KR20200043014A - Deodoring Method of Aplysia kurodai and The Deodorant - Google Patents
Deodoring Method of Aplysia kurodai and The Deodorant Download PDFInfo
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- KR20200043014A KR20200043014A KR1020180123508A KR20180123508A KR20200043014A KR 20200043014 A KR20200043014 A KR 20200043014A KR 1020180123508 A KR1020180123508 A KR 1020180123508A KR 20180123508 A KR20180123508 A KR 20180123508A KR 20200043014 A KR20200043014 A KR 20200043014A
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- 238000000034 method Methods 0.000 title claims abstract description 19
- 239000002781 deodorant agent Substances 0.000 title claims 2
- 241000237372 Aplysia kurodai Species 0.000 title description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000000284 extract Substances 0.000 claims abstract description 29
- 239000005909 Kieselgur Substances 0.000 claims abstract description 11
- 239000004927 clay Substances 0.000 claims abstract description 11
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 11
- 241001374849 Liparis atlanticus Species 0.000 claims description 42
- 239000002253 acid Substances 0.000 claims description 5
- BVEAKNZZLSUYOU-UHFFFAOYSA-N decyl 3-decoxybenzoate Chemical compound C(CCCCCCCCC)OC(C1=CC(=CC=C1)OCCCCCCCCCC)=O BVEAKNZZLSUYOU-UHFFFAOYSA-N 0.000 claims description 4
- KWLMIXQRALPRBC-UHFFFAOYSA-L hectorite Chemical compound [Li+].[OH-].[OH-].[Na+].[Mg+2].O1[Si]2([O-])O[Si]1([O-])O[Si]([O-])(O1)O[Si]1([O-])O2 KWLMIXQRALPRBC-UHFFFAOYSA-L 0.000 claims description 4
- 229910000271 hectorite Inorganic materials 0.000 claims description 4
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 4
- 229910052622 kaolinite Inorganic materials 0.000 claims description 4
- 229920000609 methyl cellulose Polymers 0.000 claims description 4
- 239000001923 methylcellulose Substances 0.000 claims description 4
- 235000010981 methylcellulose Nutrition 0.000 claims description 4
- 230000002378 acidificating effect Effects 0.000 abstract description 7
- 241000237858 Gastropoda Species 0.000 abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 14
- 239000003795 chemical substances by application Substances 0.000 description 7
- 238000001914 filtration Methods 0.000 description 7
- 235000013305 food Nutrition 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 239000002537 cosmetic Substances 0.000 description 4
- 239000000654 additive Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 241000237852 Mollusca Species 0.000 description 2
- 239000004480 active ingredient Substances 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 230000006837 decompression Effects 0.000 description 2
- 239000000469 ethanolic extract Substances 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 241000237373 Aplysia sp. Species 0.000 description 1
- 241000282994 Cervidae Species 0.000 description 1
- 241000195628 Chlorophyta Species 0.000 description 1
- 241000283973 Oryctolagus cuniculus Species 0.000 description 1
- 241000199919 Phaeophyceae Species 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 238000013528 artificial neural network Methods 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 235000013601 eggs Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 238000007602 hot air drying Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 210000000653 nervous system Anatomy 0.000 description 1
- 210000002569 neuron Anatomy 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000011085 pressure filtration Methods 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000001223 reverse osmosis Methods 0.000 description 1
- 230000008786 sensory perception of smell Effects 0.000 description 1
- 235000015170 shellfish Nutrition 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000003828 vacuum filtration Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/20—Removal of unwanted matter, e.g. deodorisation or detoxification
- A23L5/27—Removal of unwanted matter, e.g. deodorisation or detoxification by chemical treatment, by adsorption or by absorption
- A23L5/273—Removal of unwanted matter, e.g. deodorisation or detoxification by chemical treatment, by adsorption or by absorption using adsorption or absorption agents, resins, synthetic polymers, or ion exchangers
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/20—Removal of unwanted matter, e.g. deodorisation or detoxification
- A23L5/27—Removal of unwanted matter, e.g. deodorisation or detoxification by chemical treatment, by adsorption or by absorption
- A23L5/276—Treatment with inorganic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/15—Inorganic Compounds
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- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- General Preparation And Processing Of Foods (AREA)
- Cosmetics (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Abstract
Description
본 발명은 바다달팽이의 냄새제거 방법 및 냄새제거제에 관한 것으로, 보다 상세하게는 바다달팽이에서 발생하는 특유의 냄새를 간단하고 저렴하면서도 효과적으로 제거할 수 있는 바다달팽이의 냄새제거 방법 및 냄새제거제에 관한 것이다.The present invention relates to an odor removing method and odor removing agent for sea snails, and more particularly, to a snail removing method and odor removing agent for simple and inexpensive and effective removal of peculiar odor generated from sea snails. .
