KR20180065178A - A composition of hydrogel mask pack using mushroom mycelium and hydrogel mask pack containing the same as an active ingredient - Google Patents

Abstract

The present invention relates to a hydrogel mask pack composition using mushroom mycelium, and a hydrogel mask pack containing the same as an active ingredient. Specifically, the hydrogel mask pack produced by using the mushroom mycelia by the method of the present invention is excellent in overall satisfaction including skin feeling after an initial use, attachability during the use, softness, moisture retention functions, and moisturizing functions.

Description

FIELD OF THE INVENTION [0001] The present invention relates to a hydrogel mask pack composition using a mushroom mycelium, and a hydrogel mask pack containing the hydrogel mask pack composition as an effective ingredient. BACKGROUND OF THE INVENTION 1. Field of the Invention [0001]

The present invention relates to a hydrogel mask pack composition using mushroom mycelium and a hydrogel mask pack containing the same as an effective ingredient.

Skin that acts as a physical, chemical, and biological protection for the human body from the outside is aged by various factors. Aging can be divided into natural aging (internal aging) and aging (external aging) caused by continuous exposure to ultraviolet rays. In order to prevent skin aging and maintain healthy skin, it is important to consume functional foods or provide nutrition from outside.

Recently, interest in skin care has increased as interest in appearance has increased. In particular, packs are readily available at low cost and are preferred because they are easy to use. The pack wraps the active agent on the face to remove dirt from the pores and effectively supply moisture and cosmetic ingredients to the skin. In addition, it maintains blood circulation smoothly, restoring skin physiological function. Types of these packs include peel off, wash off, tissue off, patch, powder, sheet, and sleeping type. Among them, the sheet type includes a non-woven fabric, a hydrogel and a bio-cellulose by covering the face with a pack and then peeling it off. The nonwoven fabric is made of plant cellulosic fibers or synthetic fibers mainly obtained from cotton or pulp and is used as a freshwater body / mask-shaped support of cosmetic lotion. On the other hand, bio-cellulose is produced through cultivation of microorganisms, and is used as a material for an image processing agent for biological medicines and a mask pack for cosmetics. In addition, a hydrogel is an insoluble substance in a three-dimensional network structure formed by physicochemical crosslinking of a hydrophilic polymer, and contains a large amount of water or a biological fluid due to a hydrophilic functional group, a capillary and an osmotic phenomenon. The mask pack can give various feeling and efficacy depending on the material, kind, and raw material of the raw material, and various materials researches are being conducted to differentiate the mask pack.

Mushrooms are divided into acanthaceous fungi and basidiomycetes. Most mushrooms belong to the family Mycobacterium and consist of fungi with mycelium and reproductive organs. These mushrooms contain nutrients such as carbohydrates, proteins, vitamins, and minerals, which are more than ordinary vegetables, and have been used for many years as edible and medicinal because of its flavor and pharmacological effects.

Shiitake mushroom has been used for long time in the skin, diuretic, hypertension, asthma and gastric ulcer, and has antioxidant, antimicrobial, anticancer, weight and cholesterol lowering effect. Pleurotus ostreatus is a mushroom belonging to Pleurotus ostreatus, which has the effect of promoting blood circulation, antioxidation, hypoglycemia and anticancer effect. Zanthoxylum mushroom is an edible mushroom belonging to the wrinkle mushroom neck and pine mushroom, and has an efficacy such as immunity enhancement, anti-cancer and anti-hyperlipemia. It has anticancer activity, stimulating immune function, antioxidant, anti-inflammation, antimutagenesis and cell protection by the fungus belonging to the genus Mushroom and the mushroom belonging to beard mushroom. Cloudy mushroom has long been used as a dietary supplement or as a cure for mushrooms and mushrooms belonging to the mushroom family. It has anticancer, antiviral, antibacterial and antitumor effects.

