KR910014499A - Detergent composition and preparation method thereof - Google Patents

Detergent composition and preparation method thereof Download PDF

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Publication number
KR910014499A
KR910014499A KR1019910000856A KR910000856A KR910014499A KR 910014499 A KR910014499 A KR 910014499A KR 1019910000856 A KR1019910000856 A KR 1019910000856A KR 910000856 A KR910000856 A KR 910000856A KR 910014499 A KR910014499 A KR 910014499A
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South Korea
Prior art keywords
high speed
granulator
speed mixer
process according
iii
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KR1019910000856A
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Korean (ko)
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KR960000207B1 (en
Inventor
죠지이반 데이비드
죠지 맥레오드 고돈
피터 도날드
렘지유레거 코커트
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원본미기재
유니레버 엔브이
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Application filed by 원본미기재, 유니레버 엔브이 filed Critical 원본미기재
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
    • C11D17/065—High-density particulate detergent compositions

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

내용 없음No content

Description

세제 조성물 및 그 제조방법Detergent composition and preparation method thereof

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음As this is a public information case, the full text was not included.

Claims (15)

음이온 계면활성제의 액체 산전구물질을 고체 수용성 알칼리성 무기물질로 중화시키는 단계를 포함하는, 650g/1 이상의 벌크밀도를 가지는 과립형 세제조성물 또는 성분의 배치식 제조방법에 있어서, 다음과 같은 단계로 이루어지는 것을 특징으로 하는 제조방법.In a batch production method of a granular detergent composition or component having a bulk density of 650 g / 1 or more, comprising neutralizing a liquid acid precursor of an anionic surfactant with a solid water-soluble alkaline inorganic material, comprising the following steps: Manufacturing method characterized in that. (ⅰ) 중화에 필요한 양이상의 입자상 고체 수용성 알칼리성 무기물질을, 필요에 따라 1종 이상의 기타 입자상 고체와 함께 교반작용과 커팅작용을 동시에 갖춘 고속혼합기/과립화기내에 유동화시키는 단계, (ⅱ) 55℃ 이하의 온도로 유지시킬 필요없이 상기 고속혼합기/과립화기내에 산 전구물질을 가함으로써, 수용성 알칼라성 무기질에 의한 산 전구물질의 중화가 이루어지며 혼합물은 입자형태로 존재하는 단계, (ⅲ) 이 혼합물을 액체결합제 존재하에 고속혼합기/과립하기 내에서 과립화시킴으로써, 650g/1 이상의 벌크밀도를 가지는 과립형 세제조성물 또는 성분을 얻는 단계.(Iii) fluidizing more than the amount of particulate solid water-soluble alkaline inorganic material necessary for neutralization into a high speed mixer / granulator with at least one other particulate solid, which is simultaneously stirred and cut, (ii) 55 ° C By adding acid precursors in the high speed mixer / granulator without the need to maintain the temperature below, neutralization of the acid precursors with water-soluble alkaline minerals occurs and the mixture is present in the form of particles, Granulating the mixture in a high speed mixer / granule in the presence of a liquid binder to obtain a granular detergent composition or component having a bulk density of at least 650 g / 1. 제1항에 있어서, (ⅱ) 단계에서 산 전구물질을 고속혼합기/과립화기에 점차적으로 가하는 것을 특징으로 하는 제조방법.The process according to claim 1, wherein the acid precursor is gradually added to the high speed mixer / granulator in step (ii). 제2항에 있어서, (ⅱ) 단계에서 산 전구물질을 0.5 분 이상에 걸쳐 고속혼합기/과립화기에 가하는 것을 특징으로 하는 제조방법.The process according to claim 2, wherein the acid precursor is added to the high speed mixer / granulator in step (ii) for at least 0.5 minutes. 제2항에 있어서, (ⅱ) 단계에서 산 전구물질을 0.5-12분간에 걸쳐 고속혼합기/과립화기에 가하는 것을 특징으로 하는 제조방법.The process according to claim 2, wherein the acid precursor is added to the high speed mixer / granulator in step (ii) over 0.5-12 minutes. 