MX166335B - AN IMPROVED PROCESS FOR THE PREPARATION OF 3,5,6-TRICHLOROPYRIDINE 2-OL - Google Patents

AN IMPROVED PROCESS FOR THE PREPARATION OF 3,5,6-TRICHLOROPYRIDINE 2-OL

Info

Publication number
MX166335B
MX166335B MX020686A MX2068690A MX166335B MX 166335 B MX166335 B MX 166335B MX 020686 A MX020686 A MX 020686A MX 2068690 A MX2068690 A MX 2068690A MX 166335 B MX166335 B MX 166335B
Authority
MX
Mexico
Prior art keywords
steps
preparation
trichloropyridine
improved process
improved
Prior art date
Application number
MX020686A
Other languages
Spanish (es)
Inventor
R Garth Pews
Original Assignee
Dow Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Chemical Co filed Critical Dow Chemical Co
Publication of MX166335B publication Critical patent/MX166335B/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/62—Oxygen or sulfur atoms
    • C07D213/63—One oxygen atom
    • C07D213/64—One oxygen atom attached in position 2 or 6
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00—Carboxylic acid nitriles
    • C07C255/01—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
    • C07C255/19—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms containing cyano groups and carboxyl groups, other than cyano groups, bound to the same saturated acyclic carbon skeleton

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pyridine Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Hydrogenated Pyridines (AREA)

Abstract

A process for the preparation of 3,5,6-trichloropyridin-2-ol from trichloroacetyl chloride and acrylonitrile is improved by separately conducting the individual addition, cyclization and aromatization steps. By separating these steps, water and HCl, which are by-products of the latter steps, can be precluded from interfering with the earlier steps. The individual process steps have also been improved.
MX020686A 1989-05-12 1990-05-11 AN IMPROVED PROCESS FOR THE PREPARATION OF 3,5,6-TRICHLOROPYRIDINE 2-OL MX166335B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/350,961 US4996323A (en) 1989-05-12 1989-05-12 Process for the preparation of 3,5,6-trichloropyridin-2-ol

Publications (1)

Publication Number Publication Date
MX166335B true MX166335B (en) 1992-12-29

Family

ID=23378969

Family Applications (1)

Application Number Title Priority Date Filing Date
MX020686A MX166335B (en) 1989-05-12 1990-05-11 AN IMPROVED PROCESS FOR THE PREPARATION OF 3,5,6-TRICHLOROPYRIDINE 2-OL

Country Status (19)

Country Link
US (1) US4996323A (en)
EP (1) EP0397281B1 (en)
JP (1) JP2829342B2 (en)
KR (1) KR0153446B1 (en)
CN (1) CN1027259C (en)
AT (1) ATE144979T1 (en)
AU (1) AU620245B2 (en)
BR (1) BR9001798A (en)
CA (1) CA2016620C (en)
DE (1) DE69029052T2 (en)
DK (1) DK0397281T3 (en)
ES (1) ES2095854T3 (en)
FI (1) FI97132C (en)
HU (2) HU205078B (en)
IL (1) IL94373A (en)
MX (1) MX166335B (en)
NZ (1) NZ233615A (en)
RU (1) RU1839671C (en)
UA (1) UA19168A1 (en)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IL86341A (en) * 1988-05-11 1992-02-16 Pamol Ltd Preparation of polychloropyridine derivatives and intermediates therefor
US5254712A (en) * 1990-01-06 1993-10-19 Stamicarbon B.V. Process for the preparation of 5-oxohexane nitriles and the compound 2,4-dimethyl-5-oxohexane nitrile
NL9000034A (en) * 1990-01-06 1991-08-01 Stamicarbon PROCESS FOR THE PREPARATION OF 5-OXOHEXANE NITRILLES AND THE SUBSTANCE 2,4-DIMETHYL-5-OXOHEXANE NITRILLES.
US5618942A (en) * 1993-09-03 1997-04-08 Luxembourg Industries (Pamol) Ltd. Production of 2,3,5,6-tetrachloropyridine
US5688953A (en) * 1996-07-31 1997-11-18 Dowelanco Process for the preparation of 3,3,5-trichloroglutarimide
CN102351785B (en) * 2011-08-11 2013-05-01 江苏九九久科技股份有限公司 Method for preparing 3, 5, 6-trichloropyridin-2-ol sodium
CN103086961A (en) * 2011-10-27 2013-05-08 山西三维丰海化工有限公司 Method for producing pyridone from chloroacetic acid waste liquid
CN103086960A (en) * 2011-10-27 2013-05-08 山西康得利精细化工有限公司 Novel process for producing chlopyrifos from pyridone by using aqueous phase method
CN103086959A (en) * 2011-10-27 2013-05-08 山西三维丰海化工有限公司 Novel process for producing 3,5,6-sodium trichloropyrindinol
CN103193705A (en) * 2013-03-22 2013-07-10 浙江工业大学 Synthesis method of 2-chloronicotinic acid and derivative thereof
CN103274996B (en) * 2013-05-02 2015-08-19 江苏九九久科技股份有限公司 The one kettle way of improvement prepares the method for 3,5,6-trichloropyridine-2-sodium alkoxide
CN103819397B (en) * 2014-03-14 2015-12-30 杨雪飞 A kind of efficient catalytic synthetic method of heterocyclic alcohol
CN104876858A (en) * 2015-05-13 2015-09-02 安徽国星生物化学有限公司 One-pot method for synthesizing sodium 3,5,6-trichloropyridin-2-olate