The mushroom has the effects of anticancer effect, immunity enhancement, detoxification, antioxidation, skin whitening and wrinkle improvement, and pediatric atopic dermatitis. Throat mushroom is a mushroom belonging to the throat, throat, and throat. It has anti-corruption, anticancer, anti-mutation, hepatocyte injury inhibition, antioxidant, anti-diabetic and anti-inflammatory effects. The skimmer mushroom is a wrinkled mushroom, a mushroom belonging to the skirt mushroom, and it is difficult to use it as edible food. However, the polysaccharide obtained by liquid culture of mycelium is used as an industrial material. Skimmer mushrooms have effects such as wound healing, antibacterial, anti-inflammation, antioxidant and immune enhancement. Ganoderma lucidum has been treated as a medicinal mushroom in Asia for a long time ago, and has antioxidant, anti-inflammatory, anti-allergic and anti-cancer effects. Pine mushroom is a mushroom belonging to the pine mushroom and pine mushroom. It has anti-cancer, immunity enhancement, antioxidant and whitening effects.

Research on the various physiological activities of mushrooms and search for useful ingredients are continuously being carried out. For example, Korean Unexamined Patent Publication No. 10-1458496 discloses a composition for external application for anti-inflammation containing a fruiting body extract of avium mushroom, a mycelium extract of avocado mushroom, or a culture of mycelium of avium mushroom.

Accordingly, the inventors of the present invention completed the present invention by studying a method for utilizing mushroom as a material for functional cosmetics, confirming that the hydrogel mask pack manufactured using mushroom mycelium has excellent moisture retention and moisturizing ability.

It is an object of the present invention to provide a mask pack composition comprising mushroom mycelium.

In order to achieve the above object, the present invention provides a mask pack composition comprising mushroom mycelium or powder thereof.

The hydrogel mask pack manufactured using the mushroom mycelia by the method of the present invention is excellent in overall satisfaction including initial skin feeling, use feeling during use, softness, moisture retention and moisturizing.

BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a diagram illustrating a process for producing a hydrogel mask pack using mushroom mycelium; FIG.
FIG. 2A is a chart for confirming the growth rate of shiitake mushroom, oyster mushroom, pine nut mushroom and mushroom mushroom in a liquid medium.
FIG. 2B is a chart for confirming the growth rate of cloud mushroom, mushroom, thorn mushroom and skirt mushroom in a liquid medium.
FIG. 2c is a view for confirming the growth rate of Ganoderma lucidum and Matsutake mushroom in a liquid medium.
FIG. 3 is a view showing quality characteristics of a hydrogel mask pack sheet manufactured using mushroom mycelium.
FIG. 4 is a view showing the quality characteristics of the hydrogel mask pack sheet produced using the mushroom mycelium powder.

Hereinafter, the present invention will be described in detail.

The present invention provides a mask pack composition comprising mushroom mycelium or powder thereof.

The mushroom may be a shiitake mushroom, a mushroom mushroom, a pine nut mushroom, a cormorant mushroom, a cloud mushroom, a mushroom, a thorn mushroom, a skirting mushroom, a mushroom gruel or a mushroom mushroom. In one embodiment of the present invention, the mushroom may be any one or more selected from the group consisting of pine nut, cloud mushroom, skirt mushroom, gentian mushroom and mushroom mushroom.

The mushroom mycelium may be contained in an amount of 70 to 99 parts by weight, specifically 80 to 95 parts by weight, more particularly 85 to 95 parts by weight, based on the entire mask pack composition. In one embodiment of the present invention, the mushroom mycelium may be included in an amount of 90 parts by weight.

The powder may be contained in an amount of 1 to 10 parts by weight, specifically 1 to 5 parts by weight, more specifically 1 to 3 parts by weight, based on the entire mask pack composition. In one embodiment of the present invention, the powder may be included in 2 parts by weight.

The composition may further comprise a thickener and a moisturizer.

