KR20230141001A - Solid carbonated bath composition containing melatonin and method for preparing the same - Google Patents
Solid carbonated bath composition containing melatonin and method for preparing the same Download PDFInfo
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- KR20230141001A KR20230141001A KR1020220039985A KR20220039985A KR20230141001A KR 20230141001 A KR20230141001 A KR 20230141001A KR 1020220039985 A KR1020220039985 A KR 1020220039985A KR 20220039985 A KR20220039985 A KR 20220039985A KR 20230141001 A KR20230141001 A KR 20230141001A
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- melatonin
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- 239000000203 mixture Substances 0.000 title claims abstract description 40
- YJPIGAIKUZMOQA-UHFFFAOYSA-N Melatonin Natural products COC1=CC=C2N(C(C)=O)C=C(CCN)C2=C1 YJPIGAIKUZMOQA-UHFFFAOYSA-N 0.000 title claims abstract description 35
- DRLFMBDRBRZALE-UHFFFAOYSA-N melatonin Chemical compound COC1=CC=C2NC=C(CCNC(C)=O)C2=C1 DRLFMBDRBRZALE-UHFFFAOYSA-N 0.000 title claims abstract description 35
- 229960003987 melatonin Drugs 0.000 title claims abstract description 35
- 239000007787 solid Substances 0.000 title claims abstract description 26
- 238000000034 method Methods 0.000 title claims description 4
- 239000007764 o/w emulsion Substances 0.000 claims abstract description 25
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000000654 additive Substances 0.000 claims abstract description 23
- 238000002156 mixing Methods 0.000 claims abstract description 22
- 230000000996 additive effect Effects 0.000 claims abstract description 17
- 238000004519 manufacturing process Methods 0.000 claims abstract description 13
- 239000000843 powder Substances 0.000 claims abstract description 11
- 239000013040 bath agent Substances 0.000 claims abstract description 9
- 239000003921 oil Substances 0.000 claims description 30
- 235000019198 oils Nutrition 0.000 claims description 30
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 28
- 239000004094 surface-active agent Substances 0.000 claims description 27
- 239000012071 phase Substances 0.000 claims description 18
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims description 14
- 235000017557 sodium bicarbonate Nutrition 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 13
- 150000007524 organic acids Chemical class 0.000 claims description 12
- 239000008346 aqueous phase Substances 0.000 claims description 7
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims description 6
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 claims description 4
- 235000020238 sunflower seed Nutrition 0.000 claims description 4
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 3
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 3
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 3
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 3
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 3
- 235000015165 citric acid Nutrition 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 239000001630 malic acid Substances 0.000 claims description 3
- 235000011090 malic acid Nutrition 0.000 claims description 3
- 235000016337 monopotassium tartrate Nutrition 0.000 claims description 3
- 238000000465 moulding Methods 0.000 claims description 3
- 235000005985 organic acids Nutrition 0.000 claims description 3
- KYKNRZGSIGMXFH-ZVGUSBNCSA-M potassium bitartrate Chemical compound [K+].OC(=O)[C@H](O)[C@@H](O)C([O-])=O KYKNRZGSIGMXFH-ZVGUSBNCSA-M 0.000 claims description 3
- 229940081543 potassium bitartrate Drugs 0.000 claims description 3
- 229940079776 sodium cocoyl isethionate Drugs 0.000 claims description 3
- 229940057950 sodium laureth sulfate Drugs 0.000 claims description 3
- 229940075560 sodium lauryl sulfoacetate Drugs 0.000 claims description 3
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 3
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical compound [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 claims description 3
- UAJTZZNRJCKXJN-UHFFFAOYSA-M sodium;2-dodecoxy-2-oxoethanesulfonate Chemical compound [Na+].CCCCCCCCCCCCOC(=O)CS([O-])(=O)=O UAJTZZNRJCKXJN-UHFFFAOYSA-M 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 235000002906 tartaric acid Nutrition 0.000 claims description 3
- 239000011975 tartaric acid Substances 0.000 claims description 3
- 240000004307 Citrus medica Species 0.000 claims description 2
- JDRSMPFHFNXQRB-CMTNHCDUSA-N Decyl beta-D-threo-hexopyranoside Chemical compound CCCCCCCCCCO[C@@H]1O[C@H](CO)C(O)[C@H](O)C1O JDRSMPFHFNXQRB-CMTNHCDUSA-N 0.000 claims description 2
- 235000018330 Macadamia integrifolia Nutrition 0.000 claims description 2
- 240000000912 Macadamia tetraphylla Species 0.000 claims description 2
- 235000003800 Macadamia tetraphylla Nutrition 0.000 claims description 2
- 244000018633 Prunus armeniaca Species 0.000 claims description 2
- 235000009827 Prunus armeniaca Nutrition 0.000 claims description 2
- 239000010478 argan oil Substances 0.000 claims description 2
- 239000010495 camellia oil Substances 0.000 claims description 2
- MRUAUOIMASANKQ-UHFFFAOYSA-O carboxymethyl-[3-(dodecanoylamino)propyl]-dimethylazanium Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC(O)=O MRUAUOIMASANKQ-UHFFFAOYSA-O 0.000 claims description 2
- 239000001926 citrus aurantium l. subsp. bergamia wright et arn. oil Substances 0.000 claims description 2
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 claims description 2
- 229940073507 cocamidopropyl betaine Drugs 0.000 claims description 2
- 229940073499 decyl glucoside Drugs 0.000 claims description 2
- 235000008524 evening primrose extract Nutrition 0.000 claims description 2
- 239000010475 evening primrose oil Substances 0.000 claims description 2
- 229940089020 evening primrose oil Drugs 0.000 claims description 2
- 239000003205 fragrance Substances 0.000 claims description 2
- 229940119170 jojoba wax Drugs 0.000 claims description 2
- 229940075468 lauramidopropyl betaine Drugs 0.000 claims description 2
- 229940094506 lauryl betaine Drugs 0.000 claims description 2
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 claims description 2
- DVEKCXOJTLDBFE-UHFFFAOYSA-N n-dodecyl-n,n-dimethylglycinate Chemical compound CCCCCCCCCCCC[N+](C)(C)CC([O-])=O DVEKCXOJTLDBFE-UHFFFAOYSA-N 0.000 claims description 2
