KR950006065B1 - Beauty wash composition for using microemulsion - Google Patents
Beauty wash composition for using microemulsion Download PDFInfo
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- KR950006065B1 KR950006065B1 KR1019910020841A KR910020841A KR950006065B1 KR 950006065 B1 KR950006065 B1 KR 950006065B1 KR 1019910020841 A KR1019910020841 A KR 1019910020841A KR 910020841 A KR910020841 A KR 910020841A KR 950006065 B1 KR950006065 B1 KR 950006065B1
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- microemulsion
- caprate
- mixing
- wash composition
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/85—Polyesters
Abstract
Description
제1도는 통상의 계면활성제와 이소에스테르에 의한 마이크로 에멀젼 영역을 나타내는 것.1 shows the microemulsion area | region by a conventional surfactant and isoester.
제2도는 계면활성제인 폴리글리세롤 이소스테아레이트, 피이지-8 카프릴레이트/카프레이트와 이소에스테르에 의한 마이크로에멀젼 영역을 나타내는 것.Figure 2 shows the microemulsion area by the polyglycerol isostearate, Fiji-8 caprylate / caprate and isoester as surfactants.
본 발명은 비이온 계면활성제를 사용하여 마이크로 에멀젼을 만들고 이를 이용한 화장수 조성물에 관한 것이다.The present invention relates to making a micro emulsion using a nonionic surfactant and to a cosmetic composition using the same.
통상 마이크로 에멀젼이란 계면활성제에 의해 형성된 하나 또는 두 종류 액체의 미소 영역들로 구성된 열역학적으로 안정하고 등방적으로 투명한 제제이다.Microemulsions are usually thermodynamically stable and isotropically transparent formulations consisting of microregions of one or two kinds of liquids formed by surfactants.
따라서 다음과 같은 장점 때문에 공업적으로 여러 분야에 이용되어 왔다. 즉, 마이크로 에멀젼은 제조가 용이하고, 열역학적으로 안정되어 경시변화가 적으며 매우 작은 계면장력과 입자크기로 높은 침투능력을 갖는다. 그러나 단점으로 전통적인 에멀젼 보다 많은 양의 계면활성제가 요구되어 피부 도포 제품의 경우 자극성이 문제점으로 대두되어 두발제품이나 세정제 또는 단시간 피부에 적용하는 의약제제로써 이용이 국한되어 왔다.Therefore, it has been used in various fields industrially because of the following advantages. That is, the microemulsion is easy to prepare, thermodynamically stable, has little change over time, and has a very small interfacial tension and high penetration ability with a particle size. However, as a disadvantage, a larger amount of surfactant is required than a conventional emulsion, and thus, a skin irritation problem has arisen in the case of a skin coating product, and thus it has been limited to use as a pharmaceutical product applied to a hair product, a detergent or a short time skin.
따라서 본 발명자들은 상기의 문제점을 해결코자 예의 연구한 결과 이소에스테르종류의 유연제와 글리세릴 카프릴레이트/카프레이트, 폴리글리세롤 이소스테아레이트, 피이지-8 카프릴레이트/카프레이트 같은 계면활성제를 사용함으로써 피부에 유연, 보습효과를 부여하면서도 경시 안정성이 양호하고 특히 현재까지 통상의 마이크로에멀젼은 다량의 계면활성제 사용(미국 특허 제4,722,904호)으로 계면활성제 자체에 의한 피부자극뿐만 아니라, 계면활성제는 피부자극을 주는 원료의 피부침투를 용이하게 함으로써 피부자극을 유발시키는바, 본 발명자들은 적은 양의 계면활성제를 사용하여 마이크로 에멀젼을 안정화시킴으로써 피부자극성 문제를 해결할 수 있는 본 발명을 완성하게 되었다.Therefore, the present inventors have conducted studies to solve the above problems, and as a result, a softener of isoester type and a surfactant such as glyceryl caprylate / caprate, polyglycerol isostearate, and Fiji-8 caprylate / caprate are used. By providing softness and moisturizing effect to the skin, it has good stability over time. In particular, the conventional microemulsion has used a large amount of surfactants (US Pat. No. 4,722,904). The skin irritation is induced by facilitating skin penetration of a stimulating raw material, and the present inventors have completed the present invention which can solve the skin irritation problem by stabilizing the micro emulsion using a small amount of surfactant.
이하 본 발명을 상세히 설명하면 다음과 같다.Hereinafter, the present invention will be described in detail.
본 발명은 화장수를 제조하는데 있어서 1.0-2.0중량부의 이소에스테르에 1.5-3.0중량부의 피이지-8 카프릴레이트/카프레이트, 2.0-3.0중량부의 폴리글리세롤 이소스테아레이트, 1.5-3.0중량부의 글리세릴 카프릴레이트/카프레이트 및 향료, 방부제를 흔합 용해시켜 유상 성분을 준비하고 70.0-80.0중량부의 정제수에 5.0-10.0중량부의 글리콜, 0.2-0.5중량부의 염 및 색소를 혼합 용해시켜서 수상성분을 준비한 후 수상성분에 유상 성분을 서서히 첨가 혼합 용해시켜서 화장수를 제조하는 것이다. 위에서 말하는 중량부의 일정 범위를 미달하거나 초과할 때는 마이크로 에멀젼 영역에서 벗어나거나, 안전성 또는 경시안정성에 문제가 생긴다.The present invention provides 1.5-3.0 parts by weight of Fiji-8 caprylate / caprate, 2.0-3.0 parts by weight of polyglycerol isostearate, 1.5-3.0 parts by weight of glyceryl After dissolving caprylate / caprate, fragrance, and preservatives in an oily manner, an oily ingredient is prepared. 5.0-10.0 parts by weight of glycol, 0.2-0.5 parts by weight of salt and a pigment are dissolved in 70.0-80.0 parts by weight of purified water to prepare an aqueous phase component. The aqueous phase component is gradually added, mixed and dissolved in the aqueous phase component to prepare a lotion. When it exceeds or exceeds a certain range of said weight part, it will be out of a micro emulsion area | region, or a problem will arise in safety or aging stability.