The thickening agent can control the internal resistance of the liquid, emulsion, and suspension (suspension) system to impart viscosity to the composition, prevent sagging and separation, and improve the flocculation effect and adhesion. Examples of the thickener include natural polymers such as gum arabic, carrageenan, galactan, agar, guar gum, pacific, mannan, wheat starch, rice starch, corn starch, potato starch, xanthan gum, tara gum, albumin, collagen, Cellulose, carboxymethylcellulose or its salts, carboxymethylethylcellulose or its salts, semi-synthetic polymers such as crystalline cellulose, hydroxyethylcellulose, hydroxymethylcellulose, methylhydroxypropylcellulose and carboxyvinyl polymer, sodium polyacrylate, sodium Polyvinyl alcohol, acrylate / C10-30 alkyl acrylate crosspolymer, acrylate / C12-22 alkyl methacrylate copolymer, acrylate / behenate-25 methacrylate copolymer, acrylate / Lt; / RTI > methacrylate copolymer, < RTI ID = 0.0 > Polyacrylate crosspolymer-6, ammonium acryloyldimethyltaurate / vinyl copolymer, and the like. However, it is preferable that the acrylic polymer is selected from the group consisting of Any of the enhancers known in the art can be used. In one embodiment of the present invention, the thickener may be guar gum.

Moisturizers can supply moisture to the skin, prevent moisture loss to the outside, restore skin barrier, help to spread moisture and restore the integrity of the cells. The humectant may be a water-soluble low molecular weight moisturizer, a lipid-soluble low molecular weight moisturizer, a water-soluble polymer, or a liposoluble polymer. Specifically, the water-soluble low-molecular moisturizing agent is selected from the group consisting of serine, glutamine, carrageenan, sorbitol, mannitol, sodium pyrrolidone-carboxylate, glycerin, propylene glycol, dipropylene glycol, isopropylene glycol, , Poly (ethylene glycol), polyethylene glycol B (polymerization degree n = 2 or more), polypropylene glycol (polymerization degree n = 2 or more), polyglycerin B (polymerization degree n = 2 or more), lactic acid or lactic acid salt. The liposoluble low molecular weight moisturizing agent may be cholesterol or cholesterol ester. The water-soluble polymer may be a carboxyvinyl polymer, polyaspartic acid salt, tragacanth, xanthan gum, methylcellulose, hydroxymethylcellulose, hydroxyethylcellulose, hydroxypropylcellulose, carboxymethylcellulose, water-soluble chitin, chitosan or dextrin . The oil-soluble polymer may be a polyvinylpyrrolidone / eicosene copolymer, a polyvinylpyrrolidone / hexadecene copolymer, a nitrocellulose, a dextrin fatty acid ester, or a polymeric silicone. However, the moisturizing agent may be any moisturizing agent known in the art. In one embodiment of the present invention, the humectant may be carrageenan and glycerin.

Further, the composition may further contain a stabilizer, a thickening agent, a moisturizing agent, a skin active ingredient, a perfume, and a preservative. The skin active ingredient, fragrance and preservative may contain ingredients conventionally used in cosmetic compositions.

In a specific embodiment of the present invention, the present inventors have made hydrogel mask packs using pine mushroom, cloud mushroom, skirt mushroom, Ganoderma mushroom and Pine Mushroom mycelium or powder thereof, which have a rapid growth rate (Figs. 1 to 4 and Table 1 to 5).

In addition, the inventors of the present invention confirmed that the hydrogel mask pack prepared by the method of the present invention is excellent in overall satisfaction including the first skin feeling, the close feeling during use, the softness, the water retention and the moisturizing effect (Table 6 and Table 7).

Hereinafter, the present invention will be described in detail by the following examples.

However, the following examples are illustrative of the present invention, and the contents of the present invention are not limited thereto.

< Example  1> Culture of the strain

<1-1> Solid culture of the strain

Ten mushroom strains distributed from the Agricultural Genetic Resources Information Center in Table 1 were cut into sterile 7 × 7 mm size and transplanted into a potato dextrose agar (PDA). The cells were cultured at 25 ° C for 1 week and transferred to a new PDA medium.

Types of cultivated mushroom and culture temperature number Strain Scientific name Temperature (℃) One Elevation Lentinula edodes (LE) 25-30 2 Oyster Pleurotus ostreatus (PO) 25 3 Pine nut Lentinus lepideus (LL) 25-30 4 Spindle Hericium erinaceus (HE) 25 5 cloud Coriolus versicolor (CV) 25 6 situation Phellinus linteus (PL) 25 7 Throat Auricularia auricula - judae (AA) 20-25 8 skirt Schizophyllum commune (SC) 25-30 9 wisdom Ganoderma lucidum (GL) 25-30 10 cluster Tricholoma matsutake (TM) 25

<1-2> Liquid culture of the strain

The mycelium of the strain cultured in the PDA medium of Example <1-1> was cut into a size of 7 x 7 mm. In a 250 ml flask, 100 ml of potato dextrose broth (PDB) was added, and 5 mycelium slices cut each strain were inoculated. After inoculation, the cells were cultured for 7 days with stirring at a temperature of 25 to 30 DEG C at a speed of 120 rpm. The primary cultured culture was subcultured by inoculating 10% of the culture volume, and the mycelial activity was maintained by periodic subculture once every 7 to 10 days depending on the degree of growth.

