KR960705888A - Binders based on fatty chemical reaction products [BINDERS BASED ON FAT CHEMICAL REACTION PRODUCTS] - Google Patents

Binders based on fatty chemical reaction products [BINDERS BASED ON FAT CHEMICAL REACTION PRODUCTS]

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Publication number
KR960705888A
KR960705888A KR1019960702046A KR19960702046A KR960705888A KR 960705888 A KR960705888 A KR 960705888A KR 1019960702046 A KR1019960702046 A KR 1019960702046A KR 19960702046 A KR19960702046 A KR 19960702046A KR 960705888 A KR960705888 A KR 960705888A
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South Korea
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compound
binder
adhesive
aliphatic
acid
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KR1019960702046A
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Korean (ko)
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클라우크 볼프강
루스트 에른스트-울리히
빌레케 루트거
다우테 페터
클라인 요한
슈트루베 알프레트
Original Assignee
게오르그 챠이트 · 요한 글라슬
헨켈 코만디트게젤샤프트 아우프 아크티엔
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Priority claimed from PCT/EP1994/003351 external-priority patent/WO1995011284A2/en
Publication of KR960705888A publication Critical patent/KR960705888A/en

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    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
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    • C09F—NATURAL RESINS; FRENCH POLISH; DRYING-OILS; OIL DRYING AGENTS, i.e. SICCATIVES; TURPENTINE
    • C09F7/00—Chemical modification of drying oils
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
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    • C04B24/026—Fatty alcohols
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
    • C04B24/08—Fats; Fatty oils; Ester type waxes; Higher fatty acids, i.e. having at least seven carbon atoms in an unbroken chain bound to a carboxyl group; Oxidised oils or fats
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    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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    • C08K5/00—Use of organic ingredients
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    • C08K5/10—Esters; Ether-esters
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/04—Oxygen-containing compounds
    • C08K5/10—Esters; Ether-esters
    • C08K5/101—Esters; Ether-esters of monocarboxylic acids
    • C08K5/103—Esters; Ether-esters of monocarboxylic acids with polyalcohols
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    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
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    • C08L91/00—Compositions of oils, fats or waxes; Compositions of derivatives thereof
    • C08L91/005—Drying oils
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    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D131/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid, or of a haloformic acid; Coating compositions based on derivatives of such polymers
    • C09D131/02—Homopolymers or copolymers of esters of monocarboxylic acids
    • C09D131/04—Homopolymers or copolymers of vinyl acetate
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    • C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J1/00—Adhesives based on inorganic constituents
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    • C09J11/02—Non-macromolecular additives
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    • C09J11/08—Macromolecular additives
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    • C09J125/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Adhesives based on derivatives of such polymers
    • C09J125/02—Homopolymers or copolymers of hydrocarbons
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    • C09J127/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Adhesives based on derivatives of such polymers
    • C09J127/02—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Adhesives based on derivatives of such polymers not modified by chemical after-treatment
    • C09J127/04—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Adhesives based on derivatives of such polymers not modified by chemical after-treatment containing chlorine atoms
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    • C09J131/00—Adhesives based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid, or of a haloformic acid; Adhesives based on derivatives of such polymers
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    • C09J191/00—Adhesives based on oils, fats or waxes; Adhesives based on derivatives thereof
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    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2666/00—Composition of polymers characterized by a further compound in the blend, being organic macromolecular compounds, natural resins, waxes or and bituminous materials, non-macromolecular organic substances, inorganic substances or characterized by their function in the composition
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Abstract

반응 생성물은 1,500 이상의 분자량을 갖으며, A) 지방 라티칼로 후술 작용기-OH, -SH, -NH2, -C=C-, -COOH, 무수물기 또는 에폭시드기의 1종 이상을 평균 1 내지 10, 바람직하게는 1.5 내지 6개 갖는 지방(지방은 적어도 삼작용기 지방을 1 몰% 이상 함유한다)과 B) 1종 이상의 지방의 작용와 반응할 수 있는 단일 또는 다작용기 화합물을 반응시켜 제조한다. 반등 생성물은 바람직하게는 수중의 액체로 분산된다. 상기 결합제는 도포, 밀봉 및 결합, 특히 단독 또는 공지된 접착제 및 중합체 분산액과 배합하여 접착처리하는데 적합하다. 접착 분산액, 압력-민감 물질, 보편적인 접착제 및 접착성 스틱은 특히 상기 결합제로부터 제조할 수 있다.The reaction product has a molecular weight of 1,500 or more, and A) is a fatty radical, which averages 1 to 10 or more of the following functional groups -OH, -SH, -NH 2 , -C = C-, -COOH, anhydride group or epoxide group. , Preferably from 1.5 to 6 fats (fats contain at least 1 mol% of trifunctional fats) and B) single or multifunctional compounds capable of reacting with the action of one or more fats. The rebound product is preferably dispersed in a liquid in water. The binder is suitable for applying, sealing and bonding, in particular for adhesion treatment alone or in combination with known adhesives and polymer dispersions. Adhesive dispersions, pressure-sensitive materials, universal adhesives and adhesive sticks can in particular be prepared from such binders.

