KR930702578A - Hybrid Emulsification Method of Polyethylene Oxide Homopolymers and Amino Functional Silicone Fluids - Google Patents

Hybrid Emulsification Method of Polyethylene Oxide Homopolymers and Amino Functional Silicone Fluids

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Publication number
KR930702578A
KR930702578A KR1019930700679A KR930700679A KR930702578A KR 930702578 A KR930702578 A KR 930702578A KR 1019930700679 A KR1019930700679 A KR 1019930700679A KR 930700679 A KR930700679 A KR 930700679A KR 930702578 A KR930702578 A KR 930702578A
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South Korea
Prior art keywords
polyethylene oxide
ethoxylated
amino functional
polyethylene
functional silicone
Prior art date
Application number
KR1019930700679A
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Korean (ko)
Inventor
마틴 블랜치 로버트
제임스 카주브스키 마크
보르싱거 그레고리
비. 창 어빙
크루첼 래리
Original Assignee
로날드 에이. 블리커
알라이드-시그날 인코포레이티드
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Publication date
Priority claimed from US07/698,230 external-priority patent/US5238731A/en
Application filed by 로날드 에이. 블리커, 알라이드-시그날 인코포레이티드 filed Critical 로날드 에이. 블리커
Publication of KR930702578A publication Critical patent/KR930702578A/en

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Abstract

산화 폴리에틸렌과 아미노 기능성 실리콘 유체의 혼성에멀션, 및 에톡시화 지방족 아민들, 에톡시화 노닐페놀들, 에톡시화 일차 알코올들, 에톡시화 이차 알코올들 및 기타 비이온성 유화제들로 구성된 군으로부터 선택된 최소한 하나의 성분을 함유하는 물품들, 및 그 제조방법. 본 혼성에멀션들은 지방산들, 수산화암모늄, 염들 및 물을 포함한 부가적인 성분들로 포함할 수 있다.Hybrid emulsion of polyethylene oxide and amino functional silicone fluid, and at least one component selected from the group consisting of ethoxylated aliphatic amines, ethoxylated nonylphenols, ethoxylated primary alcohols, ethoxylated secondary alcohols and other nonionic emulsifiers Articles containing the same, and methods for producing the same. The hybrid emulsions may comprise additional components including fatty acids, ammonium hydroxide, salts and water.

혼성에멀션 제조방법 역시 개시된다.A method of preparing a hybrid emulsion is also disclosed.

Description

산화 폴리에틸렌 단중합체들과 아미노 기능성 실리콘 유체들의 혼성 유화방법Hybrid Emulsification Method of Polyethylene Oxide Homopolymers and Amino Functional Silicone Fluids

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음Since this is an open matter, no full text was included.

제4-6도는 본 발명의 혼성에멀션들(coemulsions)의 광학 현미경 사진들이다.4-6 are optical micrographs of the coemulsions of the present invention.

Claims (11)