< Example  2> Identification of the growth rate of the strain

<2-1> Determination of the growth rate of the strain in a solid medium

The growth rate of the strain was determined by measuring the growth circle diameter of the strain on days 2, 4, 7, 10, and 14 with 0 day as the inoculation date of the mushroom strain inoculated in the PDA medium in Example <1-1>.

As a result, as shown in Table 2, the strains showing the highest growth rate in the PDA medium were Ganoderma Lucidum and Pine Mushroom, respectively, and the growth was completed after 4 days and 7 days after the start of the culture, respectively. Fourteen days after the start of the culture, the growth of cloud mushroom, gingko mushroom and pine mushroom was completed, and the growth of skirt mushroom was 74.50 mm (Table 2).

Growth rate of strain in solid medium Strain (mm)
Cultivation period (days) 2 4 7 10 14 Elevation 1.75 + 2.06 7.5 ± 3.56 18.00 ± 2.58 23.75 ± 3.40 44.75 ± 3.86 Oyster 1 ± 1.15 2.5 ± 0.58 7.00 ± 3.16 17.50 + - 9.54 33.00 ± 18.26 Pine nut 1.75 + 0.96 8.00 0.82 21.75 ± 2.36 34.75 + - 2.75 52.50 ± 5.80 Spindle - - - - 6.75 ± 3.77 cloud 2.5 ± 2.38 30.50 ± 2.89 76.75 ± 3.77 80.00 ± 0.00 ¹⁾ 80.00 ± 0.00 ¹⁾ situation 0.75 + 1.50 5.5 ± 4.51 13.00 5.10 22.00 ± 4.69 37.75 ± 3.69 Throat 1.50 ± 0.58 3.25 ± 0.50 16.00 ± 14.73 29.75 +/- 1.71 54.25 + - 3.40 skirt 3.00 ± 0.82 13.00 ± 1.41 43.00 + 2.94 64.75 + - 5.06 74.50 ± 3.70 wisdom 66.75 ± 1.89 80.00 ± 0.00 ¹⁾ 80.00 ± 0.00 ¹⁾ 80.00 ± 0.00 ¹⁾ 80.00 ± 0.00 ¹⁾ cluster 21.00 ± 2.31 70.25 + 1.50 80.00 ± 0.00 ¹⁾ 80.00 ± 0.00 ¹⁾ 80.00 ± 0.00 ¹⁾

1) means that the strain is fully grown in the petri dish at the time of solid culture, and the growth is completed.

<2-2> Identification of the growth rate of the strain in the liquid medium

On day 1, the inoculation date of the mushroom strain inoculated on the PDB medium in Example < 1-2 > was 0, and the culture solution inoculated with mycelium on days 1, 3, 5 and 7 was centrifuged at 10,000 rpm for 20 minutes to obtain a mycelium culture solution and a mycelium And the weight was measured to confirm growth rate.

As a result, as shown in Table 3 and Figs. 2A to 2C, the fastest growing mushroom mycelium and cloud mushroom showed 12.85 g and 12.32 g per 100 ml of culture medium after 7 days from the start of culture, The mushroom was 2.16 g which was slow in growth as in solid medium (Table 3 and Figures 2a-2c).

