KR960030970A - Method and apparatus for monitoring the operation of an air separation plant - Google Patents
Method and apparatus for monitoring the operation of an air separation plant Download PDFInfo
- Publication number
- KR960030970A KR960030970A KR1019960002881A KR19960002881A KR960030970A KR 960030970 A KR960030970 A KR 960030970A KR 1019960002881 A KR1019960002881 A KR 1019960002881A KR 19960002881 A KR19960002881 A KR 19960002881A KR 960030970 A KR960030970 A KR 960030970A
- Authority
- KR
- South Korea
- Prior art keywords
- nitrous oxide
- evaporator
- oxide content
- condenser
- plant
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract 8
- 238000012544 monitoring process Methods 0.000 title claims abstract 4
- 238000000926 separation method Methods 0.000 title claims 2
- GQPLMRYTRLFLPF-UHFFFAOYSA-N Nitrous Oxide Chemical compound [O-][N+]#N GQPLMRYTRLFLPF-UHFFFAOYSA-N 0.000 claims abstract 20
- 239000001272 nitrous oxide Substances 0.000 claims abstract 10
- 239000007788 liquid Substances 0.000 claims 6
- 238000004821 distillation Methods 0.000 claims 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 2
- 238000004887 air purification Methods 0.000 claims 1
- 229910052757 nitrogen Inorganic materials 0.000 claims 1
- 230000002000 scavenging effect Effects 0.000 claims 1
- 239000006227 byproduct Substances 0.000 abstract 1
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04763—Start-up or control of the process; Details of the apparatus used
- F25J3/04769—Operation, control and regulation of the process; Instrumentation within the process
- F25J3/04854—Safety aspects of operation
- F25J3/0486—Safety aspects of operation of vaporisers for oxygen enriched liquids, e.g. purging of liquids
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
- F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
- F25J3/04—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
- F25J3/04406—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system
- F25J3/04412—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a dual pressure main column system in a classical double column flowsheet, i.e. with thermal coupling by a main reboiler-condenser in the bottom of low pressure respectively top of high pressure column
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/35—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
- G01N21/3504—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing gases, e.g. multi-gas analysis
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
- F25J2220/00—Processes or apparatus involving steps for the removal of impurities
- F25J2220/52—Separating high boiling, i.e. less volatile components from oxygen, e.g. Kr, Xe, Hydrocarbons, Nitrous oxides, O3
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S62/00—Refrigeration
- Y10S62/912—External refrigeration system
- Y10S62/913—Liquified gas
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/11—Automated chemical analysis
- Y10T436/115831—Condition or time responsive
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/12—Condition responsive control
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/17—Nitrogen containing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/17—Nitrogen containing
- Y10T436/177692—Oxides of nitrogen
Landscapes
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Mechanical Engineering (AREA)
- Thermal Sciences (AREA)
- General Engineering & Computer Science (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Separation By Low-Temperature Treatments (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
본 발명은 저온 중류에 의해 공기를 분리시키기 위한 플랜트의 작동을 모니터하기 위한 방법에 있어서, 상기 플랜트의 증발기-응축기 배쓰의 아산화 질소 함량 변화를 검출하는 것을 특징으로 하는 방법에 관한 것이다.The present invention relates to a method for monitoring the operation of a plant for separating air by low temperature by-products, characterized in that a change in the nitrous oxide content of the evaporator-condenser bath of the plant is detected.
아산화 질소 함량은 적외선 분석기를 사용하여 측정할 수 있다.The nitrous oxide content can be measured using an infrared analyzer.
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음Since this is a trivial issue, I did not include the contents of the text.
