KR890701720A - Disinfecting cleaning or disinfecting agent and its preparation - Google Patents

Disinfecting cleaning or disinfecting agent and its preparation

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KR890701720A
KR890701720A KR1019890700490A KR890700490A KR890701720A KR 890701720 A KR890701720 A KR 890701720A KR 1019890700490 A KR1019890700490 A KR 1019890700490A KR 890700490 A KR890700490 A KR 890700490A KR 890701720 A KR890701720 A KR 890701720A
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group
carbon atoms
bactericidal
alkyl group
alkyl
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KR1019890700490A
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KR910005713B1 (en
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로버트 에이취 맥킨토쉬
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원본미기재
인터페이스 리서취 코포레이션
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02—Amines; Quaternary ammonium compounds
    • A01N33/08—Amines; Quaternary ammonium compounds containing oxygen or sulfur
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
    • A01N57/12—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing acyclic or cycloaliphatic radicals
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
    • A01N57/14—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing aromatic radicals
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/36—Organic compounds containing phosphorus
    • C11D3/362—Phosphates or phosphites

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Detergent Compositions (AREA)

Abstract

내용 없음No content

Description

살균성 세척 또는 소독제제 및 그의 제법Disinfecting cleaning or disinfecting agent and its preparation

본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음Since this is a trivial issue, I did not include the contents of the text.

Claims (29)