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3007931A (en) * 1959-03-09 1961-11-07 Phillips Petroleum Co Production of unsaturated heterocyclic nitrogen bases
US4245098A (en) * 1978-12-05 1981-01-13 Ciba-Geigy Corporation Process for producing 2,3,5-trichloropyridine, 2,4,4-trichloro-4-formyl-butyronitrile as a novel compound and a process for producing it
DE3070085D1 (en) * 1979-11-30 1985-03-14 Ciba Geigy Ag Process for the preparation of 2,3,5,6-tetrachloropyridine and 3,5,6-trichloropyridin-2-ol
US4469896A (en) * 1981-08-17 1984-09-04 Ciba-Geigy Corporation Process for the production of chloropyridines substituted by methyl, trichloromethyl or trifluoromethyl groups
US4435573A (en) * 1982-10-25 1984-03-06 The Dow Chemical Company Process for the preparation of substituted pyridines
US4468354A (en) * 1983-02-15 1984-08-28 The Dow Chemical Company Continuous process for preparing 5-oxo-2,4-dichloro-4-substituted pentanenitriles
US4465186A (en) * 1983-07-14 1984-08-14 Meyers Jonathan H Holder for clips
AR243869A1 (en) * 1987-06-05 1993-09-30 Quimica Estrella Aca Sa A procedure for synthesising 2-hydroxy-3,5,6-trichloropyridine.
JPS63313771A (en) * 1987-06-15 1988-12-21 Nippon Kayaku Co Ltd Production of 3,5,6-trichloro-2-pyridinol
IL86341A (en) * 1988-05-11 1992-02-16 Pamol Ltd Preparation of polychloropyridine derivatives and intermediates therefor

Also Published As

Publication number Publication date
CN1047281A (en) 1990-11-28
FI97132C (en) 1996-10-25
HU205078B (en) 1992-03-30
AU5494590A (en) 1990-11-15
KR0153446B1 (en) 1998-11-16
US4996323A (en) 1991-02-26
NZ233615A (en) 1992-06-25
HU913709D0 (en) 1992-02-28
ATE144979T1 (en) 1996-11-15
UA19168A1 (en) 1997-12-25
AU620245B2 (en) 1992-02-13
DE69029052D1 (en) 1996-12-12
CA2016620A1 (en) 1990-11-12
JPH035458A (en) 1991-01-11
HU903008D0 (en) 1990-09-28
DE69029052T2 (en) 1997-03-06
CN1027259C (en) 1995-01-04
FI97132B (en) 1996-07-15
DK0397281T3 (en) 1997-04-14
RU1839671C (en) 1993-12-30
KR900018028A (en) 1990-12-20
FI902363A0 (en) 1990-05-11
IL94373A0 (en) 1991-03-10
IL94373A (en) 1994-06-24
EP0397281B1 (en) 1996-11-06
BR9001798A (en) 1991-06-11
ES2095854T3 (en) 1997-03-01
CA2016620C (en) 2001-05-08
EP0397281A3 (en) 1991-10-02
JP2829342B2 (en) 1998-11-25
HUT54984A (en) 1991-04-29
EP0397281A2 (en) 1990-11-14

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