Growth rate of strain in liquid medium The strain (g / 100 ml)
Cultivation period (days) One 3 5 7 Elevation 1.76 3.91 6.17 7.40 Oyster 1.40 1.76 3.14 3.87 Pine nut 1.11 2.60 3.79 6.09 Spindle 0.85 1.59 1.90 2.16 cloud 1.42 6.58 10.33 12.32 situation 0.84 1.20 2.32 3.12 Throat 0.98 1.87 3.20 5.00 skirt 1.66 6.30 7.48 10.95 wisdom 8.06 9.91 12.05 12.85 cluster 1.15 4.38 5.88 6.15

< Manufacturing example  1> Mushroom  Mycelial Hydrogel Mask Pack  Manufacture of sheet

To prepare a hydrogel mask pack containing the pine nut mushroom mycelium, 90 parts by weight of pine nut mushroom was first mixed with carrageenan, guar gum, glycerin and purified water in the amounts listed in Table 4 below and heated to 85 ° C for 10 minutes . After the mixture was cooled to 75 캜, cellulose, a flavoring agent, a preservative and hyaluronic acid were added, and the mixture was stirred for 5 minutes to prepare a composition for a hydrogel mask pack. The composition and content of the specific mask pack are shown in Table 4 below. The composition was dispensed into a mask pack frame and dried to prepare a hydrogel mask pack (FIGS. 1 and 4).

Composition of hydrogel mask pack sheet containing mushroom mycelium ingredient Content (parts by weight) relative to the weight of the entire mask pack composition Carrageenan 0.5 Guar gum 0.5 glycerin 5.0 Xylitol 0.1 Hyaluronic acid 1.0 Dimethicone 0.1 1,3-butylene glycol 0.2 Cellulose 0.1 Sorbitol 0.1 Purified water 2.4

< Manufacturing example  2> Cloud mushroom  Mycelial Hydrogel Mask Pack  Manufacture of sheet

The same conditions and methods as those of Production Example 1 were used except that the mushroom mycelium was replaced with the mushroom mycelium.

< Manufacturing example  3> Skirt mushroom  Mycelial Hydrogel Mask Pack  Manufacture of sheet

The same conditions and methods as in Preparation Example 1 were used, except that the mycelia of skimmed mushrooms were used instead of the pine mushroom mycelium.

< Manufacturing example  4> Containing mycelia of Ganoderma lucidum Hydrogel Mask Pack  Manufacture of sheet

The same conditions and methods as in Preparation Example 1 were used except that the mycelia of Ganoderma lucidum were used instead of the pine needle mycelium.

< Manufacturing example  5> containing pine mushroom mycelium Hydrogel Mask Pack  Manufacture of sheet

The same conditions and methods as in Preparation Example 1 were used, except that pine mushroom mycelium was used instead of pine mushroom mycelium.

< Manufacturing example  6> Mushroom  Containing a powder of mycelium Hydrogel Mask Pack  Manufacture of sheet

In order to prepare a hydrogel mask pack containing powder of pine nut mushroom mycelium was centrifuged at 10,000 rpm for 20 minutes to separate the mycelia from the cultures of the strains cultivated in Example <1-2> And then lyophilized to prepare a mycelial powder. 2 parts by weight of the powder of the pine nut mushroom was mixed with carrageenan, guar gum, glycerin and purified water in the contents shown in the following Table 5 and completely dissolved by heating at 85 캜 for 10 minutes. After the mixture was cooled to 75 캜, cellulose, a perfume, a preservative and an active ingredient were added and stirred for 5 minutes to prepare a composition for a hydrogel mask pack. The composition and content of the specific mask pack are shown in Table 5 below. The composition was dispensed into a mask pack mold and dried to prepare a hydrogel mask pack (FIGS. 1 and 5).

Composition of hydrogel mask pack sheet containing powder of mushroom mycelium ingredient Content (parts by weight) relative to the weight of the entire mask pack composition Carrageenan 0.5 Guar gum 0.5 glycerin 5.0 Xylitol 0.1 Hyaluronic acid 1.0 Dimethicone 0.1 1,3-butylene glycol 0.2 Cellulose 0.1 Sorbitol 0.1 Purified water 90.4

< Manufacturing example  7> Cloud mushroom  Containing a powder of mycelium Hydrogel Mask Pack  Manufacture of sheet

Except that the powder of the cloud mushroom mycelium was used instead of the powder of the pine mushroom mycelium.