살균효과가 있을 정도의 양의 포스페이트 에스테르를 갖는 세정제를 포함하며, 다음의 구조식을 갖는 살균성 있는 세척조성물：CLAIMS What is claimed is: 1. A bactericidal cleaning composition comprising a detergent having an amount of phosphate ester sufficient to have a bactericidal effect, 여기서 R과 R＇는 알킬, 아릴, 아랄킬, 알카릴기이며, R 또는 R＇의 하나는 수소가 될 수 있으며, 적어도 하나의 자유 하이드록시기를 갖는 것을 나타낸다.Wherein R and R 'are alkyl, aryl, aralkyl, alkaryl groups, and one of R or R' may be hydrogen and has at least one free hydroxy group. 제1항에 있어서, 포스페이트 에스테르가 다음의 구조식을 가지는, 부분적으로 중화된 산인 것을 특징으로 하는 살균성 세척조성물：The bactericidal cleaning composition according to claim 1, wherein the phosphate ester is a partially neutralized acid having the following structure: 여기서, R과 R＇는 알킬, 아릴, 아랄킬, 알카릴기에서부터 선택되며, R이나 R＇는 수소가 될 수 있으며；X는 유기이온, 1A족 금속, 2A족 금속, 전이금속 중에서 선택된 것을 나타낸다.Wherein R and R 'are selected from alkyl, aryl, aralkyl, alkaryl groups, R or R' can be hydrogen, and X is selected from organic ions, Group 1A metals, Group 2A metals and transition metals . 제2항에 있어서, R이나 R＇가 1개 내지 18개의 탄소원자를 가지는 알킬기인 것을 특징으로 하는 살균성 세척조성물.A bactericidal cleaning composition according to claim 2, wherein R or R 'is an alkyl group having from 1 to 18 carbon atoms. 제2항에 있어서, X가 다음의 구조식을 갖는 것을 특징으로 하는 살균성 세척조성물：A bactericidal cleaning composition according to claim 2, wherein X has the following structure: 여기서, R1은 4개 내지 18개의 탄소원자를 갖는 알킬기와 1개 내지 18개의 탄소원자를 갖는 하이드록시 알킬기로 구성된 그룹에서 선택되며；R2는 8개 내지 18개의 탄소원자를 갖는 알킬기를 나타낸다.Wherein R 1 is selected from the group consisting of an alkyl group having 4 to 18 carbon atoms and a hydroxyalkyl group having 1 to 18 carbon atoms and R 2 represents an alkyl group having 8 to 18 carbon atoms. 제4항에 있어서, 상기의 살균성 포스페이트 에스테르가 다음의 구조식을 갖는 것을 특징으로 하는 살균성 세척조성물：5. A bactericidal cleaning composition according to claim 4, wherein said bactericidal phosphate ester has the following structure: 여기서, R은 H나 C2H5를 나타낸다.Here, R represents H or C 2 H 5 . 제2항에 있어서, X가 4급아민이고 R은 수소인 것을 특징으로 하는 살균성 세척조성물.3. The bactericidal cleaning composition of claim 2, wherein X is a quaternary amine and R is hydrogen. 제6항에 있어서, 살균성 포스페이트 유도체의 X가 다음의 구조식을 갖는 4급아민인 것을 특징으로 하는 살균성 세척조성물：The bactericidal cleaning composition according to claim 6, wherein X of the bactericidal phosphate derivative is a quaternary amine having the following structure: 여기서, R1은 4개 내지 18개의 탄소원자를 가지는 알킬기와, 1개 내지 18개의 탄소원자를 가지는 하이드록시 알킬기로 구성된 그룹에서 선택되며；R2는 8개 내지 18개의 탄소원자를 가지는 것을 나타낸다.Wherein R 1 is selected from the group consisting of an alkyl group having from 4 to 18 carbon atoms and a hydroxyalkyl group having from 1 to 18 carbon atoms and R 2 has 8 to 18 carbon atoms. 제7항에 있어서, 상기 살균성 포스페이트 유도체가 다음의 구조식을 갖는 것을 특징으로 하는 살균성 세척조성물.8. The bactericidal cleaning composition of claim 7, wherein the bactericidal phosphate derivative has the following structural formula. 다음의 과정과 같이；(가)인산을 약 1몰 내지 2몰의 비스(하이드록시 에틸) 코코아민으로 중화시키고, (나)이 혼합물을 약 0.01% 내지 70%(중량비)의 농도에서 세정제와 혼합하여, 살균성 세척조성물을 제조하는 방법.