LU102852B1 - Process for continuous extraction of lignocellulosic material - Google Patents

Process for continuous extraction of lignocellulosic material

Info

Publication number
LU102852B1
LU102852B1 LU102852A LU102852A LU102852B1 LU 102852 B1 LU102852 B1 LU 102852B1 LU 102852 A LU102852 A LU 102852A LU 102852 A LU102852 A LU 102852A LU 102852 B1 LU102852 B1 LU 102852B1
Authority
LU
Luxembourg
Prior art keywords
lignocellulosic material
pressate
flow rate
solvent
extractor
Prior art date
Application number
LU102852A
Inventor
Marc CONRAD
Irina Smirnova
Original Assignee
Technische Univ Hamburg
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Technische Univ Hamburg filed Critical Technische Univ Hamburg
Priority to LU102852A priority Critical patent/LU102852B1/en
Priority to PCT/EP2022/071526 priority patent/WO2023012094A1/en
Priority to KR1020247003969A priority patent/KR20240035817A/en
Priority to CN202280053498.0A priority patent/CN117751215A/en
Application granted granted Critical
Publication of LU102852B1 publication Critical patent/LU102852B1/en

Links

Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/20Pulping cellulose-containing materials with organic solvents or in solvent environment

Abstract

The invention provides a process for continuous extraction of lignocellulosic material, the process comprising at least one stage comprising the steps of a) conveying the lignocellulosic material into an extractor, b) forming, in the extractor, a suspension of the lignocellulosic material and a solvent, c) extracting the lignocellulosic material in the extractor with the solvent, d) withdrawing part of the suspension from the extractor and conveying it to a pressing device at a flow rate m4, e) separating the solvent from the lignocellulosic material by pressing off the solvent from the lignocellulosic material in the pressing device and conveying pressed-off solvent as a pressate to a pressate tank at a flow rate rh7, f) withdrawing pressed lignocellulosic material from the pressing device at a flow rate rh6, g) returning a first part of the pressate from the pressate tank at a flow rate rh8 into the extractor, h) withdrawing a second part of the pressate as an extract from the pressate tank at a flow rate rh9, i) Adding solvent to the lignocellulosic material in any one or more of steps a, b, c, d, e or g at a flow rate m2.
LU102852A 2021-08-02 2021-08-02 Process for continuous extraction of lignocellulosic material LU102852B1 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
LU102852A LU102852B1 (en) 2021-08-02 2021-08-02 Process for continuous extraction of lignocellulosic material
PCT/EP2022/071526 WO2023012094A1 (en) 2021-08-02 2022-08-01 Process for continuous extraction of lignocellulosic material
KR1020247003969A KR20240035817A (en) 2021-08-02 2022-08-01 Continuous extraction method for lignocellulosic materials
CN202280053498.0A CN117751215A (en) 2021-08-02 2022-08-01 Method for continuous extraction of lignocellulosic material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
LU102852A LU102852B1 (en) 2021-08-02 2021-08-02 Process for continuous extraction of lignocellulosic material

Publications (1)

Publication Number Publication Date
LU102852B1 true LU102852B1 (en) 2023-02-02

Family

ID=78073964

Family Applications (1)

Application Number Title Priority Date Filing Date
LU102852A LU102852B1 (en) 2021-08-02 2021-08-02 Process for continuous extraction of lignocellulosic material

Country Status (2)

Country Link
CN (1) CN117751215A (en)
LU (1) LU102852B1 (en)

