KR20230060367A - Method to remove pesticide residue from vegetables - Google Patents
Method to remove pesticide residue from vegetables Download PDFInfo
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- KR20230060367A KR20230060367A KR1020210145019A KR20210145019A KR20230060367A KR 20230060367 A KR20230060367 A KR 20230060367A KR 1020210145019 A KR1020210145019 A KR 1020210145019A KR 20210145019 A KR20210145019 A KR 20210145019A KR 20230060367 A KR20230060367 A KR 20230060367A
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- vegetables
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- washing
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- 238000000034 method Methods 0.000 title claims abstract description 31
- 235000013311 vegetables Nutrition 0.000 title claims abstract description 27
- 239000000447 pesticide residue Substances 0.000 title claims abstract description 14
- 238000011282 treatment Methods 0.000 claims abstract description 42
- 238000005406 washing Methods 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000000575 pesticide Substances 0.000 claims abstract description 12
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229910052801 chlorine Inorganic materials 0.000 claims abstract description 11
- 239000000460 chlorine Substances 0.000 claims abstract description 11
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 10
- 238000009210 therapy by ultrasound Methods 0.000 claims abstract description 8
- 239000003610 charcoal Substances 0.000 claims abstract description 5
- 239000003599 detergent Substances 0.000 claims abstract description 5
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims abstract description 5
- 235000017557 sodium bicarbonate Nutrition 0.000 claims abstract description 5
- 239000008399 tap water Substances 0.000 claims abstract description 5
- 235000020679 tap water Nutrition 0.000 claims abstract description 5
- 239000000052 vinegar Substances 0.000 claims abstract description 5
- 235000021419 vinegar Nutrition 0.000 claims abstract description 5
- 239000012459 cleaning agent Substances 0.000 claims description 10
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 6
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 claims description 5
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 3
- 239000001569 carbon dioxide Substances 0.000 claims description 3
- 230000000813 microbial effect Effects 0.000 abstract description 3
- 239000004480 active ingredient Substances 0.000 abstract description 2
- 239000000796 flavoring agent Substances 0.000 abstract description 2
- 235000019634 flavors Nutrition 0.000 abstract description 2
- 238000011221 initial treatment Methods 0.000 abstract description 2
- 230000000694 effects Effects 0.000 description 2
- 235000012055 fruits and vegetables Nutrition 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 244000005700 microbiome Species 0.000 description 2
- 244000298479 Cichorium intybus Species 0.000 description 1
- 235000007542 Cichorium intybus Nutrition 0.000 description 1
- 240000008415 Lactuca sativa Species 0.000 description 1
- 235000003228 Lactuca sativa Nutrition 0.000 description 1
- 206010033546 Pallor Diseases 0.000 description 1
- 244000000231 Sesamum indicum Species 0.000 description 1
- 235000003434 Sesamum indicum Nutrition 0.000 description 1
- 244000300264 Spinacia oleracea Species 0.000 description 1
- 235000009337 Spinacia oleracea Nutrition 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 230000007059 acute toxicity Effects 0.000 description 1
- 231100000403 acute toxicity Toxicity 0.000 description 1
- 239000012773 agricultural material Substances 0.000 description 1
- 230000007665 chronic toxicity Effects 0.000 description 1
- 231100000160 chronic toxicity Toxicity 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 235000013348 organic food Nutrition 0.000 description 1
- 235000013324 preserved food Nutrition 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23N—MACHINES OR APPARATUS FOR TREATING HARVESTED FRUIT, VEGETABLES OR FLOWER BULBS IN BULK, NOT OTHERWISE PROVIDED FOR; PEELING VEGETABLES OR FRUIT IN BULK; APPARATUS FOR PREPARING ANIMAL FEEDING- STUFFS
- A23N12/00—Machines for cleaning, blanching, drying or roasting fruits or vegetables, e.g. coffee, cocoa, nuts
- A23N12/02—Machines for cleaning, blanching, drying or roasting fruits or vegetables, e.g. coffee, cocoa, nuts for washing or blanching
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/08—Cleaning involving contact with liquid the liquid having chemical or dissolving effect
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/10—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
- B08B3/12—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration by sonic or ultrasonic vibrations
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Preparation Of Fruits And Vegetables (AREA)
- Storage Of Fruits Or Vegetables (AREA)
Abstract
Description
본 발명은 채소의 잔류 농약 제거방법에 관한 것으로, 더욱 상세하게는 채소에 대한 농약 및 미생물 안전성에 효과적인 잔류 농약 제거방법에 관한 것이다.The present invention relates to a method for removing pesticide residues from vegetables, and more particularly, to a method for removing pesticide residues effective for the safety of pesticides and microorganisms for vegetables.