바다달팽이는 무순목 군소과의 연체동물로 학명은 Aplysia kurodai이다. 몸의 길이는 약 40 cm 정도로 긴 달걀모양을 하고 있으며, 흑갈색 바탕에 회백색의 얼룩무늬를 가지고 있다. 머리에 더덤이를 갖고 있어 그 모습이 토끼와 닮아 sea hare라고 불린다. 주로 녹조와 갈조를 먹고 살며, 조개류와 같은 연체동물이지만 패각이 없고 대신 보라색 계열의 특이한 색소를 내뿜어 몸을 보호한다.The sea snail is a mollusk from the order of the order of the order of the order of the Aplysia kurodai. The body is about 40 cm long, egg-shaped, and has an off-white speckled pattern on a dark brown background. It has a deer on its head, so it looks like a rabbit and is called a sea hare. It mainly eats green algae and brown algae, and it is a mollusk like shellfish, but it has no shell and instead emits a unique purple-based pigment to protect the body.
바다달팽이는 고단백 저칼로리 식품이라 성장촉진과 성인병 예방에 도움이 된다고 알려져 있으며, 남부 지방을 중심으로 데쳐서 먹기도 한다. 바다달팽이에 대한 연구로 바다달팽이육의 단백질 및 아미노산 조성에 대해 연구하였고, 바다달팽이 알의 열수 추출물이 항암활성이 있음이 보고된 바 있으며, 이 외에도 바다달팽이 내장 추출물로부터 항산화 및 항균효과를 보고한 연구들이 있다. 또한 바다달팽이는 신경망이 단순하고 신경세포가 커서 신경계와 관련된 연구에 많이 이용되고 있다.Sea snail is a high-protein, low-calorie food that is known to help promote growth and prevent adult diseases. It is also eaten by boiling in the southern regions. As a study on sea snail, we studied the protein and amino acid composition of sea snail meat, and it has been reported that hot water extract of sea snail eggs has anti-cancer activity. In addition, it reported antioxidant and antibacterial effects from sea snail gut extract. There are studies. In addition, sea snails are used in research related to the nervous system because their neural networks are simple and their nerve cells are large.
하지만, 바다달팽이는 그 자체만으로도 영양성분이나 생리활성성분이 충분하여 식품학상 내지 화장품의 소재로써 그 잠재적 가치가 높은 것이 사실이지만, 특유의 냄새로 인해 제품화에 한계가 있고, 이를 위해 냄새를 효과적으로 저비용으로 제거할 수 있는 방법이 요구되고 있다. However, it is true that the sea snail has sufficient nutrients or physiologically active ingredients by itself, so it has high potential value as a material for food science or cosmetics. However, due to its characteristic odor, there is a limit to productization, and for this purpose, the odor is effectively low cost. There is a need for a method that can be removed.
이에 본 발명자들은 상기한 문제점을 해결하기 위하여 안출된 것으로, 그 목적은 바다달팽이에서 발생하는 특유의 냄새를 간단하고 저렴하면서도 효과적으로 제거할 수 있는 바다달팽이의 냄새제거 방법 및 냄새제거제를 제공함에 있다.Accordingly, the present inventors have been devised to solve the above-described problems, and the object is to provide a method and an odor removing agent for sea snails that can easily and effectively remove the peculiar smell generated from sea snails.
