MA32520B1 - ELABORATION OF CATHODE MATERIALS NaxVOPO4, nH2O IN THIN FILM - Google Patents

ELABORATION OF CATHODE MATERIALS NaxVOPO4, nH2O IN THIN FILM

Info

Publication number
MA32520B1
MA32520B1 MA32467A MA32467A MA32520B1 MA 32520 B1 MA32520 B1 MA 32520B1 MA 32467 A MA32467 A MA 32467A MA 32467 A MA32467 A MA 32467A MA 32520 B1 MA32520 B1 MA 32520B1
Authority
MA
Morocco
Prior art keywords
thin film
naxvopo4
nh2o
studied
oxidation
Prior art date
Application number
MA32467A
Other languages
Arabic (ar)
French (fr)
Inventor
Guessous Aicha
Bououd Sahar
Elhourch Abderrahim
Elkacemi Kacem
Original Assignee
Univ Mohammed V Agdal
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Univ Mohammed V Agdal filed Critical Univ Mohammed V Agdal
Priority to MA32467A priority Critical patent/MA32520B1/en
Priority to PCT/MA2010/000022 priority patent/WO2011081507A2/en
Publication of MA32520B1 publication Critical patent/MA32520B1/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D9/00—Electrolytic coating other than with metals
    • C25D9/04—Electrolytic coating other than with metals with inorganic materials
    • C25D9/06—Electrolytic coating other than with metals with inorganic materials by anodic processes
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00—Phosphorus; Compounds thereof
    • C01B25/16—Oxyacids of phosphorus; Salts thereof
    • C01B25/26—Phosphates
    • C01B25/45—Phosphates containing plural metal, or metal and ammonium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G31/00—Compounds of vanadium
    • C01G31/006—Compounds containing, besides vanadium, two or more other elements, with the exception of oxygen or hydrogen
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C25B1/01—Products
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D9/00—Electrolytic coating other than with metals
    • C25D9/04—Electrolytic coating other than with metals with inorganic materials
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/04—Processes of manufacture in general
    • H01M4/0438—Processes of manufacture in general by electrochemical processing
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/136—Electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
    • H01M4/139—Processes of manufacture
    • H01M4/1397—Processes of manufacture of electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M4/36—Selection of substances as active materials, active masses, active liquids
    • H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/02—Electrodes composed of, or comprising, active material
    • H01M2004/021—Physical characteristics, e.g. porosity, surface area
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10—Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Paints Or Removers (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)

Abstract

فيلم رقيق من نوع naxvopo4، nh2o يتم ترسبه الكهرلي انطلاقا من محلول مائي يحتوي على 0,1m من سولفات الفانديل،1m من حامض الفوسفوريك المعدل في درجة حموضة (1،9؛2؛2،1). يتم انجاز صياغة الفيلم الرقيق من خلال الأكسدة الغالفانية الثابتة. أو من خلال التدوير الفولتي-الأمبيري. يجري تفاعل الترسب الكهرلي في مرحلتين: الأكسدة إلى أنواع قابلة للذوبان متبوعة بعملية ترسيب. تتم دراسة تأثير متغيرات التوليف على تحضير فيلم رقيق من نوع naxvopo4، nh2o.البنية البلورية للترسبات المدروسة من خلال حيود الأشعة السينية تم ربطها بشكل سليم بالبنية المتعددة الأضلاع na0,45 vopo4 1,58h2o. الدراسة المورفولوجية تم انجازها بالمجهر الإلكتروني الماسح وكشفت عن سطح متجانس. حجم البلورات الدقيقة التي تم حسابها من خلال خطوط مرسومة (002) (023) و (131) بواسطة معادلة "شيرير" scherrer هو في حدود 30 نانومتر.Thin film of type naxvopo4, nh2o is electrolytic deposition from an aqueous solution containing 0,1m of vandel sulfate, 1 m of phosphoric acid modified at pH (1,9; 2; 2,1). The thin film formulation is accomplished by constant galvanic oxidation. Or through amperage. The electrolyte deposition reaction takes place in two stages: oxidation into soluble species followed by a deposition process. The effect of synthesis variables on the preparation of a thin film of naxvopo4, nh2o is studied. The crystal structure of the sediments studied by X-ray diffraction has been properly linked to the polygonal structure na0,45 vopo4 1,58h2o. The morphological study was performed by scanning electron microscopy and revealed a homogeneous surface. The size of the fine crystals calculated by drawn lines (002) (023) and (131) by the Scherrer equation is in the range of 30 nm.

MA32467A 2009-12-31 2009-12-31 ELABORATION OF CATHODE MATERIALS NaxVOPO4, nH2O IN THIN FILM MA32520B1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
MA32467A MA32520B1 (en) 2009-12-31 2009-12-31 ELABORATION OF CATHODE MATERIALS NaxVOPO4, nH2O IN THIN FILM
PCT/MA2010/000022 WO2011081507A2 (en) 2009-12-31 2010-12-24 Production of thin-film naxvopo4, nh2o cathodic materials

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
MA32467A MA32520B1 (en) 2009-12-31 2009-12-31 ELABORATION OF CATHODE MATERIALS NaxVOPO4, nH2O IN THIN FILM

Publications (1)

Publication Number Publication Date
MA32520B1 true MA32520B1 (en) 2011-08-01

Family

ID=44246945

Family Applications (1)

Application Number Title Priority Date Filing Date
MA32467A MA32520B1 (en) 2009-12-31 2009-12-31 ELABORATION OF CATHODE MATERIALS NaxVOPO4, nH2O IN THIN FILM

Country Status (2)

Country Link
MA (1) MA32520B1 (en)
WO (1) WO2011081507A2 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111403181A (en) * 2019-05-01 2020-07-10 江西师范大学 Method for preparing capacitor cathode material with ultrahigh capacity and stability
CN111646452A (en) * 2020-06-17 2020-09-11 广东工业大学 Nano flaky hydrated sodium vanadyl phosphate cathode material and preparation method and application thereof

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4376709A (en) 1980-11-10 1983-03-15 Exxon Research And Engineering Co. Intercalated layered mixed oxides
US4465846A (en) 1981-11-12 1984-08-14 The Standard Oil Company Preparation of maleic anhydride
CA2442257C (en) * 2001-04-06 2013-01-08 Valence Technology, Inc. Sodium ion batteries

Also Published As

Publication number Publication date
WO2011081507A3 (en) 2011-09-09
WO2011081507A2 (en) 2011-07-07

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