여기서는, 본 개시에 관한 배경기술이 제공되며, 이들이 반드시 공지기술을 의미하는 것은 아니다.BACKGROUND OF THE INVENTION Here, background art related to the present disclosure is provided, and they are not necessarily meant to be prior art.
경제성장에 따라 식생활에 있어서 유기농산물의 선호도 향상 및 농약 안전성에 많은 관심과 그에 따른 사회적 영향이 커져 가고 있으며, 신선하면서도 자연 성분이 그대로 보존된 식품을 선호하는 경향이 증가하고 있다. 그러나 구입 후 특별한 열처리나 조리과정 없이 생식으로 섭취되는 신선 농산물의 경우 미생물이나 농약 등의 안전성에 있어서 문제가 될 수 있다. In accordance with economic growth, a lot of interest in the improvement of preference for organic produce and the safety of pesticides in diet and the social impact thereof are growing, and the preference for fresh and preserved food with natural ingredients is increasing. However, in the case of fresh agricultural products that are consumed raw without special heat treatment or cooking after purchase, there may be a problem in the safety of microorganisms or pesticides.
최근 국내 유통되고 있는 과채류 12종, 총 289건에 대해 농약 잔류량을 분석한 결과 289건의 과채류 중 21.2%에서 잔류농약이 검출되었고, 5.2%가 잔류 농약 허용기준치를 초과하였으며, 부적합률이 높은 과채류는 깻잎, 상추, 시금치, 치커리 등의 순으로 나타났다. As a result of analyzing pesticide residues on a total of 289 cases of 12 types of fruits and vegetables currently circulating in Korea, residual pesticides were detected in 21.2% of 289 fruits and vegetables, and 5.2% exceeded the permitted standard for pesticide residues. Sesame leaves, lettuce, spinach, and chicory appeared in that order.
농약은 농산물의 생산증대를 위해 불가피하게 사용되는 농자재로 농약살포 중 발생하는 급성 독성 이외에도 농산물에 잔류하여 장기간에 걸친 섭취로 인체에 영향을 미치는 만성독성이 문제가 되고 있다. 또한 식품의 원료에 남아 있는 잔류 농약은 시간의 경과에 따라 소실될 뿐만 아니라 세척, 데치기, 가열 등의 과정으로 많은 양이 제거되는 것으로 알려져 있다. Pesticides are agricultural materials that are inevitably used to increase the production of agricultural products. In addition to acute toxicity generated during pesticide spraying, chronic toxicity that remains in agricultural products and affects the human body by long-term intake has become a problem. In addition, it is known that residual pesticides remaining in raw materials of food are not only lost over time, but also removed in large amounts through processes such as washing, blanching, and heating.
본 발명은 채소에 대한 농약 및 미생물 안전성에 효과적인 잔류 농약 제거방법을 제공하고자 한다. The present invention is to provide a pesticide residue removal method effective for pesticide and microbial safety for vegetables.
그러나 본 발명의 목적들은 상기에 언급된 목적으로 제한되지 않으며, 언급되지 않은 또 다른 목적들은 아래의 기재로부터 당업자에게 명확하게 이해될 수 있을 것이다.However, the objects of the present invention are not limited to the above-mentioned objects, and other objects not mentioned will be clearly understood by those skilled in the art from the description below.
본 발명은 세척제를 이용하여 세척하는 1차 처리단계; 및 상기 세척 후 염소용액 처리, 초음파 처리, 초임계 처리 및 오존수 처리 중 어느 하나 이상의 처리를 하는 2차 처리단계를 포함하는 채소의 잔류 농약 제거방법을 제공한다. The present invention includes a first treatment step of washing using a detergent; And it provides a method for removing residual pesticides from vegetables comprising a secondary treatment step of performing any one or more of chlorine solution treatment, ultrasonic treatment, supercritical treatment and ozonated water treatment after the washing.