- 239000010466 nut oil Substances 0.000 claims description 2
- 239000004006 olive oil Substances 0.000 claims description 2
- 235000008390 olive oil Nutrition 0.000 claims description 2
- 239000000049 pigment Substances 0.000 claims description 2
- FSYKKLYZXJSNPZ-UHFFFAOYSA-N sarcosine Chemical compound C[NH2+]CC([O-])=O FSYKKLYZXJSNPZ-UHFFFAOYSA-N 0.000 claims description 2
- 229940032094 squalane Drugs 0.000 claims description 2
- 239000010677 tea tree oil Substances 0.000 claims description 2
- 229940111630 tea tree oil Drugs 0.000 claims description 2
- 229940080421 coco glucoside Drugs 0.000 claims 1
- -1 jojoba oil Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 18
- 238000010521 absorption reaction Methods 0.000 abstract description 6
- 238000009472 formulation Methods 0.000 abstract description 4
- 238000012423 maintenance Methods 0.000 abstract description 4
- 210000003491 skin Anatomy 0.000 description 13
- 238000003287 bathing Methods 0.000 description 8
- 239000002537 cosmetic Substances 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
- 210000002615 epidermis Anatomy 0.000 description 4
- 210000000434 stratum corneum Anatomy 0.000 description 4
- 239000004480 active ingredient Substances 0.000 description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 2
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 2
- 230000017531 blood circulation Effects 0.000 description 2
- 239000001569 carbon dioxide Substances 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 210000004027 cell Anatomy 0.000 description 2
- 230000004060 metabolic process Effects 0.000 description 2
- 230000008092 positive effect Effects 0.000 description 2
- 230000007306 turnover Effects 0.000 description 2
- SGHZXLIDFTYFHQ-UHFFFAOYSA-L Brilliant Blue Chemical compound [Na+].[Na+].C=1C=C(C(=C2C=CC(C=C2)=[N+](CC)CC=2C=C(C=CC=2)S([O-])(=O)=O)C=2C(=CC=CC=2)S([O-])(=O)=O)C=CC=1N(CC)CC1=CC=CC(S([O-])(=O)=O)=C1 SGHZXLIDFTYFHQ-UHFFFAOYSA-L 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 description 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 1
- 102000011782 Keratins Human genes 0.000 description 1
- 108010076876 Keratins Proteins 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- 208000013738 Sleep Initiation and Maintenance disease Diseases 0.000 description 1
- 229930003268 Vitamin C Natural products 0.000 description 1
- 229930003427 Vitamin E Natural products 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 230000036528 appetite Effects 0.000 description 1
- 235000019789 appetite Nutrition 0.000 description 1
- 210000003403 autonomic nervous system Anatomy 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- UQWIHFJXDRNUDP-UHFFFAOYSA-N chembl1206007 Chemical compound COC1=CC(S(O)(=O)=O)=C(C)C=C1N=NC1=C(O)C=CC2=CC(S(O)(=O)=O)=CC=C12 UQWIHFJXDRNUDP-UHFFFAOYSA-N 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000004299 exfoliation Methods 0.000 description 1
- 230000037406 food intake Effects 0.000 description 1
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- 150000008131 glucosides Chemical class 0.000 description 1
- 210000003780 hair follicle Anatomy 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 206010022437 insomnia Diseases 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 239000000955 prescription drug Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000002040 relaxant effect Effects 0.000 description 1
- 230000000241 respiratory effect Effects 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- 230000009759 skin aging Effects 0.000 description 1
- 210000004927 skin cell Anatomy 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- KOJJEWBIWHKEIN-UHFFFAOYSA-N sodium 5-amino-4-hydroxy-3-phenyldiazenylnaphthalene-2,7-disulfonic acid Chemical compound C1=CC=C(C=C1)N=NC2=C(C3=C(C=C(C=C3C=C2S(=O)(=O)O)S(=O)(=O)O)N)O.[Na+] KOJJEWBIWHKEIN-UHFFFAOYSA-N 0.000 description 1
- 239000002438 stress hormone Substances 0.000 description 1
- 210000002820 sympathetic nervous system Anatomy 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- UJMBCXLDXJUMFB-UHFFFAOYSA-K trisodium;5-oxo-1-(4-sulfonatophenyl)-4-[(4-sulfonatophenyl)diazenyl]-4h-pyrazole-3-carboxylate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1N=NC1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-UHFFFAOYSA-K 0.000 description 1
- 210000001835 viscera Anatomy 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/062—Oil-in-water emulsions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/362—Polycarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/447—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof containing sulfur
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
- A61K8/492—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid having condensed rings, e.g. indol
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/22—Gas releasing
- A61K2800/222—Effervescent
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Emergency Medicine (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
본 개시는 멜라토닌을 함유하는 고체형 탄산 입욕제 조성물 및 이의 제조방법에 관한 것이다. 구체적으로, 본 발명의 일 측면에 의한 입욕제 첨가용 수중유형 조성물은 멜라토닌이 콜로이드 형태로 유상에 분산됨으로써 우수한 제형 안정성을 나타낼 수 있으며, 본 발명의 다른 측면에 의한 고체형 탄산 입욕제 조성물은 멜라토닌이 안정적으로 분산된 수중유형 조성물을 포함함으로써 우수한 멜라토닌의 경피 흡수 효과를 나타낼 수 있고, 본 발명의 또 다른 측면에 의한 고체형 탄산 입욕제 조성물의 제조방법은 수중유형 조성물과 분말상을 혼합한 후 구연산을 마지막 단계에서 혼합함으로써 우수한 기포 생성 및 유지 효과와 멜라토닌의 피부 전달력 증가 효과를 나타낼 수 있다.The present disclosure relates to a solid carbonated bath agent composition containing melatonin and a method for producing the same. Specifically, the oil-in-water composition for adding bath additives according to one aspect of the present invention can exhibit excellent formulation stability by dispersing melatonin in the oil phase in colloidal form, and the solid carbonated bath additive composition according to another aspect of the present invention has melatonin stable. By including an oil-in-water composition dispersed in , it is possible to exhibit an excellent transdermal absorption effect of melatonin, and the method for producing a solid carbonated bath composition according to another aspect of the present invention includes mixing the oil-in-water composition and the powder phase and then adding citric acid as the last step. By mixing in , excellent bubble creation and maintenance effects and an increase in melatonin's skin delivery ability can be achieved.
