MX2016012816A - Lithium-intercalated titanium dioxide, lithium titanate particles made therefrom, and related methods. - Google Patents
Lithium-intercalated titanium dioxide, lithium titanate particles made therefrom, and related methods.Info
- Publication number
- MX2016012816A MX2016012816A MX2016012816A MX2016012816A MX2016012816A MX 2016012816 A MX2016012816 A MX 2016012816A MX 2016012816 A MX2016012816 A MX 2016012816A MX 2016012816 A MX2016012816 A MX 2016012816A MX 2016012816 A MX2016012816 A MX 2016012816A
- Authority
- MX
- Mexico
- Prior art keywords
- lithium
- titanium dioxide
- particles
- particle
- electrode
- Prior art date
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Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/04—Oxides; Hydroxides
- C01G23/047—Titanium dioxide
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82B—NANOSTRUCTURES FORMED BY MANIPULATION OF INDIVIDUAL ATOMS, MOLECULES, OR LIMITED COLLECTIONS OF ATOMS OR MOLECULES AS DISCRETE UNITS; MANUFACTURE OR TREATMENT THEREOF
- B82B1/00—Nanostructures formed by manipulation of individual atoms or molecules, or limited collections of atoms or molecules as discrete units
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/485—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of mixed oxides or hydroxides for inserting or intercalating light metals, e.g. LiTi2O4 or LiTi2OxFy
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/003—Titanates
- C01G23/005—Alkali titanates
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/08—Intercalated structures, i.e. with atoms or molecules intercalated in their structure
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/30—Three-dimensional structures
- C01P2002/32—Three-dimensional structures spinel-type (AB2O4)
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/60—Compounds characterised by their crystallite size
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
- C01P2004/32—Spheres
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/51—Particles with a specific particle size distribution
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/16—Pore diameter
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M2004/021—Physical characteristics, e.g. porosity, surface area
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
- H01M2004/027—Negative electrodes
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Nanotechnology (AREA)
- Manufacturing & Machinery (AREA)
- Crystallography & Structural Chemistry (AREA)
- Physics & Mathematics (AREA)
- Composite Materials (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Secondary Cells (AREA)
Abstract
The invention provides a method for preparing lithium-containing particles suitable for use in an electrode of a battery, the method including forming a mixture comprising titanium dioxide precursor particles and an aqueous solution of a lithium compound; and heating the mixture at elevated temperature in a sealed pressure vessel in order to form lithium-inserted titanium dioxide particles, wherein at least one particle size characteristic selected from average primary particle size, particle size distribution, average intra-particle pore size, average inter-particle pore size, pore size distribution, and particle shape of the titanium dioxide particles is substantially unchanged by said heating step. The invention further includes a battery including a first electrode, a second electrode, and a separator including an electrolyte between the first and second electrodes, wherein one of the first and second electrodes comprises lithium-inserted titanium dioxide particles or lithium titanate spinel particles made according to the invention.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US14/230,435 US11223042B2 (en) | 2014-03-31 | 2014-03-31 | Lithium-intercalated titanium dioxide, lithium titanate particles made therefrom, and related methods |