상기한 바와 같은 본 발명의 기술적 과제는 다음과 같은 수단에 의해 달성되어진다.The technical problem of the present invention as described above is achieved by the following means.
(1) 바다달팽이 추출물에 산성백토, 실리카, 규조토, 및 포졸란의 군에서 선택된 적어도 1종의 성분을 첨가하여 반응시켜 바다달팽이로부터 냄새를 제거하는 방법.(1) A method of removing odor from a sea snail by adding at least one component selected from the group of acid white clay, silica, diatomaceous earth, and pozzolan to the sea snail extract for reaction.
(2) 산성백토, 실리카, 규조토, 및 포졸란의 군에서 선택된 적어도 1종의 성분을 포함하는 바다달팽이의 냄새제거제. (2) Odor removing agent of sea snails comprising at least one component selected from the group of acidic white clay, silica, diatomaceous earth, and pozzolan.
(3) 상기 (2)에 있어서, 3-데실옥시벤조익애씨드데실에스터 0.1~0.5중량%, 메틸셀룰로즈 0.1~0.5중량%, 카올리나이트 0.1~0.2 중량%, 헥토라이트 0.1~0.2중량%, 및 베이델라이트 0.1~0.2중량%를 더 포함하는 것을 특징으로 하는 바다달팽이의 냄새제거제. (3) In the above (2), 3-decyloxybenzoic acid decyl ester 0.1 to 0.5% by weight, methyl cellulose 0.1 to 0.5% by weight, kaolinite 0.1 to 0.2% by weight, hectorite 0.1 to 0.2% by weight, and bay Odor remover of sea snails characterized in that it further comprises 0.1 to 0.2% by weight of delite.
상기와 같이 본 발명에 의하면, 바다달팽이에서 발생하는 특유의 냄새를 간단하고 저렴하면서도 효과적으로 제거할 수 있다.According to the present invention as described above, it is possible to simply and inexpensively and effectively remove the peculiar smell generated from sea snails.
상기한 목적을 달성하기 위하여 본 발명에 따른 바다달팽이의 냄새제거방법은, 바다달팽이의 추출물에 산성백토, 실리카, 규조토, 및 포졸란의 군에서 선택된 적어도 1종의 성분을 첨가하여 반응시키는 단계를 포함한다.In order to achieve the above object, the method for removing odor of sea snails according to the present invention includes reacting by adding at least one component selected from the group of acidic clay, silica, diatomaceous earth, and pozzolan to the extract of sea snails. do.
이하, 본 발명의 내용을 구체적으로 설명하면 다음과 같다.Hereinafter, the contents of the present invention will be described in detail.
본 발명에 따른 바다달팽이의 냄새제거방법은 산성백토, 실리카, 규조토, 및 포졸란의 군에서 선택된 적어도 1종의 성분을 냄새제거제의 활성성분으로 함유한다.The method for removing odor of sea snail according to the present invention contains at least one component selected from the group of acidic white clay, silica, diatomaceous earth, and pozzolan as an active ingredient of the odor removing agent.
상기 산성백토, 실리카, 규조토, 및 포졸란의 군에서 선택된 적어도 1종의 물질은 바다달팽이에 포함된 방향성 물질을 선택적으로 흡착하여 제거하는 효율이 높은 물질이다.The acidic clay, silica, diatomaceous earth, and at least one material selected from the group of pozzolans is a material having high efficiency for selectively adsorbing and removing aromatic substances contained in sea snails.