제1항에 있어서, (ⅱ) 단계에서 산 전구물질을 고속혼합기/과립화기내의 온도는 100℃를 초과하지 않는 것을 특징으로 하는 제조방법.The process according to claim 1, wherein the temperature of the acid precursor in the high speed mixer / granulator in step (ii) does not exceed 100 ° C. 제1항에 있어서, 입자상 수용성 알칼리성 무기질은 탄산나트륨을 포함하는 것을 특징으로 하는 제조방법.The method of claim 1 wherein the particulate water-soluble alkaline mineral comprises sodium carbonate. 제1항에 있어서, 산 전구물질은 선형 알킬벤젠 술폰산염인 것을 특징으로 하는 제조방법.The process of claim 1 wherein the acid precursor is a linear alkylbenzene sulfonate. 제1항에 있어서, (ⅰ) 단계에서 존재하는 고체물질은 수용성 알칼리성 무기물질과 함께 결정형 또는 무정형 알칼리금속 알루미노규산염을 포함하는 것을 특징으로 하는 제조방법.The method of claim 1, wherein the solid material present in step (iii) comprises a crystalline or amorphous alkali metal aluminosilicate together with a water-soluble alkaline inorganic material. 제8항에 있어서, 물은 (ⅲ) 단계 이전에 첨가되지 않는 것을 특징으로 하는 제조방법.9. A process according to claim 8 wherein water is not added before step (iii). 제1항에 있어서, (ⅰ)단계에서 존재하는 총 고체물질의 양은 (ⅱ) 단계에서 존재하는 총조성물의 60중량％이상인 것을 특징으로 하는 제조방법.The method according to claim 1, wherein the total amount of solid material present in step (iii) is at least 60% by weight of the total composition present in step (ii). 제1항에 있어서, 고속혼합기/과립화기는 보올형태이며 근본적으로 수직 교반축을 가지는 것을 특징으로 하는 제조방법.2. A process according to claim 1 wherein the high speed mixer / granulator has a bowl shape and essentially has a vertical stirring shaft. 제1항에 있어서, 고속혼합기/과립화기는 (ⅰ),(ⅱ),(ⅲ) 단계 동안 교반기속도 60-150rpm, 커터속도 1000-3000rpm으로 작동되는 것을 특징으로 하는 제조방법.The method according to claim 1, wherein the high speed mixer / granulator is operated at a stirrer speed of 60-150 rpm and a cutter speed of 1000-3000 rpm during steps (iii), (ii) and (iii). 제1항에 있어서, 과립화단계인 (ⅲ) 단계 완료후의 과립형 세제조성물 또는 성분에 미세입자상 유동보조제를 혼합시키는 단계가 추가로 포함되는 것을 특징으로 하는 제조방법.The method according to claim 1, further comprising the step of mixing the granular detergent composition or component with the granular detergent composition after the completion of the granulation step (iii). 제13항에 있어서, 고속혼합기/과립화기는 유동보조제의 첨가동안 교반기속도 60-80rpm, 커터속도 0rpm으로 작동되는 것을 특징으로 하는 제조방법.14. A process according to claim 13, wherein the high speed mixer / granulator is operated at stirrer speed 60-80 rpm and cutter speed 0 rpm during addition of the flow aid. 제1항의 제조방법에 의해 제조된, 벌크밀도가 650g/1이상이고 1700㎛이하인 입자를 50중량％이상 함유하는 과립형 세제조성물 또는 성분.A granular detergent composition or component prepared by the process according to claim 1, containing 50% by weight or more of particles having a bulk density of 650 g / 1 or more and 1700 μm or less. ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.※ Note: The disclosure is based on the initial application.
KR1019910000856A 1990-01-19 1991-01-18 Detergent compositions and process for preparing them KR960000207B1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
GB9001285 1990-01-19
GB909001285A GB9001285D0 (en) 1990-01-19 1990-01-19 Detergent compositions and process for preparing them
GB90012857 1990-01-19

Publications (2)

Publication Number Publication Date
KR910014499A true KR910014499A (en) 1991-08-31
KR960000207B1 KR960000207B1 (en) 1996-01-03

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ID=10669596

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Application Number Title Priority Date Filing Date
KR1019910000856A KR960000207B1 (en) 1990-01-19 1991-01-18 Detergent compositions and process for preparing them

Country Status (11)