Description
본 개시는 멜라토닌을 함유하는 고체형 탄산 입욕제 조성물 및 이의 제조방법에 관한 것이다.The present disclosure relates to a solid carbonated bath agent composition containing melatonin and a method for producing the same.
멜라토닌(Melatonine)이란 뇌에서 생성되는 호르몬의 일종으로 흔히 불면증 치료에 사용되는 약물로서, 주로 복용하는 형태로 이용되고 있으며 요즘에 들어 화장품에 적용된 제품이 심심치 않게 출시되고 있다.Melatonin is a type of hormone produced in the brain and is a drug commonly used to treat insomnia. It is mainly used in the form of ingestion, and these days, cosmetic products are being released frequently.
화장품 원료로서의 멜라토닌은 복용 시와는 다르게 전문의약품으로 분류되지 않으며, 일반 화장품 원료로서 사용이 가능하다. 피부에 적용 시 1) 피부톤 회복 및 개선 2) 안티에이징 3) 피부노화 징후 반전 등의 효과가 대표적이라고 볼 수 있으며, 신체의 수면 및 각성주기를 개선하는데 도움이 되고 비타민 C와 비타민 E에 필적하는 항산화 특성이 있는 것으로 공지되어 있다. 또한, 인간의 피부와 모낭은 기능적 멜라토닌(Functional Melatonin)을 발현하며 이는 멜라토닌 합성에 상당히 기여하는 것으로 알려져 있으며, 이를 통해 멜라토닌이 단순히 화장품 원료로서 표피층에서만 작용하는 것뿐 아니라 피부를 통해 체내에 흡수되어 복용 시와 유사한 효과를 보조적으로 발현할 수 있다는 것을 알 수 있다. Unlike when taken, melatonin as a cosmetic raw material is not classified as a prescription drug and can be used as a general cosmetic raw material. When applied to the skin, the main effects include 1) recovery and improvement of skin tone, 2) anti-aging, and 3) reversal of signs of skin aging. It helps improve the body's sleep and wake cycle and is comparable to vitamin C and vitamin E. It is known to have antioxidant properties. In addition, human skin and hair follicles express functional melatonin, which is known to significantly contribute to melatonin synthesis. Through this, melatonin not only acts in the epidermal layer as a cosmetic raw material, but is also absorbed into the body through the skin. It can be seen that similar effects as when taken can be achieved supplementally.
욕탕에 몸을 담구며 하는 목욕은 혈액순환 촉진, 호흡 순환계 개선, 면역력 증대, 식욕 억제, 대사 상승으로 인한 비만 개선 등의 여러 측면에서 연구되고 있다. 또한 목욕은 스트레스 호르몬을 억제하는 효과에 긍정적인 영향을 끼치는 것으로 알려져 있다. 이처럼 목욕은 단순히 피부의 표피층을 단정하게 하려는 화장품적인 효과에서 나아가 신체 내부적(자율신경계 및 교감신경계) 등에 영향을 주어 긍정적인 효과를 이끌어내는 행위이다. 목욕은 또한 근육을 이완시키고 피로를 푸는데 도움을 주어 숙면에도 도움을 줄 수 있다. 이러한 숙면은 신체 내부에서의 멜라토닌 생성에 큰 영향을 끼치게 되며 표피에 대한 영향을 넘어 신체 대사에 영향을 준다고 볼 수 있다.Bathing by soaking in a bath is being studied in many aspects, including promoting blood circulation, improving the respiratory circulatory system, increasing immunity, suppressing appetite, and improving obesity due to increased metabolism. Bathing is also known to have a positive effect on suppressing stress hormones. In this way, bathing is not simply a cosmetic effect that aims to neaten the epidermal layer of the skin, but is also an act that produces positive effects by influencing the body's internal organs (autonomic nervous system and sympathetic nervous system). Bathing can also help you sleep better by relaxing your muscles and helping relieve fatigue. This type of deep sleep has a significant impact on the production of melatonin within the body and can be seen to have an effect on body metabolism beyond its effect on the epidermis.
오랜시간 욕탕에 몸을 담구고 하는 반신욕과 같은 입욕의 효과는 체내적인 효과 외에 피부 표피/각질층에도 영향을 줄 수 있다. 피부는 일반적으로 28일의 턴오버(Turn over) 주기를 가지고 있다. 피부층의 세포가 새로 자라나고 오랜 세포들은 각질층으로 점점 밀려올라가다가 탈락하게 되는 것을 턴오버 주기라고 하는데, 목욕 행위는 이러한 주기를 물리적, 의도적으로 이끌어내어 각질층의 탈락을 유도할 수 있다. 20-30분의 입욕을 통해 불려진 각질층은 때밀기나 계면활성제를 통해 일정 수준까지 의도적으로 탈락을 시킬 수 있으며 이러한 행위로 얇아진 각질층에 유효성분을 도포한다면 일상에서 첩포하는 원료의 흡수율보다 더욱 높은 비율로 유효성분을 흡수시킬 수 있다.The effects of bathing, such as half-body bathing where you soak in a bath for a long time, can affect the skin's epidermis/stratum keratin in addition to the internal effects. Skin generally has a turnover cycle of 28 days. The turnover cycle is when new cells in the skin layer grow and old cells are gradually pushed up into the stratum corneum and then fall off. The act of bathing can physically and intentionally induce this cycle, leading to the exfoliation of the stratum corneum. The stratum corneum that has been softened by bathing for 20-30 minutes can be intentionally exfoliated to a certain level through scrubbing or surfactants. If the active ingredient is applied to the stratum corneum that has become thinner through these actions, the absorption rate is higher than the absorption rate of raw materials applied in daily life. The active ingredients can be absorbed.
본 발명은 일 측면에서, 멜라토닌이 콜로이드 형태로 유상에 분산되어 우수한 제형 안정성을 갖는 입욕제 첨가용 수중유형 조성물을 제공하는 것을 목적으로 한다.In one aspect, the purpose of the present invention is to provide an oil-in-water composition for adding bath additives in which melatonin is dispersed in an oil phase in colloidal form and has excellent formulation stability.
본 발명은 다른 측면에서, 멜라토닌이 안정적으로 분산된 수중유형 조성물을 포함함으로써 멜라토닌의 경피 흡수율이 증가된 고체형 탄산 입욕제 조성물을 제공하는 것을 목적으로 한다.In another aspect, the purpose of the present invention is to provide a solid carbonated bath composition with increased transdermal absorption rate of melatonin by including an oil-in-water composition in which melatonin is stably dispersed.