(B) neutralizing the phosphoric acid with about 1 to 2 moles of bis (hydroxyethyl) cocoamine, (b) treating the mixture with a detergent at a concentration of about 0.01% to 70% ≪ / RTI > to prepare a bactericidal cleaning composition. 다음의 과정과 같이；(가)적어도 하나의 자유 하이드록시기를 갖는 포스페이트 유도체를 얻기 위해, 약 60-120℃에서 약 1몰 내지 3몰의 하이드록시 알킬, 아릴, 아라릴 또는 알카릴 화합물과 포스포러스 펜톡사이드와 반응시키고, (나)이 혼합물을 약 0.01% 내지 70%(중량비)의 농도에서 세정제와 혼합하여, 살균성 세척조성물을 제조하는 방법.(A) about 1 to 3 moles of a hydroxyalkyl, aryl, aralyl or alkaryl compound at about 60-120 占 폚 and a phosphorous compound at a temperature of about 60-120 占 폚 to obtain a phosphate derivative having at least one free hydroxy group, (B) mixing the mixture with a detergent at a concentration of about 0.01% to 70% (weight ratio) to produce a bactericidal cleaning composition. 제10항에 있어서, 상기 하이드록시 알킬기가 1개 내지 18개의 탄소원자를 갖는 것.11. The composition of claim 10, wherein the hydroxyalkyl group has from 1 to 18 carbon atoms. 제10항에 있어서, (가)단계의 생성물을 약 0.5 내지 1.5몰의 3급아민과 반응시키며, 이 3급아민은 8개 내지 18개의 탄소원자를 갖는 알킬기로 구성되는 하나의 치환체를 가지며, 다른 종류의 두알킬기(즉, 4개 내지 18개의 탄소원자를 갖는 알킬기와 1개 내지 18개의 탄소원자를 갖는 하이드록시 알킬기로 구성된 그룹에서 선택된 것)를 두 치환체로 하는 것을 특징으로 하는 살균성 세척조성물의 제법.11. The process of claim 10, wherein the product of step (a) is reacted with from about 0.5 to 1.5 moles of a tertiary amine, said tertiary amine having one substituent consisting of an alkyl group having from 8 to 18 carbon atoms, Wherein two substituents are selected from the group consisting of two alkyl groups (i.e., an alkyl group having 4 to 18 carbon atoms and a hydroxyalkyl group having 1 to 18 carbon atoms). 제12항에 있어서, 3급아민은 비스(하이드록시 에틸)코코아민인 것을 특징으로 하는 살균성 세척조성물의 제법.13. The method of claim 12, wherein the tertiary amine is bis (hydroxyethyl) cocoamine. 다음의 과정과 같이；(가)적어도 하나의 자유하이드록시기를 갖는 포스페이트 유도체를 얻기 위해, 약 60-120℃에서 포스포러스 펜톡사이드의 몰당 약 1몰 내지 3몰의 하이드록시 알킬, 아릴, 아라릴 또는 알카릴 화합물을 포스포러스 펜톡사이드와 반응시키고, (4)이 생성물을 약 0.5 내지 1.5몰의 3급아민과 반응시키는데, 이 3급아민은 8개 내지 18개의 탄소원자를 갖는 알킬기로 구성되는 하나의 치환체를 갖고 다른 종류의 두 알킬기(즉, 1개 내지 18개의 탄소원자를 갖는 알킬기와, 1개 내지 18개의 탄소원자를 갖는 하이드록시 알킬기로 구성되는 그룹에서 선택된 것)를 두 치환체로 가지며, (다)상기 (가)단계에서 얻은 혼합물을 약 0.01%-70%(중량비)의 농도에서 세정제와 혼합하여 얻는 살균성 세척조성물의 제법.(A) from about 1 to 3 moles of hydroxyalkyl, aryl, aralyl (as defined above) per mole of phosphorus pentoxide at about 60-120 DEG C to obtain a phosphate derivative having at least one free hydroxy group, Or an alkaryl compound with phosphorus pentoxide; (4) reacting the product with about 0.5 to 1.5 moles of a tertiary amine, wherein the tertiary amine is an alkyl group having from 8 to 18 carbon atoms Having two substituents of the same kind and having two substituents of the other kind (i.e., selected from the group consisting of an alkyl group having 1 to 18 carbon atoms and a hydroxyalkyl group having 1 to 18 carbon atoms) ) A process for producing a bactericidal cleaning composition obtained by mixing the mixture obtained in the step (a) with a detergent at a concentration of about 0.01% -70% (weight ratio). 다음의 구조식을 갖고, 살균력을 발휘할 수 있는 분량의 포스페이트 에스테르를 포함하는 소독제의 조제(調製)방법.A method for preparing (disinfecting) a disinfectant having the following structural formula and comprising a phosphate ester in an amount capable of exhibiting sterilizing power. 