KR920009780A - 시클로헥산디온 유도체 및 그 제조방법 - Google Patents

시클로헥산디온 유도체 및 그 제조방법 Download PDF

Info

Publication number
KR920009780A
KR920009780A KR1019910021397A KR910021397A KR920009780A KR 920009780 A KR920009780 A KR 920009780A KR 1019910021397 A KR1019910021397 A KR 1019910021397A KR 910021397 A KR910021397 A KR 910021397A KR 920009780 A KR920009780 A KR 920009780A
Authority
KR
South Korea
Prior art keywords
cyclohex
trimethylphenyl
butyryl
ethoxyimino
propyl
Prior art date
Application number
KR1019910021397A
Other languages
English (en)
Other versions
KR100232517B1 (ko
Inventor
제이 찰머스 피터
에프 키어바이 앤드류
피 헤스 로저
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Publication of KR920009780A publication Critical patent/KR920009780A/ko
Application granted granted Critical
Publication of KR100232517B1 publication Critical patent/KR100232517B1/ko

Links

Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N35/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
    • A01N35/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical at least one of the bonds to hetero atoms is to nitrogen
    • A01N35/10Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical at least one of the bonds to hetero atoms is to nitrogen containing a carbon-to-nitrogen double bond
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/02Compounds containing nitrogen atoms doubly-bound to a carbon skeleton containing imino groups
    • C07C251/04Compounds containing nitrogen atoms doubly-bound to a carbon skeleton containing imino groups having carbon atoms of imino groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C251/10Compounds containing nitrogen atoms doubly-bound to a carbon skeleton containing imino groups having carbon atoms of imino groups bound to hydrogen atoms or to acyclic carbon atoms to carbon atoms of an unsaturated carbon skeleton
    • C07C251/14Compounds containing nitrogen atoms doubly-bound to a carbon skeleton containing imino groups having carbon atoms of imino groups bound to hydrogen atoms or to acyclic carbon atoms to carbon atoms of an unsaturated carbon skeleton containing rings other than six-membered aromatic rings
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/14Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/32Oximes
    • C07C251/34Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C251/42Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups bound to a carbon atom of a ring other than a six-membered aromatic ring

Landscapes

  • Organic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Plant Pathology (AREA)
  • Agronomy & Crop Science (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

내용 없음.

Description

시클로헥산디온 유도체 및 그 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (7)

  1. 화학명이 2-[1-(에톡시이미노)프로필]-3-히드록시-5-(3-부티릴-2, 4, 6-트리메틸페닐)-시클로헥스-2-엔-1-온 인 무수 결정성 분말 형태의 시클로헥산디온 유도체.
  2. 2-[1-(에톡시이미노)프로필]-3-히드록시-5-(3-부티릴-2, 4, 6-트리메틸페닐)-시클로헥스-2-엔-1-온 화합물을 끓는 점이 낮은 탄화수소 용매에 가하여 용액을 제조하고; 이 용액을 최소한 0℃로 냉각시킨 후, 생성되는 결정을 모으는 단계를 포함하는 제1항의 무수 결정성 분말 형태의 시클로헥산디온 유도체의 제조방법.
  3. 제2항에 있어서, 화합물 2-[1-(에톡시이미노)프로필]-3-히드록시-5-(3-부티릴-2, 4, 6-트리메틸페닐)-2-프로피오닐-시클로헥스-2-엔-1-온을 n-부티릴-2, 4, 6-트리메틸페닐)-2-프로피오닐-시클로헥스-2-엔-1-온과 반응시키고 그 생성물을 에톡시아민과 반응시킴을 특징으로 하는 시클로헥산디온 유도체의 제조방법.
  4. 제2항에 있어서, 탄화수소 용매는 끓는 점이 100℃ 이하인 용매임을 특징으로 하는 시클로헥산디온 유도체의 제조방법.
  5. 제2항에 있어서, 탄화수소 용매는 시클로헥산, 알칸 및 석유 스피릿 가운데 선택한 것임을 특징으로 하는 시클로헥산디온 유도체의 제조방법.
  6. 제2항에 있어서, 화합물 2-[1-(에톡시이미노)프로필]-3-히드록시-5-(3-부티릴-2, 4, 6-트리메틸페닐)-시클로헥스-2-엔-1-온은 용액을 최소한 -10℃로 냉각시킴을 특징으로 하는 시클로헥산디온 유도체의 제조방법.
  7. 실시예와 관련하여 상세히 기술한 바와 같은 화학명이 2-[1-(에톡시이미노)프로필]-3-히드록시-5-(3-부티릴-2, 4, 6-트리메틸페닐)-시클로헥스-2-엔-1-온 인 시클로헥산디온 유도체의 제조방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019910021397A 1990-11-27 1991-11-27 무수 결정 분말 형태의 페녹시딤 및 그 제조방법 KR100232517B1 (ko)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AUPK356990 1990-11-27
AUPK3569 1990-11-27

Publications (2)

Publication Number Publication Date
KR920009780A true KR920009780A (ko) 1992-06-25
KR100232517B1 KR100232517B1 (ko) 1999-12-01