상기 세척제는 수돗물, 베이킹소다 용액, 숯을 담가둔 물 또는 식초 용액을 포함하는 것을 특징으로 한다.The cleaning agent is characterized in that it comprises tap water, baking soda solution, charcoal soaked water or vinegar solution.
또한 상기 1차 처리단계는 2종 이상의 세척제들을 순차적으로 처리하는 단계이고, 세척제 처리 시간은 5 내지 15분인 것을 특징으로 한다.In addition, the first treatment step is a step of sequentially treating two or more types of cleaning agents, and the cleaning agent treatment time is characterized in that 5 to 15 minutes.
또한 상기 염소용액 처리는 상기 1차 처리된 채소를 60 내지 100ppm 의 염소 용액에 1 내지 3분간 침지하는 방법이고, 상기 초음파 처리는 상기 1차 처리된 채소를 24 내지 45kHz의 초음파가 발생되는 세척기로 3 내지 8분간 처리하는 방법이며, 상기 초임계 처리는 상기 1차 처리된 채소를 초임계 상태의 이산화탄소로 10 내지 30초간 처리하는 방법이고, 상기 오존수 처리는 상기 1차 처리된 채소를 0.1 내지 0.5ppm의 오존이 발생되는 세척기로 3 내지 7분간 처리하는 방법인 것을 특징으로 한다.In addition, the chlorine solution treatment is a method of immersing the primary treated vegetables in a chlorine solution of 60 to 100 ppm for 1 to 3 minutes, and the ultrasonic treatment is a washing machine in which ultrasonic waves of 24 to 45 kHz are generated. The supercritical treatment is a method of treating the primary treated vegetables with supercritical carbon dioxide for 10 to 30 seconds, and the ozonated water treatment is a method of treating the primary treated vegetables with 0.1 to 0.5 It is characterized in that it is a method of treating for 3 to 7 minutes with a washing machine that generates ppm ozone.
또한 상기 2차 처리단계는 2종류 이상의 방법을 순차적으로 처리하는 단계인 것을 특징으로 한다.In addition, the secondary processing step is characterized in that it is a step of sequentially processing two or more types of methods.
본 발명은 채소에 대한 농약 및 미생물 안전성에 효과적이고, 채소의 유효 성분 및 향미 소실을 최소화할 수 있는 잔류 농약 제거방법을 제공할 수 있다. The present invention can provide a pesticide residue removal method that is effective for pesticide and microbial safety for vegetables and can minimize the loss of active ingredients and flavor of vegetables.
본 명세서에 사용되는 모든 기술용어 및 과학용어는 다른 언급이 없는 한은 기술적으로 통상의 기술을 가진 자에게 일반적으로 이해되는 것과 동일한 의미를 가진다. 또한 본 명세서 및 청구범위의 전반에 걸쳐, 다른 언급이 없는 한 포함(comprise, comprises, comprising)이라는 용어는 언급된 물건, 단계 또는 일군의 물건, 및 단계를 포함하는 것을 의미하고, 임의의 어떤 다른 물건, 단계 또는 일군의 물건 또는 일군의 단계를 배제하는 의미로 사용된 것은 아니다.All technical and scientific terms used herein have the same meaning as commonly understood by a person of ordinary skill in the art unless otherwise specified. Also throughout this specification and claims, the terms "comprise", "comprising", and "comprising", unless stated otherwise, are meant to include a stated object, step or group of objects, and steps, and any other It is not intended to exclude an object, step or group of objects or steps.
이하에 본 발명을 상세하게 설명하기에 앞서, 본 명세서에 사용된 용어는 특정의 실시예를 기술하기 위한 것일 뿐 첨부하는 특허청구의 범위에 의해서만 한정되는 본 발명의 범위를 한정하려는 것은 아님을 이해하여야 한다.Prior to describing the present invention in detail below, it is understood that the terms used herein are intended to describe specific embodiments and are not intended to limit the scope of the present invention, which is limited only by the appended claims. shall.
