-05 EP EP08770190A patent/EP2152630A4/en not_active Withdrawn
- 2008-06-05 JP JP2010511321A patent/JP2010529623A/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| US20080303004A1 (en) | 2008-12-11 |
| TW200906715A (en) | 2009-02-16 |
| EP2152630A4 (en) | 2012-04-04 |
| JP2010529623A (en) | 2010-08-26 |
| CA2689098A1 (en) | 2008-12-18 |
| EP2152630A1 (en) | 2010-02-17 |
| KR20100031728A (en) | 2010-03-24 |
| CN101730659A (en) | 2010-06-09 |
| WO2008154287A1 (en) | 2008-12-18 |
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