Description

지방 화학 반응 생성물 기재의 결합제 [BINDERS BASED ON FAT CHEMICAL REACTION PRODUCTS]Binders based on fatty chemical reaction products [BINDERS BASED ON FAT CHEMICAL REACTION PRODUCTS]

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음Since this is an open matter, no full text was included.

Claims (15)

A) 지방족 성분으로 후술 작용기: -OH, -COOH, -SH, -NH2, -C=C-, 무수물기 또는 에폭시드기중의 1종 이상을 평균 1 내지 10, 바람직하게는 1.5 내지 6개 함유하는 1종 이상의 지방족 화합물(지방족 화합물은 삼작용기 지방족 분자를 1 몰% 이상 함유한다)과, B) 지방족 화합물의 작용기가 반응할 수 있는 1종 이상의 단일 또는 다작용기 화합물의 반응 생성물을 기재로하고 분자량이 1,500 이상인 결합제.A) one or more of the following functional groups as the aliphatic component: -OH, -COOH, -SH, -NH 2 , -C = C-, anhydride group or epoxide group, on average 1 to 10, preferably 1.5 to 6 Based on the reaction product of at least one aliphatic compound containing (the aliphatic compound contains at least 1 mol% of trifunctional aliphatic molecules) and at least one single or multifunctional compound to which the functional groups of the aliphatic compound can react. And a binder having a molecular weight of at least 1,500. 제1항에 있어서 분자량이 〉200, 더 구체적으로는 〉300, 바람직하게는 〉800이며, 포화, 불포화, 비분지 또는 분지된 지방산, 탄소수8 이상의 지방 알코올 및 이의 에스테르, 더 구체적으로는 고지방산의 트리글리세라이드, 바람직하게는 천연 형태 및 열처리 및/또는 산화 처리 또는 에폭시드화 후 또는 친핵체의 첨가후의, 천연 유지로 이루어진 지방족 화합물의 군으로부터 선택된 1종 이상의 물질을 사용하는 것을 특징으로 하는 결합제.A fatty acid according to claim 1 having a molecular weight of > 200, more specifically > 300, preferably > 800, saturated, unsaturated, unbranched or branched fatty acids, fatty alcohols having 8 or more carbon atoms and esters thereof, more particularly high fatty acids. A binder characterized by using at least one substance selected from the group of aliphatic compounds consisting of natural fats and oils, preferably in natural form and after heat treatment and / or oxidation treatment or epoxidation or addition of nucleophiles. 제1 또는 2항에 있어서, 지방족 화합물이 친유성인 결합제.The binder according to claim 1 or 2, wherein the aliphatic compound is lipophilic. 제1 내지 3항 중 어느 한 항에 있어서, 작용기 화합물 B)의 분자량이 20,000 미만, 더 구체적으로 8,000미만, 바람직하게는 2,000 미만인 것을 특징으로 하는 결합제.The binder according to any one of claims 1 to 3, wherein the molecular weight of functional compound B) is less than 20,000, more specifically less than 8,000, preferably less than 2,000. 제1내지 4항 중 어느 한 항에 있어서, 에폭시드기를 함유하는 지방족 화합물 및 작용기의 평균수가 바람직하게는 1.5 내지 5이고, 폴리올, 폴리아민, 아미노알코올 및 폴리카르복실산, 더 구체적으로는 이량체 지방산 및 이량체 알코올인 다작용기 화합물 B)를 특징으로 하는 결합제.The average number of aliphatic compounds and functional groups containing epoxide groups is preferably 1.5 to 5, polyols, polyamines, aminoalcohols and polycarboxylic acids, more specifically dimers according to any one of claims 1 to 4. A binder characterized by a multifunctional compound B) which is a fatty acid and a dimer alcohol. 제1 내지 4항 중 어느 한 항에 있어서, OH 및/또는 NH2기를 함유하는 지방족 화합물 및 작용기의 평균수는 바람직하게는 1.5 내지 5이고, 무수 폴리카르복실산, 폴리이소시아네이트, 폴리에폭시드 및/또는 폴리카르복실산 염화물인 다작용기 화합물 B)를 특징으로 하는 결합제.The average number of aliphatic compounds and functional groups containing OH and / or NH 2 groups is preferably 1.5 to 5, and anhydrous polycarboxylic acids, polyisocyanates, polyepoxides and / or Or a polyfunctional compound B) which is a polycarboxylic acid chloride. 