한편, 본 발명의 여러 가지 실시예들은 명확한 반대의 지적이 없는 한 그 외의 어떤 다른 실시예들과 결합될 수 있다. 특히 바람직하거나 유리하다고 지시하는 어떤 특징도 바람직하거나 유리하다고 지시한 그 외의 어떤 특징 및 특징들과 결합될 수 있다. 이하, 첨부된 도면을 참조하여 본 발명의 실시예 및 이에 따른 효과를 설명하기로 한다.On the other hand, various embodiments of the present invention can be combined with any other embodiments unless clearly indicated to the contrary. Any feature indicated as being particularly desirable or advantageous may be combined with any other features and characteristics indicated as being particularly desirable or advantageous. Hereinafter, embodiments of the present invention and effects thereof will be described with reference to the accompanying drawings.
본 발명의 일실시예에 따른 채소의 잔류 농약 제거방법은 세척제를 이용하여 세척하는 1차 처리단계 및 상기 세척 후 염소용액 처리, 초음파 처리, 초임계 처리 및 오존수 처리 중 어느 하나 이상의 처리를 하는 2차 처리단계를 포함하여 이루어진다. A method for removing pesticide residues from vegetables according to an embodiment of the present invention includes a first treatment step of washing with a detergent and after the washing, 2 treatments of any one or more of chlorine solution treatment, ultrasonic treatment, supercritical treatment and ozonated water treatment It consists of a tea processing step.
상기 1차 처리단계는 채소 중량 대비 8 내지 12배의 세척제에 담근 다음 흐르는 물에 세척하여 물기를 제거하는 단계이다. 상기 세척제는 수돗물, 베이킹소다(0.1~0.5%) 용액, 숯을 20 내지 25시간 담가둔 물(20g/L, pH 7.2) 또는 식초(3~7%) 용액을 사용한다. 세척제에 따른 잔류농약 평균 제거율은 숯을 담가둔 물, 베이킹 소다 용액, 수돗물, 식초 용액 순으로 높으며, 2종 이상의 세척제들을 순차적으로 처리하여 1차 처리할 수 있다. The first treatment step is a step of soaking in 8 to 12 times the weight of vegetables in a detergent and then washing with running water to remove moisture. The cleaning agent uses tap water, baking soda (0.1-0.5%) solution, water (20g/L, pH 7.2) in which charcoal has been soaked for 20-25 hours, or vinegar (3-7%) solution. The average pesticide residue removal rate according to the cleaning agent is high in the order of charcoal soaked water, baking soda solution, tap water, and vinegar solution, and the primary treatment can be performed by sequentially treating two or more types of cleaning agents.
상기 1차 처리단계에서 세척제 처리 시간은 5 내지 15분으로 이루어진다. The cleaning agent treatment time in the first treatment step consists of 5 to 15 minutes.
상기 2차 처리단계인 염소용액 처리는 상기 1차 처리된 채소들을 60 내지 100ppm 의 염소 용액에 1 내지 3분간 침지하는 방법이고, 초음파 처리는 상기 1차 처리된 채소들을 24 내지 45kHz의 초음파가 발생되는 세척기로 3 내지 8분간 처리하는 방법이며, 초임계 처리는 상기 1차 처리된 채소들을 초임계 상태의 이산화탄소로 10 내지 30초간 처리하는 방법이고, 오존수 처리는 상기 1차 처리된 채소들을 0.1 내지 0.5ppm의 오존이 발생되는 세척기로 3 내지 7분간 처리하는 방법이다. The secondary treatment step, the chlorine solution treatment, is a method of immersing the primary treated vegetables in a 60 to 100 ppm chlorine solution for 1 to 3 minutes, and the ultrasonic treatment is a method in which ultrasonic waves of 24 to 45 kHz are generated for the primary treated vegetables. Supercritical treatment is a method of treating the primary treated vegetables with carbon dioxide in a supercritical state for 10 to 30 seconds, and ozone water treatment is a method of treating the primary treated vegetables with 0.1 to 30 seconds. It is a method of treating for 3 to 7 minutes with a washing machine that generates 0.5 ppm ozone.