본 발명은 또 다른 측면에서, 수중유형 조성물과 분말상을 혼합한 후 구연산을 마지막 단계에서 혼합함으로써 우수한 기포 생성 및 유지 효과와 멜라토닌의 피부 전달력 증가 효과를 나타내는 고체형 탄산 입욕제 조성물의 제조방법을 제공하는 것을 목적으로 한다.In another aspect, the present invention provides a method for producing a solid carbonated bath composition that exhibits excellent bubble generation and maintenance effects and an increase in melatonin's skin delivery ability by mixing the oil-in-water composition and the powder phase and then mixing citric acid in the last step. The purpose is to
상기한 목적을 달성하기 위하여, 본 발명의 일 실시예는 액상형 계면활성제를 포함하는 수상부; 및 오일 및 멜라토닌을 포함하는 유상부를 포함하는, 입욕제 첨가용 수중유형 조성물을 제공한다.In order to achieve the above object, an embodiment of the present invention includes an aqueous phase containing a liquid surfactant; and an oil-in-water composition for adding a bath additive, comprising an oil phase containing oil and melatonin.
또한, 본 발명의 다른 실시예는, 입욕제 첨가용 수중유형 조성물; 중탄산나트륨 및 분말형 계면활성제를 포함하는 분말상; 및 구연산, 사과산, 주석산, 및 중주석산칼륨 중에서 선택된 하나 이상의 유기산을 포함하는, 고체형 탄산 입욕제 조성물을 제공한다.In addition, another embodiment of the present invention is an oil-in-water composition for adding bath additives; Powder form containing sodium bicarbonate and powdered surfactant; and at least one organic acid selected from citric acid, malic acid, tartaric acid, and potassium bitartrate.
또한, 본 발명의 다른 실시예는, (1) 상기 중탄산나트륨 및 분말형 계면활성제를 혼합하는 단계; (2) 액상형 계면활성제를 포함하는 수상부; 및 오일 및 멜라토닌을 포함하는 유상부를 교반하여 얻어진 수중유형 조성물을 상기 단계 (1)에서 얻어진 분말상과 혼합하는 단계; (3) 상기 단계 (2)에서 얻어진 혼합물에 상기 유기산을 투입하여 혼합하는 단계; 및 (4) 상기 단계 (3)에서 얻어진 혼합물을 성형 및 건조하여 고체형 탄산 입욕제 조성물을 제조하는 단계를 포함하는, 고체형 탄산 입욕제 조성물의 제조방법을 제공한다.In addition, another embodiment of the present invention includes the steps of (1) mixing the sodium bicarbonate and a powdered surfactant; (2) an aqueous phase containing a liquid surfactant; and mixing the oil-in-water composition obtained by stirring the oil phase containing oil and melatonin with the powder phase obtained in step (1); (3) adding and mixing the organic acid to the mixture obtained in step (2); and (4) manufacturing a solid carbonated bath additive composition by molding and drying the mixture obtained in step (3).
본 발명의 일 측면에 의한 입욕제 첨가용 수중유형 조성물은 멜라토닌이 콜로이드 형태로 유상에 분산됨으로써 우수한 제형 안정성을 나타낼 수 있다.The oil-in-water composition for adding bath additives according to one aspect of the present invention can exhibit excellent formulation stability by dispersing melatonin in the oil phase in colloidal form.
본 발명의 다른 측면에 의한 고체형 탄산 입욕제 조성물은 멜라토닌이 안정적으로 분산된 수중유형 조성물을 포함함으로써 우수한 멜라토닌의 경피 흡수 효과를 나타낼 수 있다.The solid carbonated bath composition according to another aspect of the present invention can exhibit an excellent transdermal absorption effect of melatonin by containing an oil-in-water composition in which melatonin is stably dispersed.
본 발명의 또 다른 측면에 의한 고체형 탄산 입욕제 조성물의 제조방법은 수중유형 조성물과 분말상을 혼합한 후 구연산을 마지막 단계에서 혼합함으로써 우수한 기포 생성 및 유지 효과와 멜라토닌의 피부 전달력 증가 효과를 나타낼 수 있다.The method for producing a solid carbonated bath composition according to another aspect of the present invention is to mix the oil-in-water composition and the powder phase and then mix citric acid in the last step, thereby showing excellent bubble creation and maintenance effects and an effect of increasing the skin delivery ability of melatonin. there is.
이하, 본 발명을 상세히 설명한다.Hereinafter, the present invention will be described in detail.
본 발명은 일 측면에서, 액상형 계면활성제를 포함하는 수상부; 및 오일 및 멜라토닌을 포함하는 유상부를 포함하는, 입욕제 첨가용 수중유형 조성물에 관한 것일 수 있다.In one aspect, the present invention includes an aqueous phase containing a liquid surfactant; and an oil-in-water composition for adding a bath additive, including an oil phase containing oil and melatonin.
일 실시예에 있어서, 상기 액상형 계면활성제는 수중유형의 제형 형성에 핵심적인 역할을 하는 성분으로서, 코코베타인, 데실글루코사이드, 코카미도프로필베타인, 라우라미도프로필베타인, 라우릴베타인 및 코코글루코사이드 중에서 선택된 하나 이상을 포함할 수 있다.In one embodiment, the liquid surfactant is a component that plays a key role in forming an oil-in-water formulation, and includes coco betaine, decyl glucoside, cocamidopropyl betaine, lauramidopropyl betaine, lauryl betaine, and coco. It may contain one or more selected from glucosides.
일 실시예에 있어서, 상기 오일은 스쿠알란, 타마누 오일, 마카다미아넛 오일, 해바라기씨 오일, 올리브 오일, 달맞이 꽃 오일, 아르간 오일, 살구씨 오일, 베르가못 오일, 동백 오일, 티트리 오일, 호호바 오일 및 유자씨 오일 및 해바라기씨 오일 중에서 선택된 하나 이상을 포함할 수 있다.In one embodiment, the oil includes squalane, tamanu oil, macadamia nut oil, sunflower seed oil, olive oil, evening primrose oil, argan oil, apricot seed oil, bergamot oil, camellia oil, tea tree oil, jojoba oil, and It may include one or more selected from citron seed oil and sunflower seed oil.