제1 내지 4항 중 어느 한 항에 있어서, 처음에는 무수말레인산, 메타크릴산 및 아크릴산과 같은 친디엔체와 반응하고, 이어서 추가로 폴리아민, 폴리올 또는 아미노알코올과 반응하는, C=C 이중 결합을 포함하며, 작용기의 평균수는 바람직하게는 1.5 내지 5인 지방족 화합물을 특징으로 하는 결합제.The C = C double bond according to any one of claims 1 to 4, wherein the C = C double bond is first reacted with a dienophile such as maleic anhydride, methacrylic acid and acrylic acid, followed by further reaction with a polyamine, polyol or aminoalcohol. And an average number of functional groups is preferably 1.5 to 5 binders. 제1 내지 4항 중 어느 한 항에 있어서, C=C 이중 결합을 포함하는 지방족 화합물을 산소,라디칼 개시제의 존재 또는 상승된 온도에서 반응시키는 것을 특징으로 하는 결합제.The binder according to any one of claims 1 to 4, wherein the aliphatic compound containing a C = C double bond is reacted in the presence of an oxygen or radical initiator or at an elevated temperature. 제1 내지 4항 또는 제8항 중 어느 한 항에 있어서, 올레핀계 C=C 이중 결합을 포함하는 라디칼-중합성 화합물의 존재하에서, 더 구체적으로는 1종 이상의 스티렌, 비닐 에스테르, 비닐 클로라이드 부타디엔, 에틸렌, 아크릴산, (메트)아크릴레이트, 크로톤산, 아크릴로니트릴 또는 이들 단량체의 혼합물인 단량체의 존재하에서 반응되는 C=C 이중 결합을 포함하는 지방 화합물을 특징으로 하는 결합제.The process according to any one of claims 1 to 4 or 8, in the presence of a radical-polymerizable compound comprising an olefinic C = C double bond, more specifically at least one styrene, vinyl ester, vinyl chloride butadiene A binder characterized by a fatty compound comprising a C = C double bond which is reacted in the presence of a monomer which is ethylene, acrylic acid, (meth) acrylate, crotonic acid, acrylonitrile or a mixture of these monomers. 제1 내지 9항 중 어느 한 항에 있어서, 최상으로는 염기(예, NAOH 및 아민), 유화제(예, 비이온성 계면활성제, 에테르 술폰산 및 에테르 카르복실산) 및/또는 보호성 콜로이드와 같은 보조제를 사용하여, 바람직하게는 강력하게 전단하면서, 특히 반응 생성물을 수중의 액체 형태로 분산시키거나-선택적으로는 50~150。C로 가열한 후-또는, 역으로, 반응 생성물중의 물 형태로 분산시켜 수성 분산액의 형태로 제조되는 것을 특징으로 하는 결합제.10. The adjuvant according to any one of claims 1 to 9, wherein at best it is a base (e.g. NAOH and amine), an emulsifier (e.g. nonionic surfactant, ether sulfonic acid and ether carboxylic acid) and / or protective colloids. Using, preferably, while shearing strongly, in particular dispersing the reaction product in liquid form in water or optionally heating to 50-150 ° C., or vice versa, in the form of water in the reaction product. A binder, which is prepared in the form of an aqueous dispersion by dispersion. 제10항에 있어서, 반응 생성물의 분자량이 최상으로는 경화제 및/또는 개시제를 사용하여 분산시킨 후 증가되는 것을 특징으로 하는 결합제.11. The binder according to claim 10, wherein the molecular weight of the reaction product is best increased after dispersing with a curing agent and / or initiator. 바람직하게는 결합 중합쳉에 대해, 2 내지 90중량%의 % 함량으로 시판용 중합체 분산액 또는 접착제와 혼합된, 도포, 밀봉, 주조 및 결합용으로 사용되는 제1 내지 11항 중 어느 한 항에서 청구된 결합제의 용도.Claims 1 to 11 used for coating, sealing, casting and bonding, preferably mixed with commercially available polymer dispersions or adhesives in a% content of 2 to 90% by weight relative to the binder polymerization. Use of binders. 