바람직하게는 산성백토, 실리카, 규조토, 및 포졸란이 각각 10~30중량%씩 조성된 것이다. 보다 바람직하게는 냄새성분의 흡착률을 보다 높이기 위해 상기 성분 외에 3-데실옥시벤조익애씨드데실에스터 0.1~0.5중량%, 메틸셀룰로즈 0.1~0.5중량%, 카올리나이트 0.1~0.2 중량%, 헥토라이트 0.1~0.2중량%, 및 베이델라이트 0.1~0.2중량%가 더 포함된다.Preferably, the acid white clay, silica, diatomaceous earth, and pozzolan are each composed of 10 to 30% by weight. More preferably, in order to further increase the adsorption rate of the odor component, 3-decyloxybenzoic acid decyl ester 0.1-0.5% by weight, methyl cellulose 0.1-0.5% by weight, kaolinite 0.1-0.2% by weight, hectorite 0.1- 0.2% by weight, and beiderite 0.1 to 0.2% by weight is further included.
본 발명에서 상기 냄새제거제를 이용하여 처리하고자 하는 바다달팽이 추출물 등을 함유하여 화장품의 원료 내지 각종 식품의 첨가물로써 제공되어질 수 있다.In the present invention, it can be provided as a raw material for cosmetics or as an additive for various foods by containing sea snail extract to be treated using the odor removing agent.
본 발명이 적용될 수 있는 상기 바다달팽이 추출물은 열수추출물, 에탄올 추출물 등 식품 첨가물로의 제조에 적용될 수 있는 다양한 방법에 의해 얻어질 수 있는 어떠한 추출물도 이용될 수 있음은 물론이다. 예를 들어, 열수추출물은 바다달팽이의 중량대비 1∼10배의 물을 가하여 1 내지 2기압, 80∼120℃하에 1∼12시간 추출한 것이 이용될 수 있으며, 에탄올 추출물의 경우 50 내지 100% 에탄올로 이루어진 추출용매를 이용할 수 있고, 초임계 추출물은 에탄올을 추출용매로 하여 250 내지 350bar의 압력하에 수행되어진 것이 이용될 수 있다. The sea snail extract to which the present invention can be applied can be used any extract that can be obtained by various methods that can be applied to the production of food additives such as hot water extract, ethanol extract, of course. For example, the hot water extract may be used to extract 1 to 12 hours under 1 to 2 atmospheres and 80 to 120 ° C by adding water 1 to 10 times the weight of sea snails, and in the case of ethanol extract, 50 to 100% ethanol An extraction solvent consisting of may be used, and a supercritical extract may be used that is performed under pressure of 250 to 350 bar using ethanol as an extraction solvent.
바다달팽이는 다양한 생리활성물질이나 영양성분을 함유하고 있지만, 특유의 냄새로 인해 대개는 폐기처리되고 있는 상황으로 전술한 바와 같이 화장품이나 각종 식품의 첨가물의 성분으로 활용이 가능한 점을 감안할 때, 냄새의 제거과정은 매우 중요하다.Sea snails contain a variety of physiologically active substances or nutrients, but given the fact that they can be used as ingredients in cosmetics or additives of various foods as described above, they are usually disposed of due to their characteristic odor. The removal process is very important.
상기와 같이 본 발명에 따른 냄새 제거반응은 진탕배양기 등을 이용하여 30~60분간 100~500rpm 하에 수행한 후, 감압여과하는 단계를 포함하는 것이 바람직하다.As described above, the odor removal reaction according to the present invention is preferably performed under 100 to 500 rpm for 30 to 60 minutes using a shake incubator or the like, and then includes filtering under reduced pressure.
본 발명에서 냄새제거제는 다양한 방법에 의해 얻어진 추출액에 대하여 10~30%(w/v), 바람직하게는 20%(w/v) 첨가하여 준다.In the present invention, the odor removing agent is added in an amount of 10 to 30% (w / v), preferably 20% (w / v) to the extract obtained by various methods.
감압여과과정은 바람직하게는 3M 페이퍼가 장착된 장비 내지는 통상적으로 사용되어지는 다른 어떠한 감압여과장치를 이용하여 수행되어질 수도 있다.The decompression filtration process may preferably be performed using equipment equipped with 3M paper or any other decompression filtration device commonly used.