본 발명에서 사용한 폴리글리세롤 이소스테아레이트는 다음의 구조식을 갖는다.The polyglycerol isostearate used in the present invention has the following structural formula.
n : 0 또는 1n: 0 or 1
m : 1에서 10까지m: 1 to 10
본 발명을 삼상분계로 설명하면, 제1도에서와 같이 통상의 계면활성제로는 계면활성제가 많은 영역에서 마이크로에멀젼이 형성되나 제2도와 같이 폴리글리세롤 이소스테아레이트, 피이지-8 카프릴레이트/카프레이트, 글리세릴 카프릴레이트/카프레이트를 사용하면 적은양의 계면활성제로도 마이크로 에멀젼영역이 형성되어 화장수로써 적합한 마이크로에멀젼을 얻을 수 있었다.Referring to the three-phase system, as shown in FIG. 1, as a conventional surfactant, a microemulsion is formed in a region having many surfactants, but as shown in FIG. 2, polyglycerol isostearate, Fiji-8 caprylate / When caprate and glyceryl caprylate / caprate were used, a microemulsion area was formed even with a small amount of surfactant to obtain a microemulsion suitable as a lotion.
이하 본 발명을 실시예와 비교예를 통하여 상세히 설명한다.Hereinafter, the present invention will be described in detail through Examples and Comparative Examples.
[표 1]TABLE 1
[표 2]TABLE 2
상기 실시예와 비교예의 효과를 측정하기 위하여 다음과 같은 시험을 행하였다.In order to measure the effect of the said Example and a comparative example, the following test was done.
1. 안정성시험(피부 1차 자극성시험)1. Stability test (skin primary irritation test)
적용 : 이 실험은 팻치 테스트를 이용해 10명의 20대 여성을 대상으로, 살균시킨 순수 올리브유로 50% 즉시 희석시킨 시료를 개인당 0.5㎖적용했다.Application: In this experiment, a patch test was conducted on 10 women in their 20s and 0.5 ml of each sample was immediately diluted 50% with sterile pure olive oil.
[표 3]TABLE 3
실험은 10명의 여사원을 대상으로 상기 각 시료의 일정량을 핀 챔버(Finn Chamber)에 묻혀 48시간 동안 팔안쪽에 폐색 첩포 시험을 실시한 후 핀챔버를 떼어내고 4시간 후, 24시간 후, 48시간후 판독했다.The experiment was carried out in 10 female employees, the specific amount of each sample was buried in a fin chamber and subjected to a closed patch test on the inner side of the arm for 48 hours, and then the pin chamber was removed 4 hours later, 24 hours later, and 48 hours later. Read.
0 : 무자극0: no irritation
1 : 자극이 거의 없음1: almost no stimulus
2 : 약간의 자극2: slight stimulation
3 : 보통의 자극3: normal stimulation
4 : 심한 자극4: severe stimulation
2. 안정성 시험2. Stability Test
화장수 조성물의 안정성을 평가하기 위하여 실시예 및 비교예에서 제조된 샘플을 45℃, 5℃항온조와 실온에 보관하면서 1주후, 2주후, 1개월후, 3개월후, 1년후가 되었을 때까지 관찰하여 육안으로 안정성을 평가하였다.In order to evaluate the stability of the lotion composition, the samples prepared in Examples and Comparative Examples were observed at 1, 2, 1, 3, 1 year after storage at 45 ° C, 5 ° C incubator and room temperature. The stability was evaluated visually.
[표 4]TABLE 4
이상에서와 같은 실시예와 비교예에서 알 수 있듯이 본 발명자들은 마이크로에멀젼 형성에 적절하고 적정의 계면활성제, 유용성 유연제를 사용함으로써 종래 마이크로에멀젼보다 소량의 계면활성제를 사용하여 제품의 안정성을 증가시키며 특히 피부자극성을 감고시키는 본 발명을 완성할 수 있었다.As can be seen from the examples and comparative examples as described above, the present inventors increase the stability of the product by using a smaller amount of surfactant than the conventional microemulsion, by using a suitable surfactant and oil-soluble softener suitable for forming the microemulsion. The present invention can reduce the skin irritation.
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KR1019910020841A KR950006065B1 (en) | 1991-11-21 | 1991-11-21 | Beauty wash composition for using microemulsion |
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KR1019910020841A KR950006065B1 (en) | 1991-11-21 | 1991-11-21 | Beauty wash composition for using microemulsion |
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KR950006065B1 true KR950006065B1 (en) | 1995-06-08 |
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KR100452757B1 (en) * | 2002-05-02 | 2004-10-12 | 앨트웰코스메틱 주식회사 | Manufacturing Process of Skin-Care Containing Natural Ceramide, Phytosphingoshine, Colesterol and Lecithin |
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