일 실시예에 있어서, 상기 수상부는 수용성 색소를 더 포함할 수 있다. 상기 수용성 색소는 예를 들어, 적색104호의(1), 적색227호, 적색40호, 적색504호, 황색4호, 황색5호 및 청색1호 등일 수 있으나, 이에 한정되는 것은 아니다.In one embodiment, the water-soluble portion may further include a water-soluble dye. The water-soluble pigment may be, for example, Red No. 104 (1), Red No. 227, Red No. 40, Red No. 504, Yellow No. 4, Yellow No. 5, and Blue No. 1, but is not limited thereto.
상기 유상부는 향오일을 더 포함할 수 있다.The oily part may further include fragrance oil.
본 발명은 다른 측면에서, 상기 입욕제 첨가용 수중유형 조성물; 중탄산나트륨 및 분말형 계면활성제를 포함하는 분말상; 및 구연산, 사과산, 주석산, 및 중주석산칼륨 중에서 선택된 하나 이상의 유기산을 포함하는, 고체형 탄산 입욕제 조성물에 관한 것일 수 있다.In another aspect, the present invention provides an oil-in-water composition for adding the bath additive; Powder form containing sodium bicarbonate and powdered surfactant; and one or more organic acids selected from citric acid, malic acid, tartaric acid, and potassium bitartrate.
본 발명의 다른 측면에 따른 고체형 탄산 입욕제 조성물은, 상기 입욕제 첨가용 수중유형 조성물을 포함함으로써, 중탄산나트륨, 구연산 및 물의 반응률이 높아지고 이에 따라 이산화탄소 발생에 따른 원재료들의 혼합이 보다 효과적으로 이루어질 수 있다.The solid carbonated bath agent composition according to another aspect of the present invention includes the oil-in-water composition for adding the bath agent, thereby increasing the reaction rate of sodium bicarbonate, citric acid, and water, and thus mixing the raw materials due to carbon dioxide generation can be performed more effectively.
또한, 본 발명의 다른 측면에 따른 고체형 탄산 입욕제 조성물은, 유상에 멜라토닌이 안정적으로 분산된 수중유형 조성물을 포함함으로써 우수한 멜라토닌의 경피 흡수 효과를 나타낼 수 있다.In addition, the solid carbonated bath composition according to another aspect of the present invention can exhibit an excellent transdermal absorption effect of melatonin by including an oil-in-water composition in which melatonin is stably dispersed in the oil phase.
상기 중탄산나트륨은 인체에 자극은 주지 않으면서 유기산과의 반응에 의해 이산화탄소를 발생시키며 이러한 탄산기포는 혈류순환 개선, 세정작용, 피부 각질제거, 피부 보호막 형성에 기여할 수 있다.The sodium bicarbonate generates carbon dioxide by reacting with organic acids without irritating the human body, and these carbonate bubbles can contribute to improving blood circulation, cleansing, removing dead skin cells, and forming a skin protective film.
일 실시예에 있어서, 상기 분말형 계면활성제는 소듐라우릴설포아세테이트, 소듐코코일이세티오네이트, 소듐라우릴설페이트 및 소듐라우레스설페이트 중에서 선택된 하나 이상을 포함할 수 있다.In one embodiment, the powdered surfactant may include one or more selected from sodium lauryl sulfoacetate, sodium cocoyl isethionate, sodium lauryl sulfate, and sodium laureth sulfate.
일 실시예에 있어서, 상기 고체형 탄산 입욕제 조성물은 상기 중탄산나트륨 100 중량부를 기준으로, 상기 액상형 계면활성제를 0.01 내지 5 중량부, 상기 오일을 0.1 내지 10 중량부, 상기 멜라토닌을 0.01 내지 1 중량부, 상기 분말형 계면활성제을 0.1 내지 10 중량부 및 상기 유기산을 30 내지 70 중량부로 포함할 수 있다.In one embodiment, the solid carbonated bath additive composition contains 0.01 to 5 parts by weight of the liquid surfactant, 0.1 to 10 parts by weight of the oil, and 0.01 to 1 part by weight of the melatonin, based on 100 parts by weight of the sodium bicarbonate. , may include 0.1 to 10 parts by weight of the powdered surfactant and 30 to 70 parts by weight of the organic acid.
일 실시예에 있어서, 상기 고체형 탄산 입욕제 조성물은 상기 중탄산나트륨 100 중량부를 기준으로, 상기 액상형 계면활성제를 0.01 중량부 이상, 0.05 중량부 이상, 0.1 중량부 이상, 0.2 중량부 이상, 0.3 중량부 이상, 0.4 중량부 이상, 0.5 중량부 이상, 0.6 중량부 이상, 0.7 중량부 이상, 0.8 중량부 이상, 0.9 중량부 이상, 1 중량부 이상, 2 중량부 이상, 3 중량부 이상 또는 4 중량부 이상으로 포함할 수 있으며, 또한, 상기 중탄산나트륨 100 중량부를 기준으로, 상기 액상형 계면활성제를 5 중량부 이하, 4 중량부 이하, 3 중량부 이하, 2 중량부 이하, 1 중량부 이하, 0.9 중량부 이하, 0.8 중량부 이하, 0.7 중량부 이하, 0.6 중량부 이하, 0.5 중량부 이하, 0.4 중량부 이하, 0.3 중량부 이하, 0.2 중량부 이하, 0.1 중량부 이하 또는 0.05 중량부 이하로 포함할 수 있다.In one embodiment, the solid carbonated bath additive composition contains 0.01 part by weight, 0.05 part by weight, 0.1 part by weight, 0.2 part by weight, or 0.3 part by weight of the liquid surfactant based on 100 parts by weight of sodium bicarbonate. or more, 0.4 parts by weight or more, 0.5 parts by weight or more, 0.6 parts by weight or more, 0.7 parts by weight or more, 0.8 parts by weight or more, 0.9 parts by weight or more, 1 part by weight or more, 2 parts by weight or more, 3 parts by weight or more, or 4 parts by weight or more. It may contain more than 5 parts by weight, less than 4 parts by weight, less than 3 parts by weight, less than 2 parts by weight, less than 1 part by weight, and 0.9 parts by weight of the liquid surfactant based on 100 parts by weight of sodium bicarbonate. part or less, 0.8 part or less, 0.7 part or less, 0.6 part or less, 0.5 part or less, 0.4 part or less, 0.3 part or less, 0.2 part or less, 0.1 part or less, or 0.05 part or less. You can.