Claims (10)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR95-01388 | 1995-02-07 | ||
FR9501388A FR2730172B1 (en) | 1995-02-07 | 1995-02-07 | METHOD AND APPARATUS FOR MONITORING THE OPERATION OF AN AIR SEPARATION INSTALLATION |
Publications (2)
Publication Number | Publication Date |
---|---|
KR960030970A true KR960030970A (en) | 1996-09-17 |
KR100395315B1 KR100395315B1 (en) | 2003-11-17 |
Family
ID=9475906
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019960002881A KR100395315B1 (en) | 1995-02-07 | 1996-02-07 | Method and apparatus for monitoring the operation of an air separation plant |
Country Status (12)
Country | Link |
---|---|
US (1) | US5629208A (en) |
EP (1) | EP0726434B2 (en) |
JP (1) | JP2875502B2 (en) |
KR (1) | KR100395315B1 (en) |
CN (1) | CN1077287C (en) |
AU (1) | AU705899B2 (en) |
BR (1) | BR9600322A (en) |
CA (1) | CA2168931C (en) |
DE (1) | DE69604841T3 (en) |
ES (1) | ES2140038T5 (en) |
FR (1) | FR2730172B1 (en) |
ZA (1) | ZA96938B (en) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2774754B1 (en) | 1998-02-09 | 2000-03-03 | Air Liquide | METHOD FOR DETECTING THE PRESENCE OF IMPURITIES, LIQUID VAPORIZATION STATION AND METHOD, AND DOUBLE AIR DISTILLATION COLUMN |
DE19852020A1 (en) * | 1998-08-06 | 2000-02-10 | Linde Ag | Method and device for the low-temperature separation of air |
FR2820505B1 (en) * | 2001-02-06 | 2003-08-29 | Air Liquide | METHOD AND DEVICE FOR DETECTING HYDROCARBONS IN A GAS |
FR2839153B1 (en) * | 2002-04-25 | 2005-01-14 | Air Liquide | METHOD AND APPARATUS FOR SAMPLING CRYOGENIC LIQUIDS, AND AIR SEPARATION UNIT HAVING AT LEAST ONE SUCH INSTALLATION |
JP4624336B2 (en) * | 2006-11-20 | 2011-02-02 | 鹿島石油株式会社 | Method for detecting NOx compounds accumulated in a cryogenic separation facility |
CN100491874C (en) * | 2007-05-24 | 2009-05-27 | 武汉钢铁(集团)公司 | Method for removing nitrogen monoxide gathering in large oxygen-making machine |
EP2993432A1 (en) * | 2014-09-02 | 2016-03-09 | Linde Aktiengesellschaft | Method for the low-temperature decomposition of air and air separation plant |
FR3066597B1 (en) * | 2017-05-19 | 2022-07-01 | Air Liquide | APPARATUS FOR ANALYZING TRACES OF CONTAMINANTS IN A CRYOGENIC LIQUID |
RU2755284C2 (en) | 2017-05-19 | 2021-09-14 | Л'Эр Ликид, Сосьете Аноним Пур Л'Этюд Э Л'Эксплуатасьон Де Проседе Жорж Клод | Method for analyzing traces of pollutants in cryogenic liquid |
TWI699503B (en) * | 2019-06-28 | 2020-07-21 | 中國鋼鐵股份有限公司 | Film condenser liquid-gas ratio monitoring system and monitoring method |
CN113091402B (en) * | 2021-04-30 | 2022-02-18 | 开封迪尔空分实业有限公司 | Argon making system with single tower |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4045191A (en) * | 1972-05-11 | 1977-08-30 | Union Carbide Corporation | Radioactive krypton gas separation |
JPS5513135A (en) * | 1978-07-17 | 1980-01-30 | Hitachi Ltd | Measuring device for nitrogen content of waste water |
DE3322473A1 (en) * | 1983-06-22 | 1985-01-03 | Linde Ag, 6200 Wiesbaden | Method and device for avoiding enrichment of undesired components in a liquid medium |
JP2969358B2 (en) * | 1989-10-25 | 1999-11-02 | 日本酸素株式会社 | Control method of oxygen concentration in ultra high purity nitrogen product collected from rectification column |