여기서, R과 R＇는 알킬, 아릴, 아랄킬, 알칼릴기로 구성된 그룹에서 선택되며, R이나 R＇의 하나는 수소가 될 수 있으며, 적어도 하나의 자유하이드록시기를 가지는 것을 나타낸다.Wherein R and R 'are selected from the group consisting of alkyl, aryl, aralkyl, alkaryl groups, and one of R or R' can be hydrogen and has at least one free hydroxy group. 제15항에 있어서, 상기 액체가 물인 것을 특징으로 하는 소독제의 조제방법.16. The method for preparing a disinfectant according to claim 15, wherein the liquid is water. 제15항에 있어서, 포스페이트 에스테르는 다음의 구조식을 갖는, 부분적으로 중화된 특징으로 하는 소독제의 조제방법：16. The method of claim 15, wherein the phosphate ester has a partially neutralized character with the following structure: 여기서, R가 R＇는 알킬, 아릴, 아랄킬, 알카릴기로 구성된 그룹에서 선택되며, R이나 R＇가 수소가 될 수 있는 것이며；X는 유기이온, 1A족 금속, 2A족 금속, 전이금속으로 구성된 그룹에서 선택된 양이온을 나타낸다.Wherein R is selected from the group consisting of alkyl, aryl, aralkyl, alkaryl groups, R or R 'can be hydrogen, X is an organic ion, Group 1A metal, Group 2A metal, ≪ / RTI > 제17항에 있어서, R이나 R＇가 1개 내지 18개의 탄소원자를 가지는 알킬기인 것을 특징으로 하는 소독제의 조제방법.The method of preparing a disinfectant according to claim 17, wherein R or R 'is an alkyl group having 1 to 18 carbon atoms. 제16항에 있어서, X가 다음의 구조식을 갖는 것을 특징으로 하는 소독제의 조제방법：17. The method for preparing a disinfecting agent according to claim 16, wherein X has the following structural formula: 여기서, R1은 4개 내지 18개의 탄소원자를 갖는 알킬기와 1개 내지 18개의 탄소원자를 갖는 하이드록시 알킬기로 구성된 그룹에서 선택되며, R2는 8개 내지 18개의 탄소원자를 갖는 알킬기를 나타낸다.Wherein R 1 is selected from the group consisting of an alkyl group having from 4 to 18 carbon atoms and a hydroxyalkyl group having from 1 to 18 carbon atoms and R 2 represents an alkyl group having from 8 to 18 carbon atoms. 제19항에 있어서, 상기 살균성 포스페이트 에스테르가 다음의 구조식을 갖는 것을 특징으로 하는 소독제의 조제방법：20. The method of preparing a disinfecting agent according to claim 19, wherein the bactericidal phosphate ester has the following structural formula: 여기서, R은 수소나 C2H5를 나타낸다.Here, R represents hydrogen or C 2 H 5 . 제16항에 있어서, X가 4급 아민이고 R은 수소인 것을 특징으로 하는 소독제의 조제방법.17. The method of claim 16, wherein X is a quaternary amine and R is hydrogen. 제21항에 있어서, 살균성 포스페이트 유도체가 다음의 구조식을 갖는 4급 아민임을 특징으로 하는 소독제의 조제방법：The method of claim 21, wherein the bactericidal phosphate derivative is a quaternary amine having the following structure: 여기서, R1은 4개 내지 18개의 탄소원자를 갖는 알킬기와 1개 내지 18개의 탄소원자를 갖는 하이드록시 알킬기로 구성된 그룹에서 선택되며；R2은 8개 내지 18개의 탄소원자를 갖는 알킬기를 나타낸다.Wherein R 1 is selected from the group consisting of an alkyl group having 4 to 18 carbon atoms and a hydroxyalkyl group having 1 to 18 carbon atoms and R 2 represents an alkyl group having 8 to 18 carbon atoms. 제22항에 있어서, 상기의 살균성 포스페이트 에스테르가 다음의 구조식을 갖는 것을 특징으로 하는 소독제의 조제방법：23. The method of preparing a disinfecting agent according to claim 22, wherein the bactericidal phosphate ester has the following structural formula: 여기서, R은 H나 C2H5를 나타낸다.Here, R represents H or C 2 H 5 . 다음의 과정과 같이；(가)약 1몰 내지 2몰의 비스(하이드록시 에틸) 코코아민으로 인산을 중화시키고, (나)이 혼합물을 약 0.01-70%(중량비)의 농도로 물과 혼합하여 얻는 소독제의 제조방법.