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2007051269A1 (en) * 2005-11-01 2007-05-10 Dedini S/A. Indústrias De Base Improvements in a process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor
WO2012110231A1 (en) 2011-02-16 2012-08-23 Rheinisch-Westfälische Technische Hochschule Integrated process for the selective fractionation and separation of lignocellulose in its main components
EP2520608A1 (en) 2005-07-19 2012-11-07 Inbicon A/S Method for continuous hydrothermal pretreatment of lignocellulosic biomass
US8772427B2 (en) 2008-11-26 2014-07-08 Lignol Innovations Ltd. Continuous counter-current organosolv processing of lignocellulosic feedstocks
US8822657B2 (en) 2006-05-08 2014-09-02 Vertichem Corporation Recovery of lignin and water soluble sugars from plant materials
EP2862890A1 (en) 2012-05-03 2015-04-22 Virdia Ltd. Method for the extraction of lignin from biomass
WO2015134314A1 (en) * 2014-03-03 2015-09-11 Api Intellectual Property Holdings, Llc Processes utilizing fermentation vinasse for producing energy-dense biomass and biomass sugars
US9624449B2 (en) 2009-11-30 2017-04-18 Applied Biorefinery Sciences LLC. Biorefinery process for extraction, separation and recovery of fermentable saccharides, other useful compounds, and yield of improved lignocellulosic material from plant biomass
WO2018114905A1 (en) 2016-12-21 2018-06-28 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Two-stage digestion method for chemical fractionation of lignocellulose
US20210087590A1 (en) * 2017-12-20 2021-03-25 IFP Energies Nouvelles Method for treating lignocellulosic biomass by impregnation

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2520608A1 (en) 2005-07-19 2012-11-07 Inbicon A/S Method for continuous hydrothermal pretreatment of lignocellulosic biomass
WO2007051269A1 (en) * 2005-11-01 2007-05-10 Dedini S/A. Indústrias De Base Improvements in a process for rapid acid hydrolysis of lignocellulosic material and in a hydrolysis reactor
US8822657B2 (en) 2006-05-08 2014-09-02 Vertichem Corporation Recovery of lignin and water soluble sugars from plant materials
US8772427B2 (en) 2008-11-26 2014-07-08 Lignol Innovations Ltd. Continuous counter-current organosolv processing of lignocellulosic feedstocks
US9624449B2 (en) 2009-11-30 2017-04-18 Applied Biorefinery Sciences LLC. Biorefinery process for extraction, separation and recovery of fermentable saccharides, other useful compounds, and yield of improved lignocellulosic material from plant biomass
WO2012110231A1 (en) 2011-02-16 2012-08-23 Rheinisch-Westfälische Technische Hochschule Integrated process for the selective fractionation and separation of lignocellulose in its main components
EP2862890A1 (en) 2012-05-03 2015-04-22 Virdia Ltd. Method for the extraction of lignin from biomass
WO2015134314A1 (en) * 2014-03-03 2015-09-11 Api Intellectual Property Holdings, Llc Processes utilizing fermentation vinasse for producing energy-dense biomass and biomass sugars
WO2018114905A1 (en) 2016-12-21 2018-06-28 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Two-stage digestion method for chemical fractionation of lignocellulose
US20210087590A1 (en) * 2017-12-20 2021-03-25 IFP Energies Nouvelles Method for treating lignocellulosic biomass by impregnation

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
A. PATELA.R. SHAH: "Integrated lignocellulosic biorefinery: Gateway for production of second generation ethanol and value added products", JOURNAL OF BIORESOURCES AND BIOPRODUCTS
CONRAD, M.HARING, H.SMIRNOVA, I.: "Design of an industrial autohydrolysis pretreatment plant for annual lignocellulose", BIOMASS CONV. BIOREF., 2019
CONRAD, M.SMIRNOVA, I.: "Two-Step Autohydrolysis Pretreatment: Towards High Selective Full Fractionation of Wheat Straw", CHEMIE INGENIEUR TECHNIK, vol. 92, 2020, pages 1723 - 1732
RUIZ, H.A.CONRAD, M.SUN, S.SANCHEZ, A.ROCHA, G.ROMANI, A.CASTRO, E.TORRES, A.RODRIGUEZ-JASSO, R.M.ANDRADE, L.P.: "Engineering aspects of hydrothermal pretreatment: From batch to continuous operation, scale-up and pilot reactor under biorefinery concept", BIORESOURCE TECHNOLOGY, 2019, pages 122685

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Legal Events

Date Code Title Description
FG Patent granted

Effective date: 20230202

PD Change of ownership

Owner name: MUSHLABS GMBH; DE

Free format text: FORMER OWNER: TECHNISCHE UNIVERSITAET HAMBURG

Effective date: 20231207