일 실시예에 있어서, 상기 고체형 탄산 입욕제 조성물은 상기 중탄산나트륨 100 중량부를 기준으로, 상기 오일을 0.1 중량부 이상, 0.2 중량부 이상, 0.4 중량부 이상, 0.6 중량부 이상, 0.8 중량부 이상, 1 중량부 이상, 2 중량부 이상, 3 중량부 이상, 4 중량부 이상, 5 중량부 이상, 6 중량부 이상, 7 중량부 이상, 8 중량부 이상 또는 9 중량부 이상으로 포함할 수 있으며, 또한, 상기 중탄산나트륨 100 중량부를 기준으로, 상기 오일을 10 중량부 이하, 9 중량부 이하, 8 중량부 이하, 7 중량부 이하, 6 중량부 이하, 5 중량부 이하, 4 중량부 이하, 3 중량부 이하, 2 중량부 이하, 1 중량부 이하, 0.8 중량부 이하, 0.6 중량부 이하, 0.4 중량부 이하 또는 0.2 중량부 이하로 포함할 수 있다.In one embodiment, the solid carbonated bath additive composition contains 0.1 part by weight or more, 0.2 part by weight or more, 0.4 part by weight or more, 0.6 part by weight or more, 0.8 part by weight or more, based on 100 parts by weight of sodium bicarbonate. It may contain at least 1 part by weight, at least 2 parts by weight, at least 3 parts by weight, at least 4 parts by weight, at least 5 parts by weight, at least 6 parts by weight, at least 7 parts by weight, at least 8 parts by weight, or at least 9 parts by weight, In addition, based on 100 parts by weight of sodium bicarbonate, the oil may be added in an amount of 10 parts by weight or less, 9 parts by weight or less, 8 parts by weight or less, 7 parts by weight or less, 6 parts by weight or less, 5 parts by weight or less, 4 parts by weight or less, 3 parts by weight or less. It may include less than or equal to 2 parts by weight, less than or equal to 1 part by weight, less than or equal to 0.8 parts by weight, less than or equal to 0.6 parts by weight, less than or equal to 0.4 parts by weight, or less than or equal to 0.2 parts by weight.
일 실시예에 있어서, 상기 고체형 탄산 입욕제 조성물은 상기 중탄산나트륨 100 중량부를 기준으로, 상기 멜라토닌을 0.01 중량부 이상, 0.03 중량부 이상, 0.05 중량부 이상, 0.07 중량부 이상, 0.09 중량부 이상, 0.1 중량부 이상, 0.2 중량부 이상, 0.3 중량부 이상, 0.4 중량부 이상, 0.5 중량부 이상, 0.6 중량부 이상, 0.7 중량부 이상, 0.8 중량부 이상 또는 0.9 중량부 이상으로 포함할 수 있으며, 또한, 상기 중탄산나트륨 100 중량부를 기준으로, 상기 멜라토닌을 1 중량부 이하, 0.9 중량부 이하, 0.8 중량부 이하, 0.7 중량부 이하, 0.6 중량부 이하, 0.5 중량부 이하, 0.4 중량부 이하, 0.3 중량부 이하, 0.2 중량부 이하, 0.1 중량부 이하, 0.09 중량부 이하, 0.07 중량부 이하, 0.05 중량부 이하 또는 0.03 중량부 이하로 포함할 수 있다.In one embodiment, the solid carbonated bath composition contains 0.01 parts by weight or more, 0.03 parts by weight, 0.05 parts by weight, 0.07 parts by weight or more, 0.09 parts by weight or more, based on 100 parts by weight of sodium bicarbonate. It may contain at least 0.1 part by weight, at least 0.2 part by weight, at least 0.3 parts by weight, at least 0.4 parts by weight, at least 0.5 parts by weight, at least 0.6 parts by weight, at least 0.7 parts by weight, at least 0.8 parts by weight, or at least 0.9 parts by weight, In addition, based on 100 parts by weight of sodium bicarbonate, the melatonin is added in an amount of 1 part by weight or less, 0.9 parts by weight or less, 0.8 parts by weight or less, 0.7 parts by weight or less, 0.6 parts by weight or less, 0.5 parts by weight or less, 0.4 parts by weight or less, 0.3 parts by weight or less. It may include less than 0.2 parts by weight, less than 0.1 parts by weight, less than 0.09 parts by weight, less than 0.07 parts by weight, less than 0.05 parts by weight, or less than 0.03 parts by weight.
일 실시예에 있어서, 상기 고체형 탄산 입욕제 조성물은 상기 중탄산나트륨 100 중량부를 기준으로, 상기 분말형 계면활성제를 0.1 중량부 이상, 0.2 중량부 이상, 0.4 중량부 이상, 0.6 중량부 이상, 0.8 중량부 이상, 1 중량부 이상, 2 중량부 이상, 3 중량부 이상, 4 중량부 이상, 5 중량부 이상, 6 중량부 이상, 7 중량부 이상, 8 중량부 이상 또는 9 중량부 이상으로 포함할 수 있으며, 또한, 상기 중탄산나트륨 100 중량부를 기준으로, 상기 분말형 계면활성제를 10 중량부 이하, 9 중량부 이하, 8 중량부 이하, 7 중량부 이하, 6 중량부 이하, 5 중량부 이하, 4 중량부 이하, 3 중량부 이하, 2 중량부 이하, 1 중량부 이하, 0.8 중량부 이하, 0.6 중량부 이하, 0.4 중량부 이하 또는 0.2 중량부 이하로 포함할 수 있다.In one embodiment, the solid carbonated bath additive composition contains 0.1 part by weight or more, 0.2 part by weight, 0.4 part by weight, 0.6 part by weight, or 0.8 part by weight, based on 100 parts by weight of sodium bicarbonate. It may contain at least 1 part by weight, at least 1 part by weight, at least 2 parts by weight, at least 3 parts by weight, at least 4 parts by weight, at least 5 parts by weight, at least 6 parts by weight, at least 7 parts by weight, at least 8 parts by weight, or at least 9 parts by weight. Additionally, based on 100 parts by weight of sodium bicarbonate, the powdered surfactant may be used in an amount of 10 parts by weight or less, 9 parts by weight or less, 8 parts by weight or less, 7 parts by weight or less, 6 parts by weight or less, 5 parts by weight or less, It may contain 4 parts by weight or less, 3 parts by weight or less, 2 parts by weight or less, 1 part by weight or less, 0.8 parts by weight or less, 0.6 parts by weight or less, 0.4 parts by weight or less, or 0.2 parts by weight or less.