Family

ID=3775108

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019910021397A KR100232517B1 (ko) 1990-11-27 1991-11-27 무수 결정 분말 형태의 페녹시딤 및 그 제조방법

Country Status (9)

Country Link
US (2) US5276188A (ko)
EP (1) EP0488645B1 (ko)
JP (1) JP3095191B2 (ko)
KR (1) KR100232517B1 (ko)
BR (1) BR9105133A (ko)
DE (1) DE69112999T2 (ko)
HU (1) HU209803B (ko)
IL (1) IL100203A (ko)
NZ (1) NZ240662A (ko)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19510887A1 (de) * 1995-03-24 1996-09-26 Basf Ag Stabile Festformulierungen von Cyclohexenonoximether-Herbiziden
AUPO132296A0 (en) * 1996-07-30 1996-08-22 Ici Australia Operations Proprietary Limited Chemical process

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
USRE32489E (en) * 1980-11-25 1987-09-01 Chevron Research Company Herbicidal substituted 2-(1-(oxyamino)-alkylidene)-cyclohexane-1,3-diones
AU556148B2 (en) * 1982-01-29 1986-10-23 Ici Australia Limited Cyclohexane -1,3- dione derivatives
PH20618A (en) * 1982-01-29 1987-03-06 Ici Australia Ltd Herbicidal 5-(substituted phenyl)-cyclohexan-1,3-dione derivatives
AU566671B2 (en) * 1983-07-18 1987-10-29 Ici Australia Limited Cyclohexene-1,3-dione derivatives
DD235450B1 (de) * 1983-12-29 1988-02-03 Humboldt Uni Z Berlin Verfahren zur herstellung neuer 1-(2-hydroxyaryl)-alkan-1-on-oxime
US4666516A (en) * 1986-01-21 1987-05-19 Elkem Metals Company Gray cast iron inoculant

Also Published As

Publication number Publication date
JPH04290857A (ja) 1992-10-15
EP0488645B1 (en) 1995-09-13
IL100203A (en) 1997-11-20
BR9105133A (pt) 1992-07-21
DE69112999T2 (de) 1996-08-01
EP0488645A1 (en) 1992-06-03
NZ240662A (en) 1993-04-28
US5276188A (en) 1994-01-04
US5354889A (en) 1994-10-11
JP3095191B2 (ja) 2000-10-03
DE69112999D1 (de) 1995-10-19
HUT60240A (en) 1992-08-28
KR100232517B1 (ko) 1999-12-01
HU913652D0 (en) 1992-02-28
HU209803B (en) 1994-11-28

Similar Documents

Publication Publication Date Title
Craig et al. The rate of reaction of maleic anhydride with 1, 3-Dienes as related to diene conformation
DK327583A (da) Fremgangsmaade til fremstilling af fritstroemmende ethylcellulosemikrokapsler
KR960703842A (ko) 요오파미돌의 결정화 방법(process for the crystallization of iopamidol)
KR840005123A (ko) 4-하이드록시쿠마린형의 항응고제의 제조방법
KR850001221A (ko) 세팔로스포린의 제조방법
KR920009780A (ko) 시클로헥산디온 유도체 및 그 제조방법
Milas et al. Studies in Organic Peroxides. VI. Cyclane Peroxides
Breuer et al. Fluorescence decay times and non-radiative decay rates of the first excited singlet states of methylated and fluorinated benzenes
NO120183B (ko)
KR870003183A (ko) 수소에너지 방출촉매
KR850001226A (ko) 안트라사이클린 유도체의 제조방법
KR890008156A (ko) 깅콜리드의 신규 알콜시 유도체, 그 제조 방법 및 이를 함유한 치료 조성물
Sumpter et al. The structure of Baeyer's nitro-oxindole
US2557956A (en) Process of extracting sesamin from sesame oil
Krügerke et al. Structural Dynamics of the First Alkylidenesulfur Difluoride Oxide, OFC–CH SF2 O
US4017502A (en) Process for purifying the mixed ester, ethylene glycol 1-(2-p-chlorophenoxy)-2-methylpropionate nicotinate
KR870010070A (ko) 모라노린 유도체의 제조법
Addison et al. 534. Double melting of molecular addition compounds of dinitrogen tetroxide with organic donors
US3472873A (en) Isomerization of 2,5-dihydrothiophene-1,1-dioxide
Cameron et al. The use of chiral NMR shift reagents in a study of the stereochemistry of bianthrones
KR890700539A (ko) 폐황산으로부터의 크롬 및 바나듐의 침전방법
Hargreaves et al. The resolution of 1-bromo-1-chloro-1-fluoroacetone and the preparation of (+)-and (–)-bromochlorofluoromethane
RU94035677A (ru) Способ получения хлорангидридов кислот
KR950014074A (ko) 이소프로필안티피린의 제조방법
Blagden et al. 77. Phosphoric acid compounds of menthols and other alcohols

Legal Events

Date Code Title Description
AMND Amendment
A201 Request for examination
AMND Amendment
E902 Notification of reason for refusal
AMND Amendment
E601 Decision to refuse application
J201 Request for trial against refusal decision
B701 Decision to grant
GRNT Written decision to grant
LAPS Lapse due to unpaid annual fee