(A) neutralizing phosphoric acid with about 1 to 2 moles of bis (hydroxyethyl) cocoamine, (b) mixing the mixture with water at a concentration of about 0.01 to 70% (weight ratio) Wherein the disinfecting agent is obtained by a method comprising the steps of: 다음의 과정과 같이；(가)적어도 하나의 하이드록시기를 갖는 포스페이트 유도체를 얻기 위해, 약 60-120℃에서 약 1몰 내지 3몰의 하이드록시 알킬, 아릴, 아라릴이나 알카릴 화합물을 포스포러스 펜톡사이드와 반응시키고, (나)이 혼합물을 약 0.01% 내지 70%(중량비)의 농도로 물과 혼합하여 얻는 소독제의 제조방법.(A) about 1 to 3 moles of a hydroxyalkyl, aryl, aralyl or alkaryl compound at about 60-120 DEG C to obtain a phosphate derivative having at least one hydroxy group, (B) mixing the mixture with water at a concentration of about 0.01% to 70% (weight ratio). 제25항에 있어서, 상기 하이드록시 알킬기는 1개 내지 18개의 탄소 원자를 갖는 것을 특징으로 하는 소독제의 제조방법.26. The method of claim 25, wherein the hydroxyalkyl group has from 1 to 18 carbon atoms. 제25항에 있어서, (가)단계의 생성물을 약 0.5몰 내지 1.5몰의 3급 아민으로 반응시키는데, 이 3급 아민은 8개 내지 18개의 탄소원자를 갖는 알킬기로 구성되는 한 개의 치환체를 가지며, 다른 두 알킬기(즉, 4개 내지 18개의 탄소원자를 갖는 알킬기와, 1개 내지 18개의 탄소원자를 갖는 하이드록시 알킬기로 구성되는 그룹에서 선택된 것)를 두 치환체로 가지는 것을 특징으로 하는 소독제의 제조방법.26. The method of claim 25, wherein the product of step (a) is reacted with from about 0.5 mole to about 1.5 moles of a tertiary amine, said tertiary amine having one substituent consisting of an alkyl group having from 8 to 18 carbon atoms, Wherein the substituent is selected from the group consisting of two different alkyl groups (i.e., an alkyl group having 4 to 18 carbon atoms and a hydroxyalkyl group having 1 to 18 carbon atoms). 제27항에 있어서, 3급 아민은 비스(하이드록시 에틸) 코코아민인 것을 특징으로 하는 소독제의 제조방법.28. The method of claim 27, wherein the tertiary amine is bis (hydroxyethyl) cocoamine. 다음의 과정과 같이；(가)포스트페이트 유도체를 얻기 위해, 약 60℃ 내지 120℃에서 포스포러스 펜톡사이드의 몰당 약 1몰 내지 3몰의 하이드록시 알킬, 아릴, 아라릴이나 알카릴 화합물을 포스포러스 펜톡사이드와 반응시키고, (나)이 생성물을 약 0.5몰 내지 1.5몰의 3급 아민과 반응시키는데, 이 3급아민은 8개 내지 18개의 탄소원자를 갖는 알킬기로 구성되는 한 개의 치환체를 갖고, 다른 두 종류의 알킬기(즉, 1개 내지 18개의 탄소원자를 갖는 알킬기와 1개 내지 18개의 탄소원자를 갖는 하이드록시 알킬기로 구성되는 그룹에서 선택된 것)를 두 개의 치환체로 가지며, (다)상기 (가)단계에서 얻은 혼합물을 약 0.01% 내지 70%(중량비)의 농도에서 액체와 혼합하여 얻는 소독제의 조제방법.(A) about 1 to 3 moles of a hydroxyalkyl, aryl, aralyl or alkaryl compound per mole of phosphorus pentoxide at about 60 ° C to 120 ° C to obtain a postpate derivative, (B) reacting the product with about 0.5 to 1.5 moles of a tertiary amine having one substituent consisting of an alkyl group having from 8 to 18 carbon atoms, Having two substituents other than the two alkyl groups (i.e., those selected from the group consisting of an alkyl group having 1 to 18 carbon atoms and a hydroxyalkyl group having 1 to 18 carbon atoms), and (c) ) Is obtained by mixing the mixture obtained in step (1) with a liquid at a concentration of about 0.01% to 70% (weight ratio). ※ 참고사항：최초출원 내용에 의하여 공개하는 것임.※ Note: It is disclosed by the contents of the first application.
KR1019890700490A 1987-08-03 1988-08-03 Microbiocidal cleansing or disinfecting formulations and preparation thereof KR910005713B1 (en)

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