PCT/US2015/023263 WO2015153413A1 (en) | 2014-03-31 | 2015-03-30 | Lithium-intercalated titanium dioxide, lithium titanate particles made therefrom, and related methods |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2016012816A true MX2016012816A (en) | 2017-01-13 |
Family
ID=52875291
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2016012816A MX2016012816A (en) | 2014-03-31 | 2015-03-30 | Lithium-intercalated titanium dioxide, lithium titanate particles made therefrom, and related methods. |
Country Status (22)
Country | Link |
---|---|
US (1) | US11223042B2 (en) |
EP (1) | EP3126291B1 (en) |
JP (1) | JP6671294B2 (en) |
KR (1) | KR102344348B1 (en) |
CN (2) | CN112744857B (en) |
AR (1) | AR100202A1 (en) |
AU (1) | AU2015241096B2 (en) |
BR (1) | BR112016022644B1 (en) |
CA (1) | CA2944448A1 (en) |
ES (1) | ES2939968T3 (en) |
FI (1) | FI3126291T3 (en) |
MX (1) | MX2016012816A (en) |
MY (1) | MY190596A (en) |
PH (2) | PH12016501924A1 (en) |
PL (1) | PL3126291T3 (en) |
RU (1) | RU2691086C2 (en) |
SG (2) | SG11201608117XA (en) |
SI (1) | SI3126291T1 (en) |
TW (1) | TWI718095B (en) |
UA (1) | UA121470C2 (en) |
WO (1) | WO2015153413A1 (en) |
ZA (1) | ZA201606943B (en) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106410175B (en) * | 2016-10-26 | 2018-12-21 | 河南师范大学 | A kind of modified Nano grade ThO2Anode material of lithium battery |
US11183682B2 (en) * | 2018-08-31 | 2021-11-23 | Advanced Energy Materials, Llc | Spinel lithium titanium oxide (LTO) nanowire anode material for lithium ion batteries |
Family Cites Families (27)
Publication number | Priority date | Publication date | Assignee | Title |
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GB1489927A (en) | 1974-08-10 | 1977-10-26 | Tioxide Group Ltd | Titanium dioxide carrier |
US4882128A (en) | 1987-07-31 | 1989-11-21 | Parr Instrument Company | Pressure and temperature reaction vessel, method, and apparatus |
SU1585294A1 (en) | 1988-06-13 | 1990-08-15 | Предприятие П/Я Г-4855 | Method of producing titanium dioxide of rutile modification |
US6645673B2 (en) | 1999-02-16 | 2003-11-11 | Toho Titanium Co., Ltd. | Process for producing lithium titanate and lithium ion battery and negative electrode therein |
CA2327370A1 (en) * | 2000-12-05 | 2002-06-05 | Hydro-Quebec | New method of manufacturing pure li4ti5o12 from the ternary compound tix-liy-carbon: effect of carbon on the synthesis and conductivity of the electrode |
US6827921B1 (en) | 2001-02-01 | 2004-12-07 | Nanopowder Enterprises Inc. | Nanostructured Li4Ti5O12 powders and method of making the same |
DE60202373T2 (en) | 2001-07-20 | 2005-12-08 | Altair Nanomaterials Inc., Reno | PROCESS FOR THE PREPARATION OF LITHIUM TITANATE |
DE10319464A1 (en) | 2003-04-29 | 2004-11-18 | Basf Ag | Process for the production of nanocrystalline lithium titanate spinels |
US7125536B2 (en) | 2004-02-06 | 2006-10-24 | Millennium Inorganic Chemicals, Inc. | Nano-structured particles with high thermal stability |
JP4249727B2 (en) | 2005-05-13 | 2009-04-08 | 株式会社東芝 | Nonaqueous electrolyte battery and lithium titanium composite oxide |
US7820137B2 (en) | 2006-08-04 | 2010-10-26 | Enerdel, Inc. | Lithium titanate and method of forming the same |
US7820583B2 (en) | 2006-08-24 | 2010-10-26 | Millennium Inorganic Chemicals, Inc. | Nanocomposite particle and process of preparing the same |
KR101364398B1 (en) * | 2007-05-17 | 2014-02-18 | 주식회사 엘지화학 | Lithium titanate with nanostructure |
US7763565B2 (en) | 2007-08-31 | 2010-07-27 | Millennium Inorganic Chemicals, Inc. | Transparent, stable titanium dioxide sols |
DE102008026580A1 (en) | 2008-06-03 | 2009-12-10 | Süd-Chemie AG | Process for producing lithium titanium spinel and its use |
CZ2008572A3 (en) | 2008-09-19 | 2010-02-10 | He3Da S.R.O. | Lithium accumulator with spatial-type electrodes and process for producing thereof |