JP2952855B2 (en) * | 1990-11-27 | 1999-09-27 | 電源開発株式会社 | Continuous measurement method of nitrous oxide concentration in gas |
US5313802A (en) * | 1993-02-16 | 1994-05-24 | Air Products And Chemicals, Inc. | Process to produce a krypton/xenon enriched stream directly from the main air distillation column |
FR2702040B1 (en) * | 1993-02-25 | 1995-05-19 | Air Liquide | Process and installation for the production of oxygen and / or nitrogen under pressure. |
FR2703140B1 (en) * | 1993-03-23 | 1995-05-19 | Air Liquide | Method and installation for producing gaseous oxygen and / or nitrogen gas under pressure by air distillation. |
FR2709537B1 (en) * | 1993-09-01 | 1995-10-13 | Air Liquide | Process and installation for producing oxygen and / or nitrogen gas under pressure. |
FR2709538B1 (en) * | 1993-09-01 | 1995-10-06 | Air Liquide | Method and installation for producing at least one pressurized air gas. |
FR2723184B1 (en) * | 1994-07-29 | 1996-09-06 | Grenier Maurice | PROCESS AND PLANT FOR THE PRODUCTION OF GAS OXYGEN UNDER PRESSURE WITH VARIABLE FLOW RATE |
US5507148A (en) * | 1994-10-25 | 1996-04-16 | The Boc Group, Inc. | Air separation method and apparatus to produce nitrogen |
-
1995
- 1995-02-07 FR FR9501388A patent/FR2730172B1/en not_active Expired - Fee Related
- 1995-06-05 US US08/463,741 patent/US5629208A/en not_active Expired - Lifetime
-
1996
- 1996-02-06 EP EP96400242A patent/EP0726434B2/en not_active Expired - Lifetime
- 1996-02-06 ZA ZA96938A patent/ZA96938B/en unknown
- 1996-02-06 CA CA002168931A patent/CA2168931C/en not_active Expired - Fee Related
- 1996-02-06 BR BR9600322A patent/BR9600322A/en not_active Application Discontinuation
- 1996-02-06 CN CN96102125A patent/CN1077287C/en not_active Expired - Fee Related
- 1996-02-06 ES ES96400242T patent/ES2140038T5/en not_active Expired - Lifetime
- 1996-02-06 AU AU43367/96A patent/AU705899B2/en not_active Ceased
- 1996-02-06 DE DE69604841T patent/DE69604841T3/en not_active Expired - Lifetime
- 1996-02-06 JP JP8020309A patent/JP2875502B2/en not_active Expired - Fee Related
- 1996-02-07 KR KR1019960002881A patent/KR100395315B1/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
FR2730172A1 (en) | 1996-08-09 |
JP2875502B2 (en) | 1999-03-31 |
ES2140038T3 (en) | 2000-02-16 |
CN1077287C (en) | 2002-01-02 |
US5629208A (en) | 1997-05-13 |
JPH08303947A (en) | 1996-11-22 |
FR2730172B1 (en) | 1997-03-21 |
EP0726434A1 (en) | 1996-08-14 |
EP0726434B2 (en) | 2003-10-22 |
KR100395315B1 (en) | 2003-11-17 |
AU705899B2 (en) | 1999-06-03 |
CA2168931A1 (en) | 1996-08-08 |
DE69604841T2 (en) | 2000-05-25 |
AU4336796A (en) | 1996-08-15 |
EP0726434B1 (en) | 1999-10-27 |
DE69604841T3 (en) | 2004-07-08 |
CA2168931C (en) | 2007-04-17 |
CN1143748A (en) | 1997-02-26 |
ES2140038T5 (en) | 2004-07-01 |
DE69604841D1 (en) | 1999-12-02 |
ZA96938B (en) | 1996-07-30 |
BR9600322A (en) | 1997-12-23 |
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Legal Events
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A201 | Request for examination | ||
E902 | Notification of reason for refusal | ||
E701 | Decision to grant or registration of patent right | ||
GRNT | Written decision to grant | ||
FPAY | Annual fee payment |
Payment date: 20100803 Year of fee payment: 8 |
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LAPS | Lapse due to unpaid annual fee |