제12항에 있어서, 중합체 분산액 및 접착제가 20 내지 80중량%의 고형 함량으로 카제인, 글루틴, 셀룰로오스 에테르, 전분, 덱스트린, 폴리비닐 피롤리돈, 폴리비닐 알코올, 폴리메타크릴레이트, 폴리비닐 클로라이드, 폴리비닐 알코올, 폴리메타크릴레이트, 폴리 비닐 클로라이드, 폴리부타디엔, 폴리스티렌, 스티렌/아크릴레이트 공중합체, 스티렌/부타디엔 공중합체, 폴리비닐 에스테르 및 폴리우레탄을 기재로 하는 것을 특징으로 하는 결합제의 용도.13. The polymer dispersion and adhesive according to claim 12, wherein the polymer dispersion and the adhesive are casein, glutin, cellulose ether, starch, dextrin, polyvinyl pyrrolidone, polyvinyl alcohol, polymethacrylate, polyvinyl chloride in a solid content of 20 to 80% by weight. , Polyvinyl alcohol, polymethacrylate, polyvinyl chloride, polybutadiene, polystyrene, styrene / acrylate copolymers, styrene / butadiene copolymers, polyvinyl esters and polyurethanes. 접착제는 접착성 분산액, 촉압 접착제, 다목적 접착제, 용제-기재 접착제 또는 접착성 스틱이고, 밀봉 화합물은 접합 화합물이며, 경질 표면을 갖는 기재, 직물 및 종이를 도포하는 것을 특징으로 하는 제1 내지 13항 중의 어느 한 항에서 청구한 분산액의 용도.The adhesive is an adhesive dispersion, a tack adhesive, a multipurpose adhesive, a solvent-based adhesive or an adhesive stick, and the sealing compound is a bonding compound, characterized by applying a substrate, fabric and paper having a hard surface. Use of the dispersion claimed in any one of claims. 제12 내지 14항 중 어느 한 항에 있어서, 목재, 판지,종이, 벽 피복재 (예, 벽지), 코르크, 가죽,고무, 벨트, 직물,플라스틱, 더 구체적으로는 필름 또는 쉬트형 직물 형태인 PVC, 리놀레움 및 폴리올레핀의 바닥 피복재, 유리, 석영, 슬래그, 암석 및 세라믹과 같은 광물성 기재 및 금속의 결합, 도포 및 밀봉을 특징으로 하는 용도.15. PVC according to any of claims 12 to 14, in the form of wood, cardboard, paper, wall coverings (e.g. wallpaper), cork, leather, rubber, belts, textiles, plastics, more specifically films or sheet-like fabrics. , Characterized by the bonding, application and sealing of metals and mineral bases such as glass, quartz, slag, rocks and ceramics, floor coverings of linoleum and polyolefins. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019960702046A 1993-10-20 1994-10-12 Binders based on fatty chemical reaction products [BINDERS BASED ON FAT CHEMICAL REACTION PRODUCTS] KR960705888A (en)

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DE4335672 1993-10-20
DEP4335672.9 1993-10-20
DE4430875A DE4430875A1 (en) 1993-10-20 1994-08-31 binder
DEP4430875.2 1994-08-31
PCT/EP1994/003351 WO1995011284A2 (en) 1993-10-20 1994-10-12 Binders based on fat chemical reaction products

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US5607633A (en) * 1995-07-13 1997-03-04 Archer Daniels Midland Company Co-adhesive system for bonding wood, fibers, or agriculture based composite materials
DE19734302A1 (en) * 1997-08-08 1999-02-11 Fischer Artur Werke Gmbh Curable mortar
AU1950801A (en) * 1999-12-17 2001-06-25 Archer-Daniels-Midland Company Glyceride oil based waxes
US20050075428A1 (en) * 2001-04-19 2005-04-07 W.F. Taylor Co., Inc. Low emissions one part adhesive
DE102005051716A1 (en) * 2005-10-27 2007-05-03 Fritz Egger Gmbh & Co. Binder composition for wood-based materials

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