< Manufacturing example  8> Skirt mushroom  Containing a powder of mycelium Hydrogel Mask Pack  Manufacture of sheet

The same conditions and methods as those of Production Example 6 were used except that the powder of mycelia of skimmed mushrooms was used instead of the powder of pine mushroom mycelium.

< Manufacturing example  9> containing the powder of mycelia of Ganoderma lucidum Hydrogel Mask Pack  Manufacture of sheet

Was prepared in the same manner as in Preparation Example 6, except that the powder of the matsutake mushroom was used instead of the powder of the mushroom mycelium.

< Manufacturing example  10> containing the powder of mushroom mycelium Hydrogel Mask Pack  Manufacture of sheet

The same conditions and methods as those of Production Example 6 were used except that the powder of the pine mushroom mycelium was used instead of the powder of the pine nut mushroom.

< Experimental Example  1> Depending on the type of mushroom Hydrogel Mask Pack  Comparison of quality characteristics of sheet

The quality characteristics of the hydrogel mask pack sheets prepared in <Preparation Example 1> to <Preparation Example 10> were compared.

As a result, as shown in FIG. 3, in the case of the hydrogel mask pack sheet made of mushroom mycelium, there was a difference in the color, shape, and flavor of the gel depending on the type of mushroom mycelium (FIG. 3). In addition, as shown in Fig. 4, in the case of the hydrogel mask pack sheet made of powder of mushroom mycelium, the pine mushroom and the skirt mushroom showed aggregation of mycelia (Fig. 4).

< Experimental Example  2> Hydrogel Mask pack  Sensory evaluation

The hydrogel mask pack sheet prepared in <Preparation Example 1> to <Preparation Example 5> was impregnated into a commercially available non-woven mask pack, a vitamin wood mask pack (Samsung Medicinal, Korea) emulsion, and the sensory evaluation was performed.

Specifically, we selected 50 test subjects, used mask packs, and then selected the most preferred form for each item.

As a result, as shown in Table 6, the overall satisfaction of the mask pack manufactured using the mushroom mycelium was higher than that of the commercially available nonwoven mask pack, and in particular, the mushroom mushroom (Preparation 1) and the cloud mushroom One mask pack showed a high score in all items (Table 6).

Mask pack used for sensory evaluation Comparative Example 1 Vitamin tree mask pack Production Example 1 Pine nut (LL) Production Example 2 Cloud (CV) Production Example 3 Skirt (SC) Production Example 4 Ganoderma (GL) Production Example 5 Songyou (TM)

Analysis of Sensory Characteristics of Mask Pack division First use
Skin feeling (persons) in use
Closiness (person) in use
Softness (persons) in use
Water retention (persons) after use
Sensitivity (persons) Overall
Satisfaction (persons) Comparative Example 1 3 2 One 3 2 2 Production Example 1 12 10 16 14 13 16 Production Example 2 12 11 13 12 12 14 Production Example 3 9 9 9 10 10 8 Production Example 4 6 9 3 4 5 4 Production Example 5 8 9 8 7 8 6

Claims (8)

Mushroom mycelium or powder thereof.
The mask pack composition of claim 1, wherein the mushroom mycelium is selected from the group consisting of pine nut, cloud mushroom, skirt mushroom, gentian mushroom, and pine mushroom.
The mask pack composition according to claim 1, wherein the mushroom mycelium is contained in an amount of 70 to 99 parts by weight based on the whole mask pack composition.
The mask pack composition of claim 1, wherein the powder is included in 1 to 10 parts by weight based on the total mask pack composition.
The mask pack composition according to claim 1, wherein the composition further comprises an aging agent and a humectant.
6. The method of claim 5, wherein the thickening agent is selected from the group consisting of hydroxypropylmethylcellulose, sodium magnesium silicate, carrageenan, polyacrylate, polyvinyl alcohol, guar gum, Xanthan gum, tara gum, and mixtures thereof.
6. The composition of claim 5, wherein the humectant is selected from the group consisting of carrageenan, glycerin, propylene glycol, dipropylene glycol, butylene glycol, isopropylene glycol, pentylene glycol ) And arginine. &Lt; / RTI &gt;
The mask pack composition according to claim 1, wherein the composition further comprises a stabilizer, a thickening agent, a moisturizer, a skin active ingredient, a perfume, and a preservative.

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