일 실시예에 있어서, 상기 고체형 탄산 입욕제 조성물은 상기 중탄산나트륨 100 중량부를 기준으로, 상기 유기산을 30 중량부 이상, 32 중량부 이상, 34 중량부 이상, 36 중량부 이상, 38 중량부 이상, 40 중량부 이상, 42 중량부 이상, 44 중량부 이상, 46 중량부 이상, 48 중량부 이상, 50 중량부 이상, 52 중량부 이상, 54 중량부 이상, 56 중량부 이상, 58 중량부 이상, 60 중량부 이상, 62 중량부 이상, 64 중량부 이상, 66 중량부 이상 또는 68 중량부 이상으로 포함할 수 있으며, 또한, 상기 중탄산나트륨 100 중량부를 기준으로, 상기 유기산을 70 중량부 이하, 68 중량부 이하, 66 중량부 이하, 64 중량부 이하, 62 중량부 이하, 60 중량부 이하, 58 중량부 이하, 56 중량부 이하, 54 중량부 이하, 52 중량부 이하, 50 중량부 이하, 48 중량부 이하, 46 중량부 이하, 44 중량부 이하, 42 중량부 이하, 40 중량부 이하, 38 중량부 이하, 36 중량부 이하, 34 중량부 이하 또는 32 중량부 이하로 포함할 수 있다.In one embodiment, the solid carbonated bath additive composition contains 30 parts by weight or more, 32 parts by weight, 34 parts by weight, 36 parts by weight, or more, 38 parts by weight or more, based on 100 parts by weight of sodium bicarbonate. 40 parts by weight or more, 42 parts by weight or more, 44 parts by weight or more, 46 parts by weight or more, 48 parts by weight or more, 50 parts by weight or more, 52 parts by weight or more, 54 parts by weight or more, 56 parts by weight or more, 58 parts by weight or more, It may contain more than 60 parts by weight, more than 62 parts by weight, more than 64 parts by weight, more than 66 parts by weight, or more than 68 parts by weight, and based on 100 parts by weight of sodium bicarbonate, the organic acid is added in an amount of 70 parts by weight or less, 68 parts by weight or less. Not more than 66 parts by weight, not more than 64 parts by weight, not more than 62 parts by weight, not more than 60 parts by weight, not more than 58 parts by weight, not more than 56 parts by weight, not more than 54 parts by weight, not more than 52 parts by weight, not more than 50 parts by weight, 48 It may include less than or equal to 46 parts by weight, less than or equal to 44 parts by weight, less than or equal to 42 parts by weight, less than or equal to 40 parts by weight, less than or equal to 38 parts by weight, less than or equal to 36 parts by weight, less than or equal to 34 parts by weight, or less than or equal to 32 parts by weight.
본 발명은 또 다른 측면에서, (1) 상기 중탄산나트륨 및 분말형 계면활성제를 혼합하는 단계; (2) 액상형 계면활성제를 포함하는 수상부; 및 오일 및 멜라토닌을 포함하는 유상부를 교반하여 얻어진 수중유형 조성물을 상기 단계 (1)에서 얻어진 분말상과 혼합하는 단계; (3) 상기 단계 (2)에서 얻어진 혼합물에 상기 유기산을 투입하여 혼합하는 단계; 및 (4) 상기 단계 (3)에서 얻어진 혼합물을 성형 및 건조하여 고체형 탄산 입욕제 조성물을 제조하는 단계를 포함하는, 상기 고체형 탄산 입욕제 조성물의 제조방법에 관한 것일 수 있다.In another aspect, the present invention includes the steps of (1) mixing the sodium bicarbonate and a powdered surfactant; (2) an aqueous phase containing a liquid surfactant; and mixing the oil-in-water composition obtained by stirring the oil phase containing oil and melatonin with the powder phase obtained in step (1); (3) adding and mixing the organic acid to the mixture obtained in step (2); and (4) manufacturing a solid carbonated bath agent composition by molding and drying the mixture obtained in step (3).
일 실시예에 있어서, 상기 단계 (1) 내지 (3)의 혼합은 각각 30초 내지 5분동안 수행될 수 있다.In one embodiment, the mixing of steps (1) to (3) may be performed for 30 seconds to 5 minutes each.
일 실시예에 있어서, 상기 단계 (1)의 혼합은 버티컬 믹서를 사용하여, 30초 이상, 40초 이상, 50초 이상, 60초 이상, 70초 이상, 80초 이상, 90초 이상, 120초 이상, 150초 이상 또는 180초 이상의 시간 동안 수행될 수 있으며, 또한, 300초 이하, 240초 이하, 180초 이하, 150초 이하, 120초 이하, 90초 이하, 80초 이하, 70초 이하 또는 60초 이하의 시간 동안 수행될 수 있다.In one embodiment, the mixing in step (1) is performed using a vertical mixer for 30 seconds or more, 40 seconds or more, 50 seconds or more, 60 seconds or more, 70 seconds or more, 80 seconds or more, 90 seconds or more, and 120 seconds. It may be performed for 150 seconds or more, or 180 seconds or more, and may also be performed for 300 seconds or less, 240 seconds or less, 180 seconds or less, 150 seconds or less, 120 seconds or less, 90 seconds or less, 80 seconds or less, 70 seconds or less. It can be performed for less than 60 seconds.