CN101759227A (en) * | 2008-12-24 | 2010-06-30 | 比亚迪股份有限公司 | Lithium titanate composite material and preparation method thereof |
JP5368361B2 (en) | 2010-04-20 | 2013-12-18 | 株式会社エヌ・ティ・ティ・ドコモ | Positioning device and positioning method |
US9293235B2 (en) | 2010-08-31 | 2016-03-22 | Toda Kogyo Corporation | Lithium titanate particles and process for producing the lithium titanate particles, Mg-containing lithium titanate particles and process for producing the Mg-containing lithium titanate particles, negative electrode active substance particles for non-aqueous electrolyte secondary batteries, and non-aqueous electrolyte secondary battery |
US9260483B2 (en) * | 2011-01-10 | 2016-02-16 | Technische Universität München | Triazacyclononane-based phosphinate ligand and its use for molecular imaging |
KR101873618B1 (en) * | 2011-06-27 | 2018-07-02 | 내셔널 유니버시티 오브 싱가포르 | PRODUCTION OF NANOSTRUCTURED Li4Ti5O12 WITH SUPERIOR HIGH RATE PERFORMANCE |
CN102891302A (en) * | 2011-07-19 | 2013-01-23 | 西门子公司 | Lithium titanate active substance, preparation method of the lithium titanate active substance and rechargeable lithium battery |
US8900705B2 (en) | 2011-11-16 | 2014-12-02 | Cristal Usa Inc. | Mesoporous titanium dioxide nanoparticles exhibiting bimodal pore size distributions and process for their production |
JP2014001110A (en) | 2012-06-20 | 2014-01-09 | Taiyo Yuden Co Ltd | Lithium titanium complex oxide, production method thereof and electrode for battery |
CN103545498B (en) * | 2012-07-13 | 2016-05-18 | 神华集团有限责任公司 | Lithium titanate-titanium dioxide composite material, preparation method thereof and negative electrode active material of rechargeable lithium ion battery formed by lithium titanate-titanium dioxide composite material |
CN103151507B (en) * | 2013-03-12 | 2015-05-27 | 余颖 | Preparation method of high-property lithium ion battery cathode material Li4Ti5O12 |
CN104103822B (en) * | 2013-04-12 | 2017-01-25 | 清华大学 | Preparation method of lithium ion battery cathode material |
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2014
- 2014-03-31 US US14/230,435 patent/US11223042B2/en active Active
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2015
- 2015-03-27 TW TW104109915A patent/TWI718095B/en active
- 2015-03-30 AU AU2015241096A patent/AU2015241096B2/en active Active
- 2015-03-30 SG SG11201608117XA patent/SG11201608117XA/en unknown
- 2015-03-30 MY MYPI2016001770A patent/MY190596A/en unknown
- 2015-03-30 ES ES15716649T patent/ES2939968T3/en active Active
- 2015-03-30 CA CA2944448A patent/CA2944448A1/en active Pending
- 2015-03-30 JP JP2016559846A patent/JP6671294B2/en active Active
- 2015-03-30 KR KR1020167029894A patent/KR102344348B1/en active IP Right Grant
- 2015-03-30 CN CN202110180652.8A patent/CN112744857B/en active Active
- 2015-03-30 EP EP15716649.7A patent/EP3126291B1/en active Active
- 2015-03-30 MX MX2016012816A patent/MX2016012816A/en unknown
- 2015-03-30 FI FIEP15716649.7T patent/FI3126291T3/en active
- 2015-03-30 SI SI201531916T patent/SI3126291T1/en unknown
- 2015-03-30 SG SG10201808276XA patent/SG10201808276XA/en unknown
- 2015-03-30 PL PL15716649.7T patent/PL3126291T3/en unknown
- 2015-03-30 UA UAA201610813A patent/UA121470C2/en unknown
- 2015-03-30 WO PCT/US2015/023263 patent/WO2015153413A1/en active Application Filing
- 2015-03-30 AR ARP150100961A patent/AR100202A1/en active IP Right Grant
- 2015-03-30 CN CN201580028526.3A patent/CN106458629A/en active Pending
- 2015-03-30 BR BR112016022644-5A patent/BR112016022644B1/en active IP Right Grant
- 2015-03-30 RU RU2016142399A patent/RU2691086C2/en active
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2016
- 2016-09-28 PH PH12016501924A patent/PH12016501924A1/en unknown
- 2016-10-10 ZA ZA2016/06943A patent/ZA201606943B/en unknown
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2021
- 2021-02-22 PH PH12021550369A patent/PH12021550369A1/en unknown
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