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EP (1) EP0438320A3 (en)
JP (1) JP2918710B2 (en)
KR (1) KR960000207B1 (en)
AU (1) AU640979B2 (en)
BR (1) BR9100127A (en)
CA (1) CA2034244C (en)
GB (1) GB9001285D0 (en)
IN (1) IN171897B (en)
MY (1) MY107892A (en)
TR (1) TR27438A (en)
ZA (1) ZA91385B (en)

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JP3192469B2 (en) * 1991-05-17 2001-07-30 花王株式会社 Method for producing nonionic detergent particles
ES2104884T3 (en) * 1992-02-14 1997-10-16 Procter & Gamble PROCEDURE FOR PREPARING DETERGENT GRANULES FOR SULPHONIC ACID NEUTRALIZATION.
US5486317A (en) * 1992-02-14 1996-01-23 The Procter & Gamble Company Process for making detergent granules by neutralization of sulphonic acids
AU673926B2 (en) * 1993-07-13 1996-11-28 Colgate-Palmolive Company, The Process for preparing detergent composition having high bulk density
GB9324129D0 (en) † 1993-11-24 1994-01-12 Unilever Plc Detergent compositions and process for preparing them
EP0663439B1 (en) * 1994-01-17 2000-08-16 The Procter & Gamble Company Process for preparing detergent granules
US5703037A (en) * 1994-04-20 1997-12-30 The Procter & Gamble Company Process for the manufacture of free-flowing detergent granules
ATE197811T1 (en) * 1994-04-20 2000-12-15 Procter & Gamble METHOD FOR PRODUCING FREE-FLOWING DETERGENT GRANULES
US5565137A (en) * 1994-05-20 1996-10-15 The Proctor & Gamble Co. Process for making a high density detergent composition from starting detergent ingredients
TW326472B (en) * 1994-08-12 1998-02-11 Kao Corp Method for producing nonionic detergent granules
US5573697A (en) * 1995-05-31 1996-11-12 Riddick; Eric F. Process for making high active, high density detergent granules
GB9526097D0 (en) * 1995-12-20 1996-02-21 Unilever Plc Process
CN1221448A (en) * 1996-04-17 1999-06-30 普罗格特-甘布尔公司 High density detergent-making process using high active surfactant paste having improved stability
TW462987B (en) * 1996-08-26 2001-11-11 Kao Corp Method for producing high-bulk density detergent composition
DE19700776A1 (en) * 1997-01-13 1998-07-16 Henkel Kgaa Granular detergent with improved fat washing capacity
DE69817811T2 (en) 1997-05-30 2004-04-01 Unilever N.V. GIANT GRANULAR DETERGENT COMPOSITIONS
GB9711359D0 (en) * 1997-05-30 1997-07-30 Unilever Plc Detergent powder composition
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US6576605B1 (en) 1998-10-28 2003-06-10 The Procter & Gamble Company Process for making a free flowing detergent composition
JP2002528599A (en) * 1998-10-28 2002-09-03 ザ、プロクター、エンド、ギャンブル、カンパニー Method for producing free-flowing detergent composition
DE10163603B4 (en) 2001-12-21 2006-05-04 Henkel Kgaa Process for the preparation of builder-containing surfactant granules
DE10232304B4 (en) * 2002-07-17 2005-10-27 Henkel Kgaa Neutralization in the mixer
EP1534812B1 (en) 2002-09-06 2007-08-15 Kao Corporation Detergent particles
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WO2011061045A1 (en) * 2009-11-20 2011-05-26 Unilever Nv Detergent granule and its manufacture

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GB8818613D0 (en) * 1988-08-05 1988-09-07 Paterson Zochonis Uk Ltd Detergents

Also Published As

Publication number Publication date
IN171897B (en) 1993-01-30
CA2034244C (en) 1999-11-30
EP0438320A2 (en) 1991-07-24
CA2034244A1 (en) 1991-07-20
JP2918710B2 (en) 1999-07-12
KR960000207B1 (en) 1996-01-03
AU6938991A (en) 1991-07-25
MY107892A (en) 1996-06-29
AU640979B2 (en) 1993-09-09
GB9001285D0 (en) 1990-03-21
ZA91385B (en) 1992-09-30
EP0438320A3 (en) 1992-02-19
TR27438A (en) 1995-05-24
JPH04363398A (en) 1992-12-16
BR9100127A (en) 1991-10-22

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