일 실시예에 있어서, 상기 단계 (2) 및 (3)의 혼합은 각각 30초 이상, 60초 이상, 90초 이상, 120초 이상, 150초 이상, 180초 이상, 210초 이상 또는 240초 이상, 270초 이상의 시간 동안 수행될 수 있으며, 또한, 300초 이하, 270초 이하, 240초 이하, 210초 이하, 180초 이하, 150초 이하, 120초 이하, 90초 이하 또는 60초 이하의 시간 동안 수행될 수 있다.In one embodiment, the mixing of steps (2) and (3) is performed for at least 30 seconds, at least 60 seconds, at least 90 seconds, at least 120 seconds, at least 150 seconds, at least 180 seconds, at least 210 seconds, or at least 240 seconds. , may be performed for a time of 270 seconds or more, and may also be performed for a time of 300 seconds or less, 270 seconds or less, 240 seconds or less, 210 seconds or less, 180 seconds or less, 150 seconds or less, 120 seconds or less, 90 seconds or less, or 60 seconds or less. It can be performed during
상기 고체형 탄산 입욕제 조성물의 제조방법은, 상기 수중유형 조성물과 분말상을 혼합한 후 단계 (3)에서 구연산을 별도로 혼합함으로써 우수한 기포 생성 및 유지 효과를 나타내는 입욕제 조성물을 제조할 수 있으며, 또한, 상기 방법에 의해 제조된 입욕제 조성물은 유효성분인 멜라토닌의 피부 전달력 증가 효과를 나타낼 수 있다.The method for producing the solid carbonated bath agent composition includes mixing the oil-in-water composition and the powder phase and then separately mixing citric acid in step (3) to produce a bath agent composition that exhibits excellent bubble generation and retention effects. The bath additive composition prepared by this method can exhibit the effect of increasing the skin delivery ability of melatonin, an active ingredient.
상기 분말형 계면활성제, 오일, 액상형 계면활성제, 멜라토닌, 유기산, 수상부 및 유상부에 관한 상세한 설명은 위에서 설명한 바와 같으므로 이하 생략한다.Detailed descriptions of the powdered surfactant, oil, liquid surfactant, melatonin, organic acid, aqueous phase, and oil phase are the same as described above and are therefore omitted hereinafter.
상기 고체형 탄산 입욕제 조성물의 제조방법은 위와 같이 수중유형 조성물과 분말상을 혼합한 후 마지막 단계에서 유기산을 혼합함으로써 우수한 기포 생성 및 유지 효과와 멜라토닌의 피부 전달력 증가 효과를 나타낼 수 있다.The method for producing the solid carbonated bath composition is as described above, mixing the oil-in-water composition and the powder phase, and then mixing the organic acid in the last step, which can exhibit excellent bubble creation and maintenance effects and an effect of increasing the skin delivery ability of melatonin.
Claims (11)
오일 및 멜라토닌을 포함하는 유상부를 포함하는,
입욕제 첨가용 수중유형 조성물.
An aqueous phase containing a liquid surfactant; and
Comprising an oily part containing oil and melatonin,
Oil-in-water composition for adding bath additives.
The oil-in-water type for adding bath additives according to claim 1, wherein the liquid surfactant includes one or more selected from coco betaine, decyl glucoside, cocamidopropyl betaine, lauramidopropyl betaine, lauryl betaine, and coco glucoside. Composition.
The method of claim 1, wherein the oil is squalane, tamanu oil, macadamia nut oil, sunflower seed oil, olive oil, evening primrose oil, argan oil, apricot seed oil, bergamot oil, camellia oil, tea tree oil, jojoba oil, and An oil-in-water composition for adding to a bath additive, comprising at least one selected from citron seed oil and sunflower seed oil.
The oil-in-water composition for adding a bath additive according to claim 1, wherein the water phase further includes a water-soluble pigment.
The oil-in-water composition for adding a bath additive according to claim 1, wherein the oil phase further includes a fragrance oil.
중탄산나트륨 및 분말형 계면활성제를 포함하는 분말상; 및
구연산, 사과산, 주석산, 및 중주석산칼륨 중에서 선택된 하나 이상의 유기산을 포함하는,
고체형 탄산 입욕제 조성물.
An oil-in-water composition for adding a bath additive according to any one of claims 1 to 5;
Powder form containing sodium bicarbonate and powdered surfactant; and
Containing one or more organic acids selected from citric acid, malic acid, tartaric acid, and potassium bitartrate,
Solid carbonated bath agent composition.
The solid carbonated bath composition according to claim 6, wherein the powdered surfactant includes at least one selected from sodium lauryl sulfoacetate, sodium cocoyl isethionate, sodium lauryl sulfate, and sodium laureth sulfate.
The method of claim 6, based on 100 parts by weight of the sodium bicarbonate, 0.01 to 5 parts by weight of the liquid surfactant, 0.1 to 10 parts by weight of the oil, 0.01 to 1 part by weight of the melatonin, and 0.1 part by weight of the powdered surfactant. A solid carbonated bath additive composition comprising from 10 to 10 parts by weight and 30 to 70 parts by weight of the organic acid.
(1) 상기 중탄산나트륨 및 분말형 계면활성제를 혼합하는 단계;
(2) 액상형 계면활성제를 포함하는 수상부; 및 오일 및 멜라토닌을 포함하는 유상부를 교반하여 얻어진 수중유형 조성물을 상기 단계 (1)에서 얻어진 분말상과 혼합하는 단계;
(3) 상기 단계 (2)에서 얻어진 혼합물에 상기 유기산을 투입하여 혼합하는 단계; 및
(4) 상기 단계 (3)에서 얻어진 혼합물을 성형 및 건조하여 고체형 탄산 입욕제 조성물을 제조하는 단계를 포함하는, 제조방법.
A method for producing a solid carbonated bath agent composition according to claim 6,
(1) mixing the sodium bicarbonate and powdered surfactant;
(2) an aqueous phase containing a liquid surfactant; and mixing the oil-in-water composition obtained by stirring the oil phase containing oil and melatonin with the powder phase obtained in step (1);
(3) adding and mixing the organic acid to the mixture obtained in step (2); and
(4) A manufacturing method comprising the step of manufacturing a solid carbonated bath additive composition by molding and drying the mixture obtained in step (3).
상기 단계 (1) 내지 (3)의 혼합은 각각 30초 내지 5분동안 수행되는, 제조방법.
According to clause 9,
The mixing of steps (1) to (3) is each performed for 30 seconds to 5 minutes.
상기 단계 (1)의 분말형 계면활성제는 소듐라우릴설포아세테이트, 소듐코코일이세티오네이트, 소듐라우릴설페이트 및 소듐라우레스설페이트 중에서 선택된 하나 이상을 포함하는, 제조방법.
According to clause 9,
The powdered surfactant of step (1) includes one or more selected from sodium lauryl sulfoacetate, sodium cocoyl isethionate, sodium lauryl sulfate, and sodium laureth sulfate.
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