2차 처리방법에 따른 잔류농약 평균 제거율은 오존수 처리, 염소용액 처리, 초임계 처리, 초음파 처리 순으로 높으며, 2종류 이상의 방법을 순차적으로 처리하여 2차 처리할 수 있다. The average pesticide residue removal rate according to the secondary treatment method is high in the order of ozone water treatment, chlorine solution treatment, supercritical treatment, and ultrasonic treatment, and secondary treatment can be performed by sequentially treating two or more types of methods.
전술한 각 실시예에서 예시된 특징, 구조, 효과 등은 실시예들이 속하는 분야의 통상의 지식을 가지는 자에 의하여 다른 실시예들에 대해서도 조합 또는 변형되어 실시 가능하다. 따라서 이러한 조합과 변형에 관계된 내용들은 본 발명의 범위에 포함되는 것으로 해석되어야 할 것이다. The features, structures, effects, etc. illustrated in each of the above-described embodiments can be combined or modified with respect to other embodiments by those skilled in the art in the field to which the embodiments belong. Therefore, contents related to these combinations and variations should be construed as being included in the scope of the present invention.
Claims (4)
상기 세척 후 염소용액 처리, 초음파 처리, 초임계 처리 및 오존수 처리 중 어느 하나 이상의 처리를 하는 2차 처리단계를 포함하는 채소의 잔류 농약 제거방법으로서,
상기 세척제는 수돗물, 베이킹소다 용액, 숯을 담가둔 물 또는 식초 용액을 포함하는 것을 특징으로 하는 채소의 잔류 농약 제거방법.
A first treatment step of washing with a detergent; and
As a method for removing residual pesticides from vegetables comprising a secondary treatment step of performing any one or more of chlorine solution treatment, ultrasonic treatment, supercritical treatment and ozonated water treatment after the washing,
The cleaning agent is a pesticide residue removal method of vegetables, characterized in that it comprises tap water, baking soda solution, charcoal soaked water or vinegar solution.
상기 1차 처리단계는 2종 이상의 세척제들을 순차적으로 처리하는 단계이고, 세척제 처리 시간은 5 내지 15분인 것을 특징으로 하는 채소의 잔류 농약 제거방법.
According to claim 1,
The first treatment step is a step of sequentially treating two or more types of cleaning agents, and the cleaning agent treatment time is 5 to 15 minutes.
상기 염소용액 처리는 상기 1차 처리된 채소를 60 내지 100ppm 의 염소 용액에 1 내지 3분간 침지하는 방법이고,
상기 초음파 처리는 상기 1차 처리된 채소를 24 내지 45kHz의 초음파가 발생되는 세척기로 3 내지 8분간 처리하는 방법이며,
상기 초임계 처리는 상기 1차 처리된 채소를 초임계 상태의 이산화탄소로 10 내지 30초간 처리하는 방법이고,
상기 오존수 처리는 상기 1차 처리된 채소를 0.1 내지 0.5ppm의 오존이 발생되는 세척기로 3 내지 7분간 처리하는 방법인 것을 특징으로 하는 채소의 잔류 농약 제거방법.
According to claim 1,
The chlorine solution treatment is a method of immersing the primary treated vegetables in a chlorine solution of 60 to 100 ppm for 1 to 3 minutes,
The ultrasonic treatment is a method of treating the primary treated vegetables with a washing machine in which ultrasonic waves of 24 to 45 kHz are generated for 3 to 8 minutes,
The supercritical treatment is a method of treating the primary treated vegetable with carbon dioxide in a supercritical state for 10 to 30 seconds,
The ozonated water treatment is a method of removing pesticide residues from vegetables, characterized in that the method of treating the firstly treated vegetables with a washing machine generating 0.1 to 0.5 ppm ozone for 3 to 7 minutes.
상기 2차 처리단계는 2종류 이상의 방법을 순차적으로 처리하는 단계인 것을 특징으로 하는 채소의 잔류 농약 제거방법.According to claim 1,
The secondary treatment step is a method for removing pesticide residues from vegetables, characterized in that the step of sequentially processing two or more types of methods.
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