예를 들어, 감압여과방법의 하나로 진공펌프를 이용하여 1기압 이하의 진공도를 유지하면서 연속적으로 수행할 수 있으며, 고압펌프를 이용하여 45~55kgf/cm2 정도의 압력으로 분당 10~14리터의 추출액을 역삼투막에 공급하여 염을 제거할 수 있으며, 이때 염이 제거된 추출액은 분당 1~3리터가 발생할 수 있다.For example, one of the pressure filtration method using a vacuum pump can be continuously carried out while maintaining the degree of vacuum of not more than 1 atmospheric pressure, of 45 ~ 55kgf / cm 2 between 10 and 14 liters per minute at a pressure of using the high-pressure pump The salt can be removed by supplying the extract to the reverse osmosis membrane. At this time, 1 to 3 liters per minute may be generated in the extract from which the salt has been removed.
상기와 같은 과정을 거쳐 간단하고 저렴한 방법으로 냄새가 제거된 바다달팽이의 추출액을 효과적으로 얻을 수 있다.Through the above process, it is possible to effectively obtain the extract of the sea snail with the odor removed in a simple and inexpensive way.
상기와 같이 얻어진 각 추출액들은 공지의 방법에 의해 건조과정(예로 동결건조, 열풍건조 등)에 의해 건조된 후, 분말화되어 식품 혹은 화장품 등의 첨가물로써 사용될 수 있다.Each of the extracts obtained as described above is dried by a drying method (for example, freeze drying, hot air drying, etc.) by a known method, and then powdered to be used as an additive for food or cosmetics.
이하 본 발명의 내용을 실시예를 참조하여 보다 상세하게 설명하고자 하나 이들 실시예는 본 발명의 내용을 이해하기 위한 것일 뿐 이에 의해 본 발명의 권리범위가 한정되는 것으로 해석되어져서는 아니된다.Hereinafter, the contents of the present invention will be described in more detail with reference to examples, but these examples are only for understanding the contents of the present invention and should not be interpreted as limiting the scope of the present invention.
[실시예 1][Example 1]
바다달팽이를 80℃ 열수를 이용하여 2시간 동안 추출하여 얻은 열수추출액을 진탕배양기에 넣고, 여기에 산성백토를 20%(w/v) 첨가하여 30분 동안 200rpm 하에 반응을 수행한 후, 감압여과하여 냄새가 제거된 바다달팽이 추출물을 얻었다.The sea snail was extracted by using 80 ° C hot water for 2 hours, and then the hot water extract obtained was placed in a shaker, and 20% (w / v) acidic clay was added thereto to carry out the reaction at 200 rpm for 30 minutes, followed by vacuum filtration. To obtain a sea snail extract with odor removed.
[실시예 2][Example 2]
바다달팽이를 80℃ 열수를 이용하여 2시간 동안 추출하여 얻은 열수추출액을 진탕배양기에 넣고, 여기에 실리카를 20%(w/v) 첨가하여 30분 동안 200rpm 하에 반응을 수행한 후, 감압여과하여 냄새가 제거된 바다달팽이 추출물을 얻었다.The sea snail was extracted by using 80 ° C hot water for 2 hours, and then the hot water extract obtained was placed in a shaker, and 20% (w / v) of silica was added thereto to perform a reaction at 200 rpm for 30 minutes, followed by filtration under reduced pressure. A sea snail extract with the odor removed was obtained.
[실시예 3][Example 3]
바다달팽이를 80℃ 열수를 이용하여 2시간 동안 추출하여 얻은 열수추출액을 진탕배양기에 넣고, 여기에 규조토를 20%(w/v) 첨가하여 30분 동안 200rpm 하에 반응을 수행한 후, 감압여과하여 냄새가 제거된 바다달팽이 추출물을 얻었다.The sea snail was extracted by using 80 ° C hot water for 2 hours, and then the hot water extract obtained was placed in a shaker, and 20% (w / v) of diatomaceous earth was added thereto to carry out the reaction at 200 rpm for 30 minutes, followed by filtration under reduced pressure. A sea snail extract with the odor removed was obtained.