고밀도 폴리에틸렌 단중합체들과 저밀도 폴리에틸렌 단중합체들을 포함한 폴리에틸렌 단중합체들, 폴리에틸렌/아크릴레이트 공중합체들, 아크릴레이트를 함유하는 폴리에티렌 삼원공중합체들, 및 에스테르를 함유하는 폴리에틸렌 삼원공증합체들로 구성된 군으로 부터 선택된 최소한 하나의 산화 폴리에틸렌, 및 최소한 하나의 아미노 기능성 실리콘을 함유하는 혼성에멀션을 포함하는 수성 조성물.Consisting of polyethylene homopolymers, including high density polyethylene homopolymers and low density polyethylene homopolymers, polyethylene / acrylate copolymers, polystyrene styrene terpolymers containing acrylates, and polyethylene terpolymers containing esters An aqueous composition comprising a hybrid emulsion containing at least one polyethylene oxide selected from the group and at least one amino functional silicone. 제1항에 있어서, 아미노 기능성 실록산이 폴리디오가노실록산인 물품.The article of claim 1, wherein the amino functional siloxane is polydiorganosiloxane. 제2항에 있어서, 폴리디오가노실록산이 1000-3000 범위의 아민 중성 당량을 갖는 것인 물품.The article of claim 2, wherein the polydiorganosiloxane has an amine neutral equivalent in the range of 1000-3000. 제1항에 있어서, 에톡시화 지방족 아민들, 에톡시화 옥틸페놀들, 에톡시화 노틸페놀들, 에톡시화 일차 알코올들, 에톡시화 이차 알코올들, 비이온성 유화제들, 지방산들, 수산화암모늄 및 나트륨염들로 구성된 군으로 부터 선택된 최소한 하나의 성분들 더 포함하는 수성 조성물.The ethoxylated aliphatic amines, ethoxylated octylphenols, ethoxylated nathylphenols, ethoxylated primary alcohols, ethoxylated secondary alcohols, nonionic emulsifiers, fatty acids, ammonium hydroxide and sodium salts An aqueous composition further comprising at least one component selected from the group consisting of: 제4항에 있어서, 에톡시화 지방족 아민이 포화 또는 불포화 지방족 아민들과 산화에틸렌과의 반응 산물들인 것인 조성물.The composition of claim 4 wherein the ethoxylated aliphatic amine is the reaction product of saturated or unsaturated aliphatic amines with ethylene oxide. 반응용기에 산화 폴리에틸렌과 아미노 기능성 실리콘을 제공하고, 산화 폴리에틸렌과 아미노 기능성 실리콘의 온도를 최소한 산화 폴리에틸렌 성분의 융점까지 상승시키는 단계들을 포함하는, 전술한 청구범위들중 어느 한 항에 의한 혼성에멀션을 함유하는 수성 조성물의 제조방법.Providing a hybrid emulsion according to any one of the preceding claims, comprising providing a reaction vessel with polyethylene oxide and amino functional silicone and raising the temperature of the polyethylene oxide and amino functional silicone to at least the melting point of the polyethylene oxide component. The manufacturing method of the aqueous composition containing. 제6항에 있어서, 성분들의 온도를 산화 폴리에틸렌 성분의 융점 이상의 최대 온도까지 상승시키고, 그 최대 온도에서 제1 체류시간 동안 성분들을 유지시키는 단계들을 더 포함하는 제조방법.The method of claim 6, further comprising raising the temperature of the components to a maximum temperature above the melting point of the polyethylene oxide component and maintaining the components for a first residence time at the maximum temperature. 제6항에 있어서, 산화 폴리에틸렌과 아미노 기능성 실리콘의 온도를, 교반하면서 제1가열속도로 제1 시간 간격동안, 산화 폴리에틸렌의 융점 이상으로 상승시키고, 제1 가열속도보다 작은 제2 가열속도로 제2 시간 간격동안, 성분들의 온도가 산화 폴리에틸렌 성분의 융점 보다 7-10℃ 더 높은 최대 온도 또는 최대온도 범위까지 상승하도록 가열하고, 그 최대온도 또는 최대 온도 범위에서 10-15분 동안 반응물들을 유지시키는 단계들을 포함하는 제조방법.The method of claim 6, wherein the temperature of the polyethylene oxide and the amino functional silicone is raised to a melting point of the polyethylene oxide at a first heating rate at a first heating rate while stirring, at a second heating rate smaller than the first heating rate. During the two hour interval, the temperature of the components is heated to a maximum or maximum temperature range of 7-10 ° C. above the melting point of the polyethylene oxide component, and the reactants are held at that maximum temperature or maximum temperature range for 10-15 minutes. A manufacturing method comprising the steps. 제6항에 있어서, 혼성에멀션의 pH가 4-6의 범위내에서 유지되도록 pH를 조절하는 단계를 더 포함하는 제조방법.The method of claim 6, further comprising adjusting the pH such that the pH of the hybrid emulsion is maintained in the range of 4-6. 직물, 섬유, 로우프, 토우, 웹, 실, 섬유충진물질, 종이, 릴리이즈 시이트, 릴리이즈 스트립, 및 루우핑 페이퍼와 루우핑 슁글 같은 아스팔트-함유 물품들로 구성된 군으로부터 선택된 물품으로서, 전술한 청구범위 1-5항중 어느 한 항에 의한 조성물로 최소한 부분 코팅된 물품.An article selected from the group consisting of fabrics, fibers, ropes, tows, webs, yarns, fibrous fillers, paper, release sheets, release strips, and asphalt-containing articles such as roofing papers and roofing shingles, wherein the claims An article at least partially coated with the composition according to any one of claims 1-5. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019930700679A 1990-09-07 1991-09-05 Hybrid Emulsification Method of Polyethylene Oxide Homopolymers and Amino Functional Silicone Fluids KR930702578A (en)

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