[실시예 4][Example 4]
바다달팽이를 80℃ 열수를 이용하여 2시간 동안 추출하여 얻은 열수추출액을 진탕배양기에 넣고, 여기에 포졸란을 20%(w/v) 첨가하여 30분 동안 200rpm 하에 반응을 수행한 후, 감압여과하여 냄새가 제거된 바다달팽이 추출물을 얻었다.The sea snail was extracted by using 80 ° C hot water for 2 hours, and then the hot water extract obtained was placed in a shaker, and 20% (w / v) of pozzolanic acid was added thereto to carry out the reaction at 200 rpm for 30 minutes, followed by filtration under reduced pressure. A sea snail extract with the odor removed was obtained.
[실시예 5][Example 5]
바다달팽이를 80℃ 열수를 이용하여 2시간 동안 추출하여 얻은 열수추출액을 진탕배양기에 넣고, 여기에 산성백토, 실리카, 규조토, 및 포졸란이 20중량%, 20중량%, 30중량% 및 30중량%로 조성된 것을 20%(w/v) 첨가하여 30분 동안 200rpm 하에 반응을 수행한 후, 감압여과하여 냄새가 제거된 바다달팽이 추출물을 얻었다.The sea snail was extracted by using hot water at 80 ° C for 2 hours, and the hot water extract obtained was placed in a shaker, and acidic white clay, silica, diatomaceous earth, and pozzolan were 20%, 20%, 30%, and 30% by weight. 20% (w / v) was added, and the reaction was performed at 200 rpm for 30 minutes, followed by filtration under reduced pressure to obtain a sea snail extract with the odor removed.
[실시예 6][Example 6]
실시예 5에서 포졸란의 일부를 대체하여 3-데실옥시벤조익애씨드데실에스터 0.1중량%, 메틸셀룰로즈 0.1중량%, 카올리나이트 0.2 중량%, 헥토라이트 0.2중량%, 및 베이델라이트 0.2중량%를 첨가한 것을 제외하고는 동일한 방법에 의해 바다달팽이 추출물을 얻었다.In Example 5, a part of pozzolan was replaced with 0.1% by weight of 3-decyloxybenzoic acid decyl ester, 0.1% by weight of methyl cellulose, 0.2% by weight of kaolinite, 0.2% by weight of hectorite, and 0.2% by weight of beiderite The sea snail extract was obtained by the same method except that.
[실험예] 관능평가[Experimental Example] Sensory Evaluation
바다달팽이 추출물의 냄새 제거효과는 10인으로 이루어진 패널이 후각을 이용하여 직접 냄새를 맡는 방법에 의해 측정하였으며, 측정결과는 하기 표 1에 나타낸 바와 같이 5점 척도법을 이용하였다. 관능평가 중 비교예로 냄새제거를 하지 않은 상태의 것을 사용하였다.The odor removal effect of the sea snail extract was measured by a method in which a panel made of 10 persons smelled directly using the sense of smell, and the measurement result was a 5-point scale method as shown in Table 1 below. Among sensory evaluations, those without odor removal were used as comparative examples.
상기와 같이, 본 발명의 바람직한 실시 예를 참조하여 설명하였지만 해당 기술 분야의 숙련된 당업자라면 하기의 특허청구범위에 기재된 본 발명의 사상 및 영역으로부터 벗어나지 않는 범위 내에서 본 발명을 다양하게 수정 및 변경시킬 수 있음을 이해할 수 있을 것이다.As described above, although described with reference to preferred embodiments of the present invention, those skilled in the art will variously modify and change the present invention without departing from the spirit and scope of the present invention as set forth in the claims below. You can understand that you can.
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